FACTS SAMPLE COLLECTION SCREEN pgs

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United States Food and Drug Administration Collection Report For Sample Number: 2340 This is an accurate reproduction of the original electronic record as of 11/07/2003 Flag 301(k) Sample Episode Number Flag Remarks Origin Domestic Basis Compliance Sample Type Documentary Responsible Firm Dealer FIS Smpl Num Status 00908358 In Progress PAC 56002 Hours 8 FEI 3000901032 Compliance Num Related Smpl Number Date Collected Product Code 09/25/2000 60LBA05 Country of Origin Position Class 2 Sampling District NDC Number CHI-DO Permit Number Storage Rqrmnt Dealer is Consumer Crx/DEA Schedule Recall Num Consumer Compl. Num Brand Name No Product Description Aspirin Non-Rx Combination Tablet Product Label See continuation Reason for Collection Collected during EI of dealer, dated 9/20-25/2000 to document Interstate commerce and cGMP deviations. No analysis needed Firm Legal Name Wilson Pharmaceutical Woleske Chemical Wilaprin Arthritis Formula MFG Codes Expiration Date “Lot 25C83” (Finished Product) 8/06 “Batch 5564” (Active Ingredient) 8/02 Type of Firm Dealer Ingredient Supplier Carrier Name Roadway Firm FEI 3000901032 3000901033 FCE Address 300 Riverside Chicago, IL 60606 US 100 W. Main Kansas City, MO 64111 US Size of Lot 125 CS/12 BTLS/100 TAB Est. Value $4,500 Rcpt Type None Date Shipped 06/06/1999 Description of Sample Sample consists of 3 photographs and copies of records documenting interstate commerce and cGMP deficiencies for Wilaprin Arthritis Formula Method of Collection Copies of records collected during EI of dealer, dated 09/20-25/2000. Photographs taken 09/23/2000. How Prepared See continuation. Collector’s Identification on Package and/or Label “DOC 2340 9/25/00 SHR” Collector’s Identification on Seal “DOC 2340 9/25/00 Sylvia H. Rogers” Samples Delivered To Date Delivered Orig C/R & Records To CHI-DO Date: 11/07/2003 Page 1 of 3 United States Food and Drug Administration Collection Report For Sample Number: 2340 This is an accurate reproduction of the original electronic record as of 11/07/2003 Lab w/Split Sample Lab Document Number 1. 2. 3. 4. 5. 6. Document Date Document Type Document Remarks 09/25/2000 Affidavit Affidavit signed by Robert Wilson, President 06/16/2000 Invoice Invoice no. 2346 dated 06/16/2000 from Woleske Chemical, Kansas, MO for 1-250 lb drum of Acetylsalicylic Acid, batch 5564 06/16/2000 Bill of Lading Bill of Lading no. 124679 dated 06/16/2000 from Roadway Inc. Smith Center Kansas for shipment of 250 lbs of Acetylsalicylic Acid from Woleske Chemical, Kansas City, MO to Wilson Pharmaceutical, Inc. Chicago, IL Other Raw Material Inventory Card for Acetylsalicylic Acid Batch no. 5564 Other Photographs 1-3 of labeling for bulk 250 lb. Drum of Acetylsalicylic Acid, Batch 5564 Other Wilson Pharmaceuticals Batch Record for Wilaprin Arthritis Formula, lot 25C83 (25 pages) (Page 13, 14 and 15 contain copies of all labeling distributed with lot 25C83) Remarks See EIR of dealer and FDA-483, dated 9/20-25/2000 for more information. FDA-483 points 1-12 discuss deviations specific to this product. Payment Amount $0.00 Name of Signer Payment Method No Charge 704(d) Sample No 702(b) Portion Collector’s Name No Silvia H. Rogers Meaning Date & Time of Signature Date: 11/07/2003 Page 2 of 3 United States Food and Drug Administration Collection Report For Sample Number: 2340 This is an accurate reproduction of the original electronic record as of 11/07/2003 Product Label Finished product is labeled in part: “***WILAPRIN ARTHRITIS FORMULA 500 Tablets***Active Ingredients: Acetylsalicylic Acid…5000mg, Caffeine…32mg.***100 Tablets***Lot 25C83***EXP 8/06***Wilson Pharmaceuticals, Chicago, IL 60606”. Each bottle is placed in a white, paperboard box labeled in part, “*** WILAPRIN ARTHRITIS FORMULA *** 100 Tablets Active ingredients: Acetylsalicylic Acid…5000mg, Caffeine…32mg. ***Lot #25C83 Expires 8/06 *** Wilson Pharmaceuticals, ***”. White paperboard boxes are placed in brown cardboard cartons labeled in part, “*** WILAPRIN ARTHRITIS FORMULA***Wilson Pharmaceuticals***Lot 25C83***EXP8/06***” Active ingredient documented is Acetylsalicylic Acid packaged in 250 lb drum, labeled in part: “***Acetylsalicylic Acid, USP***Batch No 5564***Use by 8/02**Woleske Chemical, Kansas City, MO 64111***” How Prepared All records and photographs identified as below and submitted to Supervisory Investigator. Negatives and extra photos placed in 525, sealed as below and submitted to Supervisor. Date: 11/07/2003 Page 3 of 3

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