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Pesticide Analytical Manual Vol. II Pesticide Analytical Manual Volume II Alphabetical Index This index to Pesticide Analytical Manual Volume II (PAM II), methods for residues of individual pesticides, is alphabetical by name. Included as names are those used in Code of Federal Regulations Title 40 (40 CFR) and those treated as “preferred names” by U.S. Food and Drug Administration, with the former considered the main entry; FDA names cross-reference the 40 CFR name unless they are the same. For additional names for these and other pesticides, see FDA Glossary of Pesticide Chemicals, also available on the WWW site maintained by FDA’s Center for Food Safety and Applied Nutrition. Dates in this index are the transmittal dates of the PAM II published methods. Asterisks indicate that additional or new method(s) have been submitted to EPA but not compiled in PAM II. Users with a need for such methods may request copies from: (Mail) Mark Law US EPA/OPP/BEAD/ACB Environmental Science Center 701 Mapes Road Fort Meade, MD 20755-5350 (410) 305-2915 (TTY)* (410) 305-3091 ResidueMethods@epa.gov (Telephone) (Fax) (Email) In this index, many names appear in different order from the previous (published) index, which was alphabetized by hand with leading numbers and other characters ignored. In this index, names are alphabetized by computer using all characters, according to the following sequence: space ! + # $ % & + ( ) * + , - . / 0 1 2 3 4 5 6 7 8 9 : ; < = > ? @ ABCDEFGHIJKLMNOPQRSTUVWXYZ[\] If needed to permit a long chemical name to fit on additional lines, an “=” is used where no space or hyphen occurs in the actual name at that point. *Requestors who do not use TTY should first dial 711 to be connected with their state’s Relay Service, or dial the Relay Service directly. The telephone number is in the user’s local directory. The call will be answered by a live operator, to whom the requestor must give the EPA phone number above. The operator will complete the connection and assist in the conversation. January 2002 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 07/01/69 07/01/67 11/01/75 11/01/75 07/01/67 * 06/85* 11/01/73 05/84 11/01/75 11/01/75 06/85 * 7/15/68 12/31/74 07/01/67* 11/01/75 11/78 07/01/67* 10/77 07/01/67 12/82 09/91 12/31/74 11/84* 09/89* 12/31/74 07/78 07/01/69* 12/31/74 11/01/73 07/01/70 01/02/69 11/01/75 12/31/74 12/31/74 10/77 * 12/82 * (2-naphthyloxy)acetic acid, see naphthoxyacetic acid, beta- (revoked) 1,1-bis(p-chlorophenyl)-2,2,2-trichloroethanol (180.163) 1,1-dichloro-2,2-bis(p-ethylphenyl)ethane (revoked) 1,2,4,5-tetrachloro-3-nitrobenzene (revoked) 1,2-dibromo-3-chloropropane (revoked) (method for inorganic bromides) 1-((2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl)methyl)-1H-1,2,4-triazole (180.434) 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone (180.410) 1-chloro-2-nitropropane (revoked) 1-methylethyl 2-((ethoxy((1-methylethyl)amino)phosphinothioyl)oxy)benzoate (revoked) 1-naphthaleneacetic acid (180.155) 1-naphthylacetic acid, see 1-naphthaleneacetic acid (180.155) 2,2-dichlorovinyl dimethyl phosphate (180.235, 180.215, 185.1900) 2,2-dimethyl-1,3-benzodioxol-4-ol methylcarbamate (180.530) 2,3,5-triiodobenzoic acid (revoked) 2,3,6-trichlorophenylacetic acid (revoked) 2,4-D (180.142) 2,4-DB, see 4-(2,4-dichlorophenoxy)butyric acid (180.331) 2,4-dichloro p-nitrophenyl ether (revoked) 2,4-dichloro-6-o-chloroanilino-s-triazine (revoked) 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate (180.341, 186.2400) 2,6-dichloro-4-nitroaniline (180.200) 2,6-dimethyl-4-tridecylmorpholine (180.372) 2-((2-chlorophenyl)methyl)-4,4-dimethyl-3-isoxazolidinone (180.425) 2-((4-chloro-6-(ethylamino)-s-triazin-2-yl)amino)-2-methylpropionitrile (180.307) 2-(1-(ethoxyimino)butyl)-5-(2-(ethylthio)propyl)-3-hydroxy-2-cyclohexen-1-one (180.412) 2-(3,5-dichlorophenyl)-2-(2,2,2-trichloroethyl)-oxirane (180.424) 2-(m-chlorophenoxy)propionic acid (180.325) 2-(thiocyanomethylthio)benzothiazole (180.288) 2-chloro-1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate (180.252, 186.950) 2-chloro-1-(2,4-dichlorophenyl)vinyl diethyl phosphate (revoked) 2-chloro-N,N-diallylacetamide (revoked) 2-chloro-N-isopropylacetanilide (180.211) 2-chloroallyl diethyldithiocarbamate (revoked) 2-methyl-4-chlorophenoxyacetic acid (180.339) 3,4,5-trimethylphenyl methylcarbamate and 2,3,5-trimethylphenyl methylcarbamate (180.305) 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide (180.317) 3,5-dimethyl-4-(methylthio)phenyl methylcarbamate (revoked) 3,7-dichloro-8-quinolinecarboxylic acid (180.463) 3-(3,5-dichlorophenyl)-5-ethenyl-5-methyl-2,4-oxazolidinedione (180.380) 3-(dichloroacetyl)-5-(2-furanyl)-2,2-dimethyloxazolidine (180.471) * Method(s)have been submitted to EPA but not compiled in PAM II; request copies from EPA. January 2002 2-(4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl)-3-quinolinecarboxylic acid (180.426) 07/88 Index: Alphabetical–Page 2 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 10/77 07/01/69 11/01/75 12/31/74 * * 07/15/68 11/01/75* 12/31/74 12/31/74 12/31/74 12/82 10/77 * 10/77 * 09/83* 07/01/69* 11/84 11/01/75 07/01/67 11/01/73 06/86* 11/85 * 08/87* 11/01/75 06/86 06/86 07/01/67* 11/01/75 11/01/75 09/83 11/85 * 11/01/75 07/01/70 11/01/75 11/01/75 * 08/87 4,6-dinitro-o-cresol (180.344) 4,6-dinitro-o-cyclohexylphenol (revoked) 4-(2,4-dichlorophenoxy)butyric acid (180.331) 4-(2-methyl-4-chlorophenoxy) butyric acid (180.318) 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane (180.465) 4-(dichloroacetyl)-3,4-dihydro-3-methyl-2H-1,4-benzoxazine (180.460) 4-(methylsulfonyl)-2,6-dinitro-N,N-dipropylaniline (revoked) 4-amino-6-(1,1-dimethylethyl)-3-(methylthio)-1,2,4-triazin-5-(4H)-one (180.332, 185.250, 186.250) 4-aminopyridine (180.312) 4-AP, see 4-aminopyridine (180.312) 4-CPA, see chlorophenoxyacetic acid, p- (180.202) 5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole (180.370) 6-methyl-1,3-dithiolo[4,5-b]quinoxalin-2-one (180.338) abamectin, see Avermectin B1 (180.449) (several methods) acephate (180.108, revoked, 186.100) acetochlor (180.470) acifluorfen sodium, see sodium salt of acifluorfen (180.383) alachlor (180.249) aldicarb (180.269, 185.150, 186.150) aldrin (revoked) allethrin (180.113) allidochlor, see 2-chloro-N,N-diallylacetamide (revoked) aluminum tris(O-ethyl phosphonate) (180.415) ametryn (180.258) aminoethoxyvinylglycine (180.502) amitraz (180.287) (memo) ammoniates of (ethylenebis(dithiocarbamato)) zinc and ethylenebis(dithiocarbamic acid) (180.217) ammonium sulfamate (revoked) ammonium sulphamate, see ammonium sulfamate (revoked) anilazine, see 2,4-dichloro-6-o-chloroanilino-s-triazine (revoked) Aramite, see aramite (revoked) arsenic acid, see orthoarsenic acid (revoked) asulam (180.360) atrazine (180.220) Avermectin B1 (180.449) (several methods) azinphos-methyl, see O,O-dimethyl S-((4-oxo-1,2,3-benzotriazin-3(4H)-yl)methyl) phosphorodithioate (180.154) barban (180.268) basic copper carbonate (180.136) basic zinc sulfate (revoked) bendiocarb, see 2,2-dimethyl-1,3-benzodioxol-4-ol methylcarbamate (180.530) benfluralin, see N-butyl-N-ethyl-alpha, alpha, alpha-trifluoro-2,6-dinitro-p-toluidine (180.208) January 2002 Index: Alphabetical–Page 3 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 11/78* * * 11/01/73 11/78 07/01/70 * * 11/01/75 10/77 * 11/01/75 * 08/87 08/87 07/01/69 10/77 07/15/68 12/31/74 * 07/01/67 07/01/67 07/78 11/01/75* 11/01/75 08/87 * 11/01/75 10/77 * * 07/01/70 07/01/67 11/01/73 07/01/67 12/31/74 06/85 12/31/74 09/89 07/01/69 benomyl (180.294, 185.350, 186.350) benoxacor, see 4-(dichloroacetyl)-3,4-dihydro-3-methyl-2H-1,4-benzoxazine (180.460) bensulfuron methyl ester (180.445) bensulide, see S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide (180.241) bentazon (180.355, 186.375) benzadox (revoked) benzoic acid, 3,5-dimethyl-1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide (180.482) (1,1'-biphenyl)-4-yloxy-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, beta(180.457, 185.---, 186.---) BHC (revoked) bifenox (revoked) bifenthrin (180.442) biphenyl (revoked) bitertanol, see beta-(1,1'-biphenyl)-4-yloxy-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol (180.457, 185.---, 186.---) bromacil (180.210) bromoxynil (180.324) bufencarb (revoked, ) butralin (revoked) butylate, see S-ethyl diisobutylthiocarbamate (180.232) cacodylic acid (180.311) cadusafos (180.461) calcium arsenate (revoked) calcium cyanide (revoked) captafol (180.267) captan (180.103) carbaryl (180.169, 186.550) carbofuran (180.254, 185.600, 186.600) carbon disulfide (180.467) carbophenothion (revoked) carboxin (180.301) carfentrazone ethyl ester, see carfentrazone-ethyl (180.515) carfentrazone-ethyl (180.515) chloramben (revoked) chlorbenside (revoked) chlorbromuron (revoked) chlordane (revoked) chlordecone, see decachlorooctahydro-1,3,4-metheno-2H-cyclobuta(cd)pentalen-2-one (revoked) chlordimeform (revoked) chlorfenvinphos, see 2-chloro-1-(2,4-dichlorophenyl)vinyl diethyl phosphate (revoked) chlorimuron ethyl ester (180.429) chlorobenzilate, see ethyl 4,4'-dichlorobenzilate (revoked) January 2002 Index: Alphabetical–Page 4 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 07/01/69 12/31/74 11/01/75 07/01/69 07/01/67 06/01/68 07/01/67 07/01/70 07/15/68 11/01/75 10/77 07/88 11/84 11/84 11/01/75 * * 09/91 12/31/74 09/91 07/01/67 11/01/75 11/01/75 11/01/75 07/01/69 12/31/74 12/31/74 11/01/75* 12/31/74 12/82* 07/15/68 11/01/75 * * 06/86 11/85 11/85 12/31/74 06/86* 07/88 11/01/75* 07/01/70 chloroneb (180.257) chlorophenoxyacetic acid, p- (180.202) chlorophenyl phenyl sulfone, p- (revoked) chlorophenyl-2,4,5-trichlorophenyl sulfide, p- (revoked) chloropicrin (180.199) (method for inorganic bromides) chloropropylate (revoked) chlorosulfamic acid (revoked) chlorothalonil (180.275) chloroxuron (revoked) chlorpropham, see CIPC (180.181) chlorpyrifos (180.342, 185.1000, 186.1000) chlorpyrifos-methyl (180.419, 185.1050, 186.1050) chlorsulfuron (180.405) chlorthiophos (revoked) CIPC (180.181) clethodim (180.458, 186.1075) clofentezine (180.446, 185.---) (several methods) clomazone, see 2-((2-chlorophenyl)methyl)-4,4-dimethyl-3-isoxazolidinone (180.425) cloprop, see 2-(m-chlorophenoxy)propionic acid (180.325) clopyralid (180.431) coordination product of zinc ion and maneb (180.176, 185.6300, 186.6300) copper (185.1200) copper arsenate (revoked) copper monoethanolamine, see copper (185.1200) coumaphos (180.189) crotoxyphos, see dimethyl phosphate of alpha-methylbenzyl 3-hydroxy-cis-crotonate (revoked) crufomate (revoked) cryolite, see fluorine compounds (180.145, 185.3375) cyanazine, see 2-((4-chloro-6-(ethylamino)-s-triazin-2-yl)amino)-2-methylpropionitrile (180.307) cyano(3-phenoxyphenyl)methyl 4-chloro-alpha-(1-methylethyl)benzeneacetate (180.379) cycloate, see S-ethyl cyclohexylethylthiocarbamate (180.212) cycloheximide (revoked) cyfluthrin (180.436) cyhalothrin, lambda- (180.438, 185.1310) cyhexatin (180.144, 185.1350, 186.1350) cypermethrin (180.418) cypermethrin, zeta- (180.418) cyprazine (revoked) cyromazine (180.414) dalapon (revoked) daminozide (revoked) DCPA, see dimethyl tetrachloroterephthalate (180.185) January 2002 Index: Alphabetical–Page 5 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 11/01/75 12/31/74 07/01/67 10/77 12/31/74 12/31/74 11/01/75 07/01/70* 06/01/68 11/01/75 06/85 05/84 07/01/67 * 07/01/67 12/31/74 11/01/75 05/84 10/77 12/82 * 06/85 11/01/73 07/01/70 12/31/74 12/31/74 07/01/70 07/01/69 10/77 10/77 11/78 11/01/73 07/01/69* 07/01/67 11/01/75 11/01/75 06/01/68 07/01/67 07/01/70 07/01/67 DDT (revoked) decachlorooctahydro-1,3,4-metheno-2H-cyclobuta(cd)pentalen-2-one (revoked) demeton (revoked) desmedipham (180.353) di-allate, see S-2,3-dichloroallyl diisopropylthiocarbamate (revoked) dialifor (revoked) diazinon (180.153, 185.1750, 186.1750) dicamba (180.227) dichlobenil (180.231) dichlone (revoked) dichlorvos, see 2,2-dichlorovinyl dimethyl phosphate (180.235, 180.215, 185.1900) diclofop-methyl (180.385) dicloran, see 2,6-dichloro-4-nitroaniline (180.200) diclosulam (180.543) dicofol, see 1,1-bis(p-chlorophenyl)-2,2,2-trichloroethanol (180.163) dicrotophos, see dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide (180.299) dieldrin (revoked, ) diethatyl-ethyl (revoked) difenzoquat methyl sulfate (180.369) diflubenzuron (180.377, 186.2000) dimethenamid (180.464) dimethipin (180.406, 186.2050) dimethoate (180.204, 186.2100) dimethyl (2,2,2-trichloro-1-hydroxyethyl)phosphonate (180.198, 186.2325) dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide (180.299) dimethyl phosphate of alpha-methylbenzyl 3-hydroxy-cis-crotonate (revoked) dimethyl tetrachloroterephthalate (180.185) dinex, see 4,6-dinitro-o-cyclohexylphenol (revoked) dinitramine (revoked) dinocap, see 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate (180.341, 186.2400) dinoseb (revoked) dioxathion (revoked, 186.2450) diphenamid (180.230, ) diphenylamine (180.190) dipropetryn (revoked) dipropyl isocinchomeronate (180.143) diquat (180.226, 185.2500, 186.2500) disul-Na, see sesone (revoked) disulfoton, see O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate (180.183, 186.1950) diuron (180.106, 186.2550) dibromochloropropane, see 1,2-dibromo-3-chloropropane (revoked) (method for inorganic bromides) 07/01/67 January 2002 Index: Alphabetical–Page 6 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 10/77 07/01/69 11/01/75* 07/01/70 11/01/73 11/01/75 11/01/75 11/01/73 * 08/87 12/31/74* 10/77 07/01/67 05/84 11/01/73* 11/01/75 * 06/85 07/01/69 11/01/75 11/85 07/01/67 12/82 11/85 12/31/74 06/85 09/91 * 10/77* * * 09/91* 09/91* * 11/01/73 11/78 12/82* 07/01/67 06/85 06/85 10/77 DNOC, see 4,6-dinitro-o-cresol (180.344) dodecachlorooctahydro-1,3,4-metheno-2H-cyclobuta(cd)pentalene (revoked) dodine (180.172) endosulfan (180.182, 185.2600) endothall (180.293) endrin (revoked) EPN (revoked) EPTC, see S-ethyl dipropylthiocarbamate (180.117) esfenvalerate (180.533) ethalfluralin (180.416) ethephon (180.300, 185.2700, 186.2700) ethiolate (revoked) ethion (180.173, 185.2750, 186.2750) ethofumesate (180.345, ) ethoprop (180.262) ethoxyquin (180.178) ethyl (2E,4E)-3,7,11-trimethyl-2,4-dodecadienoate, (R)- and (S)- (180.501) ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl)phosphoramidate (180.349, 185.2950, 186.2950) ethyl 4,4'-dichlorobenzilate (revoked) ethylan, see 1,1-dichloro-2,2-bis(p-ethylphenyl)ethane (revoked) ethylene dibromide (revoked) ethylene oxide (180.151, 185.2850) etridiazole, see 5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole (180.370) famphur (revoked) fenac, see 2,3,6-trichlorophenylacetic acid (revoked) fenamiphos, see ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl)phosphoramidate (180.349, 185.2950, 186.2950) fenarimol (180.421) fenbuconazole (180.480) fenbutatin oxide, see hexakis(2-methyl-2-phenylpropyl)distannoxane (180.362, 185.3550, 186.3550) fenhexamid (180.553) fenitrothion, see O,O-dimethyl O-4-nitro-m-tolyl phosphorothioate (180.540, 185.2200) fenoxaprop ethyl ester, see fenoxaprop-ethyl (180.430) fenoxaprop-ethyl (180.430) fenpropathrin (180.466) fensulfothion, see O,O-diethyl O-(p-(methylsulfinyl)phenyl) phosphorothioate (revoked) fenthion (180.214) fenvalerate, see cyano(3-phenoxyphenyl)methyl 4-chloro-alpha-(1-methylethyl)benzeneacetate (180.379) ferbam (180.114) fluazifop butyl ester, see fluazifop-butyl (180.411, 185.3250, 186.3250) fluazifop-butyl (180.411, 185.3250, 186.3250) fluchloralin (revoked) January 2002 Index: Alphabetical–Page 7 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 05/84* * * * 07/01/70 11/01/75* 11/01/73 07/88 09/89* 09/89* 07/01/67 11/85 11/01/73* 06/86* * 07/01/69* 07/15/68 07/15/68 11/28/00 11/28/00 11/01/75 06/86, * * 12/82 * 07/01/67 12/31/74 * 10/77* 09/83 flucythrinate (revoked) fludioxonil (180.516) flumetsulam (180.468) flumiclorac pentyl ester (180.477, 186.3325) fluometuron (180.229, 186.3350) fluorine compounds (180.145, 185.3375) fluorodifen (revoked) fluridone (180.420) fluvalinate, see fluvalinate, (alpha RS,2R)- (180.427, 186.3400) fluvalinate, (alpha RS,2R)- (180.427, 186.3400) folpet (180.191) fonofos, see O-ethyl S-phenyl ethylphosphonodithioate (180.221) formetanate hydrochloride (180.276) fosetyl-Al, see aluminum tris(O-ethyl phosphonate) (180.415) furilazole, see 3-(dichloroacetyl)-5-(2-furanyl)-2,2-dimethyloxazolidine (180.471) Gardona, see 2-chloro-1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate (180.252, 186.950) gibberellic acid, see gibberellins (removed) gibberellins (removed) glufosinate ammonium salt (1:1), see glufosinate-ammonium (180.473) glufosinate-ammonium (180.473) glyodin (revoked) glyphosate (180.364) glyphosate-trimethylsulfonium, see sulfosate (180.489, removed) glyphosine (revoked) halosulfuron-methyl (180.479) heptachlor (revoked) hexachlorophene (revoked) hexaconazole (180.488) hexakis(2-methyl-2-phenylpropyl)distannoxane (180.362, 185.3550, 186.3550) hexazinone (180.396, 185.3575, 186.3575) hydramethylnon, see tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone (3-(4-(trifluoromethyl)phenyl)-1-(2-(4(trifluoromethyl)phenyl)ethenyl)-2-propenylidene hydrazone (180.395) 09/83* hydrogen cyanide, see hydrogen cyanide (180.130, 185.3600) hydroprene, see ethyl (2E,4E)-3,7,11-trimethyl-2,4-dodecadienoate, (R)- and (S)- (180.501) imazalil (180.413, revoked, 186.3650) imazamethabenz methyl ester, see methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-p-toluate and methyl (±)-6-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-m-toluate (180.437) imazaquin, see 2-(4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl)-3-quinoline= carboxylic acid (180.426) imazethapyr ammonium salt (180.447) imidacloprid (180.472) iprodione (180.399, revoked, removed) 07/01/67 * 06/85 * 07/88 09/91 * 05/84* January 2002 Index: Alphabetical–Page 8 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL isofenphos, see 1-methylethyl 2-((ethoxy((1-methylethyl)amino)phosphinothioyl)oxy)benzoate (revoked) isopropalin (revoked) Korax, see 1-chloro-2-nitropropane (revoked) kresoxim-methyl (180.554) lactofen (180.432, 180.453) lead arsenate (revoked) leptophos (revoked) lindane (180.133) linuron (180.184) magnesium arsenate (revoked) malathion (180.111, 185.3850, 185.7000, 186.3850) maleic hydrazide (180.175, 185.3900) mancozeb, see coordination product of zinc ion and maneb (180.176, 185.6300, 186.6300) maneb (180.110) manganese dimethyldithiocarbamate, see manganous dimethyldithiocarbamate (revoked) manganous dimethyldithiocarbamate (revoked) MCPA, see 2-methyl-4-chlorophenoxyacetic acid (180.339) MCPB, see 4-(2-methyl-4-chlorophenoxy) butyric acid (180.318) mefluidide (revoked) mepiquat chloride, see N,N-dimethylpiperidinium chloride (180.384) mercaptobenzothiazole (revoked) merphos, see tributyl phosphorotrithioite (revoked) metalaxyl (180.408, 185.4000) methamidophos (180.315, 180.108) methanearsonic acid (180.289) methazole (revoked) methidathion (180.298) methiocarb, see 3,5-dimethyl-4-(methylthio)phenyl methylcarbamate (revoked) methomyl (180.253, 185.4100) methoprene (180.359, 185.4150, 186.4150) methoxychlor (180.120) methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-p-toluate and methyl (±)-6-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-m-toluate (180.437) methyl 3-((dimethoxyphosphinyl)oxy)-2-butenoate (180.157) methyl bromide (180.521, 180.522) metiram, see ammoniates of (ethylenebis(dithiocarbamato)) zinc and ethylenebis(dithiocarbamic acid) (180.217) metobromuron (revoked) metolachlor (180.368) metribuzin, see 4-amino-6-(1,1-dimethylethyl)-3-(methylthio)-1,2,4-triazin-5-(4H)-one (180.332, 185.250, 186.250) metsulfuron methyl (180.428) 05/84 12/31/74 11/01/73 * 09/91 11/01/75 07/78 11/01/75 07/01/67* 11/01/75 11/01/75* 11/01/75 07/01/67 07/01/67 07/01/67 07/01/67 11/01/75 12/31/74 09/83 09/83* 07/01/67 11/01/75 11/84* 12/31/74 11/01/75 12/82 11/78* 10/77 07/01/70 11/78 11/01/75 * 11/01/75 * 11/01/75 07/01/69 12/82 11/1/75* 09/89 January 2002 Index: Alphabetical–Page 9 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 09/89 11/01/75 10/77 07/01/69 07/15/68 12/31/74 11/01/75 * 10/77 09/83* 07/78 08/87 10/77 06/85 12/31/74 12/31/74 07/01/69 10/77 07/01/67 01/02/69 * 11/01/75 07/15/68 11/85 11/78 07/01/69 10/77* 11/01/73 07/01/69 07/01/70 * 11/01/75 * 07/88 11/85 10/77 11/01/75 10/77 07/01/69 10/77 * 10/77 metsulfuron methyl ester, see metsulfuron methyl (180.428) mevinphos, see methyl 3-((dimethoxyphosphinyl)oxy)-2-butenoate (180.157) MGK 264, see N-octyl bicycloheptene dicarboximide (180.367, 185.4500) mirex, see dodecachlorooctahydro-1,3,4-metheno-2H-cyclobuta(cd)pentalene (revoked) molinate, see S-ethyl hexahydro-1H-azepine-1-carbothioate (180.228) monocrotophos, see dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide (180.296, 185.2250) monuron (revoked) myclobutanil (180.443, 185.4350, 186.4350) N,N-diethyl-2-(1-naphthalenyloxy)propionamide (180.328) N,N-dimethylpiperidinium chloride (180.384) N-(mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorodithioate) (180.261) N-butyl-N-ethyl-alpha, alpha, alpha-trifluoro-2,6-dinitro-p-toluidine (180.208) N-octyl bicycloheptene dicarboximide (180.367, 185.4500) naled (180.215) naphthaleneacetamide, see naphthaleneacetamide, alpha- (180.309) naphthaleneacetamide, alpha- (180.309) naphthoxyacetic acid, beta- (revoked) napropamide, see N,N-diethyl-2-(1-naphthalenyloxy)propionamide (180.328) naptalam, see N-1-naphthylphthalamic acid (180.297) neodecanoic acid (revoked) nicosulfuron (180.454) nicotine (180.167) nitralin, see 4-(methylsulfonyl)-2,6-dinitro-N,N-dipropylaniline (revoked) nitrapyrin (180.350) nitrofen, see 2,4-dichloro p-nitrophenyl ether (revoked) norea (revoked) norflurazon (180.356) O,O-diethyl O-(p-(methylsulfinyl)phenyl) phosphorothioate (revoked) O,O-diethyl O-pyrazinyl phosphorothioate (revoked) O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate (180.183, 186.1950) O,O-dimethyl O-4-nitro-m-tolyl phosphorothioate (180.540, 185.2200) O,O-dimethyl S-((4-oxo-1,2,3-benzotriazin-3(4H)-yl)methyl) phosphorodithioate (180.154) O-(2-(1,1-dimethylethyl)-5-pyrimidinyl) O-ethyl O-(1-methylethyl) phosphorothioate (180.483) O-ethyl O-(4-(methylthio)phenyl) S-propyl phosphorodithioate (revoked) O-ethyl S-phenyl ethylphosphonodithioate (180.221) octhilinone (revoked) orthoarsenic acid (revoked) oryzalin (180.304, 185.4550) ovex (revoked) oxadiazon (180.346) oxadixyl (180.456) oxamyl (180.303, 186.4575) January 2002 Index: Alphabetical–Page 10 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL oxydemeton-methyl, see S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate (180.330, 186.3050) 11/01/75* oxyfluorfen (180.381) oxytetracycline (180.337) oxytetracycline hydrochloride (180.337) oxythioquinox, see 6-methyl-1,3-dithiolo[4,5-b]quinoxalin-2-one (180.338) paraquat (180.205) parathion (180.121) parathion methyl homolog (180.121) parathion-methyl, see parathion methyl homolog (180.121) pebulate, see S-propyl butylethylthiocarbamate (180.238) pendimethalin (180.361) perfluidone (revoked) permethrin (180.378) phenmedipham (180.278) phenylphenol, o- (180.129) phorate (180.206, 186.4750) phosalone (180.263, 185.4800, 186.4800) phosmet, see N-(mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorodithioate) (180.261) phosphamidon (180.239) picloram (180.292) piperonyl butoxide (180.127, 185.4900, 186.4900) pirimicarb (revoked) pirimiphos-ethyl (revoked) pirimiphos-methyl (180.409, 185.4950, 186.4950) potassium arsenite (revoked) primisulfuron-methyl (180.452) procymidone (180.455) (ref to PAM I) profenofos (180.404, 186.4975) profluralin (revoked) prometryn (180.222) pronamide, see 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide (180.317) propachlor, see 2-chloro-N-isopropylacetanilide (180.211) propanil (180.274) propargite (180.259, 185.5000, 186.5000) propargyl bromide (180.199) (method for inorganic bromides) propazine (180.243) propetamphos (180.541, 185.5100, 186.5100) propiconazole, see 1-((2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl)methyl)-1H-1,2,4-triazole (180.434) pyrazon (180.316) pyrethrins (180.128, 185.5200, 186.5200) pyridate (180.462) 11/84 07/01/67 07/01/67 10/77 11/01/75 11/01/75 11/01/75 11/01/75 11/01/75 10/77 10/77 11/84 12/31/74 11/01/75 11/01/73 07/01/70* 07/78 07/15/68 07/78 11/01/75 09/83 12/31/74 06/85* 11/01/75 * * 06/85* 10/77 07/15/68 12/31/74 07/01/70 11/01/73 11/78 07/01/67 11/85 06/86 * 12/31/74 11/01/75 * January 2002 Index: Alphabetical–Page 11 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL * 11/01/73 * * 08/87 * 11/85 07/01/70* 11/01/75* 11/01/73 12/31/74 07/15/68 07/15/68 11/01/73 07/15/68 11/01/75 11/01/75 07/01/67 12/31/74 12/31/74 07/01/67 11/84* 11/01/75 11/85 11/01/75 11/01/75 11/01/75 11/01/75 09/83* * * 01/02/69 07/01/67 01/02/69 * 11/01/75 07/88 12/31/74 12/31/74 07/78 11/01/75 quinclorac, see 3,7-dichloro-8-quinolinecarboxylic acid (180.463) quintozene, see pentachloronitrobenzene (180.291) quizalofop ethyl (180.441) quizalofop ethyl ester, see quizalofop ethyl (180.441) resmethrin (180.525) rimsulfuron (180.478) ronnel (revoked) S,S,S-tributyl phosphorotrithioate (180.272, 186.5800) S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate (180.330, 186.3050) S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide (180.241) S-2,3-dichloroallyl diisopropylthiocarbamate (revoked) S-ethyl cyclohexylethylthiocarbamate (180.212) S-ethyl diisobutylthiocarbamate (180.232) S-ethyl dipropylthiocarbamate (180.117) S-ethyl hexahydro-1H-azepine-1-carbothioate (180.228) S-propyl butylethylthiocarbamate (180.238) S-propyl dipropylthiocarbamate (180.240) schradan (revoked) sec-butylamine (revoked, 186.450) secbumeton (revoked) sesone (revoked) sethoxydim, see 2-(1-(ethoxyimino)butyl)-5-(2-(ethylthio)propyl)-3-hydroxy-2-cyclohexen-1-one (180.412) silvex (revoked) simazine (180.213, 186.5350) sodium arsenate (revoked) sodium arsenite (revoked) sodium dehydroacetate (revoked) sodium dimethyldithiocarbamate (180.152) sodium salt of acifluorfen (180.383) sodium salt of fomesafen (180.433) spinosad (180.495) streptomycin (180.245) Strobane, see terpene polychlorinates (revoked) sulfallate, see 2-chloroallyl diethyldithiocarbamate (revoked) sulfosate (180.489, removed) Sulphenone, see chlorophenyl phenyl sulfone, p- (revoked) sulprofos, see O-ethyl O-(4-(methylthio)phenyl) S-propyl phosphorodithioate (revoked) S–2,3,3-trichloroallyl diisopropylthiocarbamate (180.314) TCA (revoked) TCMTB, see 2-(thiocyanomethylthio)benzothiazole (180.288) TDE (revoked) January 2002 Index: Alphabetical–Page 12 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL * * tebuconazole (180.474) tebufenozide, see benzoic acid, 3,5-dimethyl-1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide (180.482) tebupirimfos, see O-(2-(1,1-dimethylethyl)-5-pyrimidinyl) O-ethyl O-(1-methylethyl) phosphorothioate (180.483) * tebuthiuron (180.390) tecnazene, see 1,2,4,5-tetrachloro-3-nitrobenzene (revoked) tefluthrin (180.440) temephos (revoked) TEPP, see tetraethyl pyrophosphate (revoked) terbacil (180.209) terbufos (180.352) terbuthylazine (revoked) terbutryn (revoked) terpene polychlorinates (revoked) tetradifon (180.174) tetraethyl pyrophosphate (revoked) tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone (3-(4-(trifluoromethyl)phenyl)-1-(2-(4(trifluoromethyl)phenyl)ethenyl)-2-propenylidene hydrazone (180.395) tetraiodoethylene (revoked) tetrasul, see chlorophenyl-2,4,5-trichlorophenyl sulfide, p- (revoked) thiabendazole (180.242, 185.5550, 186.5550) thidiazuron (180.403, 186.5600) thifensulfuron methyl ester (180.439) thiobencarb (180.401) thiodicarb (180.407, 186.5650) thionazin, see O,O-diethyl O-pyrazinyl phosphorothioate (revoked) thiophanate-methyl (180.371, 186.5700) thiram (180.132) toxaphene (revoked) tralomethrin (180.422) tri-allate, see S–2,3,3-trichloroallyl diisopropylthiocarbamate (180.314) triadimefon, see 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone (180.410, revoked) triasulfuron (180.459) tribenuron methyl ester (180.451) tributyl phosphorotrithioite (revoked) trichlorfon, see dimethyl (2,2,2-trichloro-1-hydroxyethyl)phosphonate (180.198, 186.2325) trichlorobenzyl chloride (revoked) triclopyr (180.417, 185.1000, 186.1000) tridemorph, see 2,6-dimethyl-4-tridecylmorpholine (180.372) tridiphane, see 2-(3,5-dichlorophenyl)-2-(2,2,2-trichloroethyl)-oxirane (180.424) trifloxystrobin (180.555) 09/83 11/01/75 * * 10/77 08/87 10/77* 11/01/75 07/01/70 07/01/67 07/01/67 10/77 09/83* 07/01/67 07/01/69 07/88 11/84 * 05/84 06/86 07/01/69 11/78* 11/01/75 07/01/67 08/87 12/31/74 06/85* * * 11/01/75 07/01/70 07/01/70 06/86 12/82 09/89* * January 2002 Index: Alphabetical–Page 13 Pesticide Analytical Manual Vol. II INDEX: ALPHABETICAL 08/87 09/83 12/31/74 11/01/73 11/01/75 11/01/75 12/82 11/01/75 11/01/75 trifluralin (180.207) triforine (180.382, 185.5950, 186.5950) trimethacarb, see 3,4,5-trimethylphenyl methylcarbamate and 2,3,5-trimethylphenyl methylcarbamate (180.305) triphenyltin hydroxide (180.236) trisodium arsenate, see sodium arsenate (revoked) vernolate, see S-propyl dipropylthiocarbamate (180.240) vinclozolin, see 3-(3,5-dichlorophenyl)-5-ethenyl-5-methyl-2,4-oxazolidinedione (180.380) zineb (revoked) ziram (180.116) January 2002 Index: Alphabetical–Page 14 Pesticide Analytical Manual Vol. II Pesticide Analytical Manual Volume II Numerical Index This index to Pesticide Analytical Manual Volume II (PAM II), methods for residues of individual pesticides, is in order by the section of Code of Federal Regulations Title 40 (40 CFR) in which tolerances for that pesticide are listed. Parts 180 (tolerances for pesticide chemicals in or on raw agricultural commodities), 185 (food additives in food for human consumption) and 186 (feed additives permitted in animal feed) are included. Each entry in this index also includes references to other 40 CFR parts for the chemical. Dates in this index are the transmittal dates of the PAM II published methods. Asterisks indicate that additional or new method(s) have been submitted to EPA but not compiled in PAM II. Users with a need for such methods may request copies from: (Mail) Mark Law US EPA/OPP/BEAD/ACB Environmental Science Center 701 Mapes Road Fort Meade, MD 20755-5350 (410) 305-2915 (TTY)* (410) 305-3091 ResidueMethods@epa.gov (Telephone) (Fax) (Email) *Requestors who do not use TTY should first dial 711 to be connected with their state’s Relay Service, or dial the Relay Service directly. The telephone number is in the user’s local directory. The call will be answered by a live operator, to whom the requestor must give the EPA phone number above. The operator will complete the connection and assist in the conversation. January 2002 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL Title 40, Part 180: Tolerances and exemptions from tolerances for pesticide chemicals in or on raw agricultural commodities Sec. No. 180.103 180.106 180.108 180.110 180.111 180.113 180.114 180.116 180.117 180.120 180.121 180.121 180.127 180.128 180.129 180.130 180.132 180.133 180.136 180.142 180.143 180.144 180.145 180.151 180.152 180.153 180.154 180.155 180.157 180.163 180.167 180.169 180.172 180.173 180.174 180.175 180.176 180.178 Name captan diuron (186.2550) acephate (revoked, 186.100) maneb malathion (185.3850, 185.7000, 186.3850) allethrin ferbam ziram S-ethyl dipropylthiocarbamate methoxychlor parathion parathion methyl homolog piperonyl butoxide (185.4900, 186.4900) pyrethrins (185.5200, 186.5200) phenylphenol, ohydrogen cyanide (185.3600) thiram lindane basic copper carbonate 2,4-D dipropyl isocinchomeronate cyhexatin (185.1350, 186.1350) fluorine compounds (185.3375) ethylene oxide (185.2850) sodium dimethyldithiocarbamate diazinon (185.1750, 186.1750) O,O-dimethyl S-((4-oxo-1,2,3-benzotriazin-3(4H)-yl)methyl) phosphorodithioate 1-naphthaleneacetic acid methyl 3-((dimethoxyphosphinyl)oxy)-2-butenoate 1,1-bis(p-chlorophenyl)-2,2,2-trichloroethanol nicotine carbaryl (186.550) dodine ethion (185.2750, 186.2750) tetradifon maleic hydrazide (185.3900) coordination product of zinc ion and maneb (185.6300, 186.6300) ethoxyquin Date 11/01/75* 07/01/67 10/77 07/01/67 11/01/75* 07/01/67 07/01/67 11/01/75 11/01/73 11/01/75 11/01/75 11/01/75 11/01/75 11/01/75 11/01/75 07/01/67 11/01/75 11/01/75 11/01/75 07/01/67* 11/01/75 06/86 11/01/75* 07/01/67 11/01/75 11/01/75 11/01/75 11/01/75 11/01/75 07/01/67 11/01/75 11/01/75 11/01/75* 07/01/67 07/01/67 11/01/75 07/01/67 11/01/75 * Method(s)have been submitted to EPA but not compiled in PAM II; request copies from EPA. January 2002 Index: Numerical–Page 2 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL 11/01/75 07/01/70 07/01/70 07/01/67* 07/01/70 07/01/69 07/01/67 07/01/67 07/01/70 70/01/67 07/01/67 07/01/67 12/31/74 11/1/73 11/1/75 11/1/73 08/87 08/87 08/87 08/87 07/01/70 07/15/68 11/85 11/78 06/85 11/85 11/85 07/15/68 06/01/68 07/01/70* 07/15/68 07/01/70 07/01/69* 06/01/68 07/15/68 06/85 11/01/73 11/01/75 07/15/68 11/01/75 180.181 180.182 180.183 180.184 180.185 180.189 180.190 180.191 180.198 180.199 180.199 180.200 180.202 180.204 180.205 180.206 180.207 180.208 180.209 180.210 180.211 180.212 180.213 180.214 180.215 180.217 180.220 180.221 180.222 180.226 180.227 180.228 180.229 180.230 180.231 180.232 CIPC endosulfan (185.2600) O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate (186.1950) linuron dimethyl tetrachloroterephthalate coumaphos diphenylamine folpet dimethyl (2,2,2-trichloro-1-hydroxyethyl)phosphonate (186.2325) chloropicrin (method for inorganic bromides) propargyl bromide (method for inorganic bromides) 2,6-dichloro-4-nitroaniline chlorophenoxyacetic acid, pdimethoate (186.2100) paraquat phorate (186.4750) trifluralin N-butyl-N-ethyl-alpha, alpha, alpha-trifluoro-2,6-dinitro-p-toluidine terbacil bromacil 2-chloro-N-isopropylacetanilide S-ethyl cyclohexylethylthiocarbamate simazine (186.5350) fenthion naled atrazine O-ethyl S-phenyl ethylphosphonodithioate prometryn diquat (185.2500, 186.2500) dicamba S-ethyl hexahydro-1H-azepine-1-carbothioate fluometuron (186.3350) diphenamid dichlobenil S-ethyl diisobutylthiocarbamate ammoniates of (ethylenebis(dithiocarbamato)) zinc and ethylenebis(dithiocarbamic acid) 11/01/75 180.235, 180.215 2,2-dichlorovinyl dimethyl phosphate (185.1900) 180.236 180.238 180.239 180.240 triphenyltin hydroxide S-propyl butylethylthiocarbamate phosphamidon S-propyl dipropylthiocarbamate January 2002 Index: Numerical–Page 3 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL 11/01/73 07/88 11/85 01/02/69 07/01/69* 07/01/69* 07/01/70 08/87 07/01/69 11/85 11/78 007/78 11/01/73* 07/01/70* 07/78 07/01/70 11/84 07/01/70* 11/01/73 07/01/70 11/01/73* 12/31/74 08/87* 07/78 11/01/75 11/01/73 07/78 11/01/73 11/78* 12/31/74 07/01/67 11/78* 12/31/74 12/31/74* 10/77 10/77 10/77 12/31/74 12/31/74 12/31/74 12/31/74 12/31/74 180.241 180.242 180.243 180.245 180.249 180.252 180.253 180.254 180.257 180.258 180.259 180.261 180.262 180.263 180.267 180.268 180.269 180.272 180.274 180.275 180.276 180.278 180.287 180.288 180.289 180.291 180.292 180.293 180.294 180.296 180.297 180.298 180.299 180.300 180.301 180.303 180.304 180.305 180.307 180.309 180.311 180.312 S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide thiabendazole (185.5550, 186.5550) propazine streptomycin alachlor 2-chloro-1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate (186.950) methomyl (185.4100) carbofuran (185.600, 186.600) chloroneb ametryn propargite (185.5000, 186.5000) N-(mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorodithioate) ethoprop phosalone (185.4800, 186.4800) captafol barban aldicarb (185.150, 186.150) S,S,S-tributyl phosphorotrithioate (186.5800) propanil chlorothalonil formetanate hydrochloride phenmedipham amitraz (memo) 2-(thiocyanomethylthio)benzothiazole methanearsonic acid pentachloronitrobenzene picloram endothall benomyl (185.350, 186.350) dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide (185.2250) N-1-naphthylphthalamic acid methidathion dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide ethephon (185.2700, 186.2700) carboxin oxamyl (186.4575) oryzalin (185.4550) 3,4,5-trimethylphenyl methylcarbamate and 2,3,5-trimethylphenyl methylcarbamate 2-((4-chloro-6-(ethylamino)-s-triazin-2-yl)amino)-2-methylpropionitrile naphthaleneacetamide, alphacacodylic acid 4-aminopyridine January 2002 Index: Numerical–Page 4 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL 12/31/74 12/31/74 12/31/74 12/31/74 12/31/74 08/87 12/31/74 10/77 11/01/75* 11/01/75 11/01/75* 07/01/67 07/01/67 10/77 11/01/75 10/77 10/77 10/77 05/84 10/77 11/85 10/77* 10/77 11/78 10/77* 11/78 09/83 10/77 10/77* 06/86* 10/77 12/82 10/77 12/82 11/78* 12/82 12/82 11/84 12/82* 12/82 180.314 S–2,3,3-trichloroallyl diisopropylthiocarbamate 180.315, 180.108 methamidophos 180.316 180.317 180.318 180.324 180.325 180.328 180.330 180.331 180.332 180.337 180.337 180.338 180.339 180.341 180.342 180.344 180.345 180.346 180.349 180.350 180.352 180.353 180.355 180.356 180.359 180.360 180.361 180.362 180.364 180.367 180.368 180.369 180.370 180.371 180.372 180.377 180.378 180.379 180.380 pyrazon 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide 4-(2-methyl-4-chlorophenoxy) butyric acid bromoxynil 2-(m-chlorophenoxy)propionic acid N,N-diethyl-2-(1-naphthalenyloxy)propionamide S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate (186.3050) 4-(2,4-dichlorophenoxy)butyric acid 4-amino-6-(1,1-dimethylethyl)-3-(methylthio)-1,2,4-triazin-5-(4H)-one (185.250, 186.250) oxytetracycline oxytetracycline hydrochloride 6-methyl-1,3-dithiolo[4,5-b]quinoxalin-2-one 2-methyl-4-chlorophenoxyacetic acid 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate (186.2400) chlorpyrifos (185.1000, 186.1000) 4,6-dinitro-o-cresol ethofumesate oxadiazon nitrapyrin terbufos desmedipham bentazon (186.375) norflurazon methoprene (185.4150, 186.4150) asulam pendimethalin hexakis(2-methyl-2-phenylpropyl)distannoxane (185.3550, 186.3550) glyphosate N-octyl bicycloheptene dicarboximide (185.4500) metolachlor difenzoquat methyl sulfate 5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole thiophanate-methyl (186.5700) 2,6-dimethyl-4-tridecylmorpholine diflubenzuron (186.2000) permethrin cyano(3-phenoxyphenyl)methyl 4-chloro-alpha-(1-methylethyl)benzeneacetate 3-(3,5-dichlorophenyl)-5-ethenyl-5-methyl-2,4-oxazolidinedione ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl)phosphoramidate (185.2950, 186.2950) 06/85 January 2002 Index: Numerical–Page 5 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL 11/84 09/83 09/83* 09/83* 05/84 09/83 09/83* 09/83 05/84* 05/84 11/84 06/85* 11/84 06/85 06/86 11/84* 06/85* 06/85* 06/85 11/84* 06/85 06/86* 06/86* 08/87 06/86 11/85 07/88 07/88 09/91 08/87 09/89* 09/91 09/89* 09/89 09/89 09/91* 09/91 09/91 * * 180.381 180.382 180.383 180.384 180.385 180.390 180.395 180.396 180.399 180.401 180.403 180.404 180.405 180.406 180.407 180.408 180.409 180.410 180.411 180.412 180.413 180.414 180.415 180.416 180.417 180.418 180.419 180.420 180.421 180.422 180.424 180.425 180.426 180.427 180.428 180.429 180.430 180.431 oxyfluorfen triforine (185.5950, 186.5950) sodium salt of acifluorfen N,N-dimethylpiperidinium chloride diclofop-methyl tebuthiuron tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone (3-(4-(trifluoromethyl)phenyl)-1-(2-(4(trifluoromethyl)phenyl)ethenyl)-2-propenylidene hydrazone hexazinone (185.3575, 186.3575) iprodione (revoked, removed) thiobencarb thidiazuron (186.5600) profenofos (186.4975) chlorsulfuron dimethipin (186.2050) thiodicarb (186.5650) metalaxyl (185.4000) pirimiphos-methyl (185.4950, 186.4950) 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone (revoked) fluazifop-butyl (185.3250, 186.3250) 2-(1-(ethoxyimino)butyl)-5-(2-(ethylthio)propyl)-3-hydroxy-2-cyclohexen-1-one imazalil (revoked, 186.3650) cyromazine aluminum tris(O-ethyl phosphonate) ethalfluralin triclopyr (185.1000, 186.1000) cypermethrin, zetachlorpyrifos-methyl (185.1050, 186.1050) fluridone fenarimol tralomethrin 2-(3,5-dichlorophenyl)-2-(2,2,2-trichloroethyl)-oxirane 2-((2-chlorophenyl)methyl)-4,4-dimethyl-3-isoxazolidinone fluvalinate, (alpha RS,2R)- (186.3400) metsulfuron methyl chlorimuron ethyl ester fenoxaprop-ethyl clopyralid 2-(4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl)-3-quinolinecarboxylic acid 07/88 180.432, 180.453 lactofen 180.433 180.434 sodium salt of fomesafen 1-((2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl)methyl)-1H-1,2,4-triazole January 2002 Index: Numerical–Page 6 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL * * * * * * * * * * 09/91 * * * * * * * * * * * * * * * * * * * * * 11/28/00 * * * * * * * * 180.436 180.437 180.438 180.439 180.440 180.441 180.442 180.443 180.445 180.446 180.447 180.449 180.451 180.452 180.454 180.455 180.456 180.457 180.458 180.459 180.460 180.461 180.462 180.463 180.464 180.465 180.466 180.467 180.468 180.470 180.471 180.472 180.473 180.474 180.477 180.478 180.479 180.480 180.482 180.483 180.488 cyfluthrin methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-p-toluate and methyl (±)-6-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-m-toluate cyhalothrin, lambda- (185.1310) thifensulfuron methyl ester tefluthrin quizalofop ethyl bifenthrin myclobutanil (185.4350, 186.4350) bensulfuron methyl ester clofentezine (185.---) (several methods) imazethapyr ammonium salt Avermectin B1 (several methods) tribenuron methyl ester primisulfuron-methyl nicosulfuron procymidone (ref to PAM I) oxadixyl (1,1'-biphenyl)-4-yloxy-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, beta(185.---, 186.---) clethodim (186.1075) triasulfuron 4-(dichloroacetyl)-3,4-dihydro-3-methyl-2H-1,4-benzoxazine cadusafos pyridate 3,7-dichloro-8-quinolinecarboxylic acid dimethenamid 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane fenpropathrin carbon disulfide flumetsulam acetochlor 3-(dichloroacetyl)-5-(2-furanyl)-2,2-dimethyloxazolidine imidacloprid glufosinate-ammonium tebuconazole flumiclorac pentyl ester (186.3325) rimsulfuron halosulfuron-methyl fenbuconazole benzoic acid, 3,5-dimethyl-1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide O-(2-(1,1-dimethylethyl)-5-pyrimidinyl) O-ethyl O-(1-methylethyl) phosphorothioate hexaconazole January 2002 Index: Numerical–Page 7 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL * * * * * * * 08/87 * * * 06/86 * * * * 180.489 180.495 180.501 180.502 180.515 180.516 sulfosate (removed) spinosad ethyl (2E,4E)-3,7,11-trimethyl-2,4-dodecadienoate, (R)- and (S)aminoethoxyvinylglycine carfentrazone-ethyl fludioxonil 180.521, 180.522 methyl bromide 180.525 180.530 180.533 180.540 180.541 180.543 180.553 180.554 180.555 resmethrin 2,2-dimethyl-1,3-benzodioxol-4-ol methylcarbamate esfenvalerate O,O-dimethyl O-4-nitro-m-tolyl phosphorothioate (185.2200) propetamphos (185.5100, 186.5100) diclosulam fenhexamid kresoxim-methyl trifloxystrobin January 2002 Index: Numerical–Page 8 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL Title 40, Part 185: Food additives permitted in food for human consumption Sec. No. 185.--185.--185.1000 185.1000 185.1050 185.1200 185.1310 185.1350 185.150 185.1750 185.1900 185.2200 185.2250 185.250 185.2500 185.2600 185.2700 185.2750 185.2850 185.2950 185.3250 185.3375 185.350 185.3550 185.3575 185.3600 Name (1,1'-biphenyl)-4-yloxy-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, betaclofentezine (several methods) chlorpyrifos triclopyr chlorpyrifos-methyl copper cyhalothrin, lambdacyhexatin aldicarb diazinon 2,2-dichlorovinyl dimethyl phosphate O,O-dimethyl O-4-nitro-m-tolyl phosphorothioate dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide 4-amino-6-(1,1-dimethylethyl)-3-(methylthio)-1,2,4-triazin-5-(4H)-one diquat endosulfan ethephon ethion ethylene oxide ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl)phosphoramidate fluazifop-butyl fluorine compounds benomyl hexakis(2-methyl-2-phenylpropyl)distannoxane hexazinone hydrogen cyanide Date * * 10/77 06/86 07/88 11/01/75 * 06/86 11/84 11/01/75 06/85 * 12/31/74 11/01/75* 06/01/68 07/01/70 12/31/74* 07/01/67 07/01/67 06/85 06/85 11/01/75* 11/78* 10/77* 09/83 07/01/67 11/01/75* 11/01/75 11/84* 07/01/70 11/78 * 10/77 10/77 07/01/70* 11/01/75 06/85* 11/78 06/86 185.3850, 185.7000 malathion 185.3900 185.4000 185.4100 185.4150 185.4350 185.4500 185.4550 185.4800 185.4900 185.4950 185.5000 185.5100 maleic hydrazide metalaxyl methomyl methoprene myclobutanil N-octyl bicycloheptene dicarboximide oryzalin phosalone piperonyl butoxide pirimiphos-methyl propargite propetamphos January 2002 Index: Numerical–Page 9 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL 11/01/75 07/88 09/83 08/87 07/01/67 185.5200 185.5550 185.5950 185.600 185.6300 pyrethrins thiabendazole triforine carbofuran coordination product of zinc ion and maneb January 2002 Index: Numerical–Page 10 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL Title 40, Part 186: Feed additives permitted in animal feed Sec. No. 186.--186.100 186.1000 186.1000 186.1050 186.1075 186.1350 186.150 186.1750 186.1950 186.2000 186.2050 186.2100 186.2325 186.2400 186.2450 186.250 186.2500 186.2550 186.2700 186.2750 186.2950 186.3050 186.3250 186.3325 186.3350 186.3400 186.350 186.3550 186.3575 186.3650 186.375 186.3850 186.4150 186.4350 186.450 186.4575 186.4750 186.4800 186.4900 Name (1,1'-biphenyl)-4-yloxy-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, betaacephate chlorpyrifos triclopyr chlorpyrifos-methyl clethodim cyhexatin aldicarb diazinon O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate diflubenzuron dimethipin dimethoate dimethyl (2,2,2-trichloro-1-hydroxyethyl)phosphonate 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate dioxathion 4-amino-6-(1,1-dimethylethyl)-3-(methylthio)-1,2,4-triazin-5-(4H)-one diquat diuron ethephon ethion ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl)phosphoramidate S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate fluazifop-butyl flumiclorac pentyl ester fluometuron fluvalinate, (alpha RS,2R)benomyl hexakis(2-methyl-2-phenylpropyl)distannoxane hexazinone imazalil bentazon malathion methoprene myclobutanil sec-butylamine oxamyl phorate phosalone piperonyl butoxide Date * 10/77 10/77 06/86 07/88 * 06/86 11/84 11/01/75 07/01/70 12/82 06/85 11/01/73 07/01/70 10/77 11/01/73 11/01/75* 06/01/68 07/01/67 12/31/74* 07/01/67 06/85 11/01/75* 06/85 * 07/01/70 09/89* 11/78* 10/77* 09/83 06/85 11/78 11/01/75* 11/78 * 12/31/74 10/77 11/01/73 07/01/70* 11/01/75 January 2002 Index: Numerical–Page 11 Pesticide Analytical Manual Vol. II INDEX: NUMERICAL 06/85* 06/85* 11/78 06/86 11/01/75 11/85 11/01/75 07/88 11/84 06/86 11/78* 07/01/70* 09/83 08/87 07/1/67 07/1/69* 186.4950 186.4975 186.5000 186.5100 186.5200 186.5350 186.550 186.5550 186.5600 186.5650 186.5700 186.5800 186.5950 186.600 186.6300 186.950 pirimiphos-methyl profenofos propargite propetamphos pyrethrins simazine carbaryl thiabendazole thidiazuron thiodicarb thiophanate-methyl S,S,S-tributyl phosphorotrithioate triforine carbofuran coordination product of zinc ion and maneb 2-chloro-1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate January 2002 Index: Numerical–Page 12