ROCKY MOUNTAIN CONFERENCE ON ANALYTICAL CHEMISTRY ANALYTICAL METHODS MONDAY JULY

50th ROCKY MOUNTAIN CONFERENCE ON ANALYTICAL CHEMISTRY ANALYTICAL METHODS MONDAY, JULY 28, 2008 Session I-A, Advances and Applications, Keith Miller presiding TIME 9:00 TITLE / AUTHORS Complex Fluid Analysis with the Advanced Distillation Curve Approach. Thomas J. Bruno, National Institute of Standards and Technology Analysis of Bio-Gasoline Mixtures with the Advanced Distillation Curve Method. Arron Wolk, Alexander Naydich and Thomas J. Bruno, National Institute of Standards and Technology Analytical Determination of the Vapor Pressures of Organic Aerosol Formers by the Gas Saturation Technique. Jason A. Widegren and Thomas J. Bruno, National Institute of Standards and Technology BREAK Simple, Quantitative Headspace Analysis by Cryoadsorption on a Short Alumina PLOT Column. Tara M. Lovestead and Thomas J. Bruno, National Institute of Standards and Technology Subcritical Water Chromatography: Green Liquid Chromatography with a Thermal Separation Mechanism. Daniel E. Connors and Keith E. Miller, University of Denver LUNCH (complimentary buffet included with registration fee) Analysis of Melamine and Cyanuric Acid Residues in Catfish, Trout, Tilapia, Salmon and Shrimp by Liquid Chromatography with Tandem Mass Spectrometry. Christine M. Karbiwnyk, Wendy C. Andersen and Sherri B. Turnipseed, U.S. Food and Drug Administration Spatial Variability of Atomic and Molecular Emission Signatures in SparkInduced Breakdown Spectroscopy. Morgan Steele and Amy Bauer, University of Denver BREAK Zeolite Cation Channel Structures by X-Ray Diffraction. William J. Miles, Miles Industrial Mineral Research Integrating Pharmaceutical and Food Safety Analyses into the Analytical Chemistry Curriculum. Keith E. Miller, University of Denver CONFERENCE RECEPTION 9:30 10:00 10:30 11:00 11:30 12:00 1:30 2:00 2:30 3:00 3:30 5:00 – 7:00 Session I-B, Microfluidics, Chuck Henry presiding 8:30 Microfluidics Meet Surfaces: Analysis Of Biologically Relevant Compounds Using Microchips, Capillary Electrophoresis, and Biosensors. Maria F. Mora, Jessica Felhofer, Gabrielle Guy, Jennifer Wehmeyer, Rena Bizios, Arturo Ayon and Carlos D. Garcia, The University of Texas at San Antonio Immobilization of Magnetic Beads in the Presence of Electroosmotic Flow. S. Douglass Gilman, Rattikan Chantiwas and Xiaoyan Yan, Louisiana State University Carbon Based Electrodes for Microfluidic Electrochemical Biosensors. Carlos F. Gonzalez and Donald M. Cropek, U.S. Army Corps of Engineers; J. Mason, Janet S. Locklear and Charles S. Henry, Colorado State University BREAK Nanofluidics and Mass-Limited Chemical Analysis: Au-Coated Nanocapillary Array Membranes as Switchable Fluidic Elements for Multiplexed Chemical Characterization. Paul W. Bohn, University of Notre Dame Transport Issues in Microarray and µTAS Devices. David S. Dandy, N. Scott Lynn and Charles S. Henry, Colorado State University Selective Detection using Electrode Arrays and Microchip Capillary Electrophoresis. James R. Kraly, Ryan E. Holcomb, Qian Guan and Charles S. Henry, Colorado State University LUNCH (complimentary buffet included with registration fee) Environmental Monitoring Using Microchip Electrophoresis. Dr. Charles S. Henry, Colorado State University Multilayer Microfluidic Systems for Microchip Liquid Chromatography and Capillary Electrophoresis. Adam T. Woolley, Brigham Young University 9:00 9:30 10:00 10:30 11:00 11:30 12:00 1:30 2:00 2:30 Optimization of Micro-Fluidic Network Geometries for Micromosaic Immunoassays. N. Scott Lynn, Brian Murphy, Charles S. Henry and David S. Dandy, Colorado State University BREAK Microfluidic / Nanofluidic Sensors Using Catalytic DNA For Heavy Metal Detection. Donald M. Cropek, U.S. Army Engineer Research and Development Center Moving HPLC to the Microscale - Integration and Microfabrication. Don W Arnold, Eksigent Technologies Multilayer Crossover Poly(methyl Methacrylate) Separation Devices for Protein Analysis. Daniel J. Eves, Hernan V. Fuentes and Adam T. Woolley, Brigham Young University CONFERENCE RECEPTION 3:00 3:30 4:00 4:30 5:00 – 7:00 TUESDAY, JULY 29, 2008 Session II-A, Pharmaceutical Analysis, J. Shawn Roach presiding 8:15 9:15 10:15 10:45 FEATURED SPEAKER: LC – Method Development. Dr. Harold McNair, Virginia Tech A Systematic Approach to Reducing Matrix Effects in LC/MS/MS Analyses. Erin Chambers, Waters Corporation BREAK Utilization of LC/MS/MS Based Quantitative Assays for GLP Studies in the Academic Laboratory Setting. Daniel L. Gustafson, Bradley J. Samber and Ryan J. Hansen, Colorado State University Evaluating the Use of Total Organic Carbon (TOC) for Pharmaceutical Cleaning Validation (CV)/Verification of Phase I and Phase II Drug Candidates. Charles Pacheco, David Knight and Carman Bryant, Array BioPharma Inc. LUNCH (complimentary buffet included with registration fee) Understanding the Road to the IND. Dr. Dorothy Colagiovanni, Replidyne Foreign Particle Size Distribution and Characterization in Pharmaceutical Drug Products, Devices and Formulations using a High Throughput Electron Bean Analyzer. Marie C. Vicéns, Ph.D., Aspex Corporation Good Laboratory Practices and Standards for Laboratory Balances. Steve Wildberger, Shimadzu Scientific Instruments 11:45 12:15 1:30 2:10 3:00 Session II-B, LC/MS, Robert Lantz presiding 2:00 Development and Validation of a HPLC/MS/MS Assay to Determine the OSI-027 in Plasma. C. Tucker, S. Poondru, M. Hamilton, D. Gingrich, T Yang, E. Conklin and B. Johnson, OSI Pharmaceuticals Identification of Endogenous Levels of Adhesion Proteins from Cells Grown on 1 in2 Surfaces. Melanie J. Schroeder and Milan Mrksich, University of Chicago The Utility of Accurate Mass and High Resolution LC/MS/MS for the Analysis of Chemical Residues in the Environment. Michael C. Zumwalt, James M. Lau and Chin-Kai Meng, Agilent Technologies, Inc. 2:45 3:30 Session II-C, Poster Session 4:00 – 5:00 POSTER SESSION WEDNESDAY, JULY 30, 2008 Session III-A, MALDI, Scott Warder presiding Desorption Electrospray Ionization Mass Spectrometry (DESI-MS): Rapid In-situ Analysis of Ambient Surfaces. Nari Talaty, Christopher C. Mulligan, Ayanna U. Jackson and R. Graham Cooks, Purdue University; Steve Cepa, Abbott Laboratories Enhanced Microorganism Detection with Mass Spectrometry: Rapid Conversion of Bioagents to Ions. Nicolas Hauser, Yong-Seung Shin, Shaofeng Zhang and Franco Basile, University of Wyoming LUNCH (complimentary buffet included with registration fee) FEATURED SPEAKER: 50 Years of Chromatography. Dr. Harold McNair, Virginia Tech 9:30 10:30 12:00 1:15 2:15 Label-Free Protein Microarrays of Shewanella Oneidensis. Violeta Marin, Elizabeth Landorf, Frank Collart and Milan Mrksich, University of Chicago Mapping Protein Microheterogeneity: Applications in the Development of Biomarkers for Type 2 Diabetes. Randall W. Nelson, Ph.D. Arizona State University 3:15 Session III-B, Optical Biosensor Array, Greg Schneider presiding 8:30 9:30 10:30 11:00 Optical Sensors: The Current Time Point. Gregory P. Schneider, ForteBio, Inc. Development of the Octet RED System for Label-free, Multi-channel Kinetic Analysis of Biomolecular Interactions. Krista Witte, ForteBio, Inc. BREAK Analytical Applications for Biotherapeutic Protein Production. Ned Watson, SAFC Biosciences 50th Anniversary Banquet (complimentary dinner included with registration fee) 7:00 - 9:30 The Outlook for Energy: A View to 2030. Todd W. Onderdonk, Corporate Planning Exxon Mobil Corporation

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