CHL 202 Laboratory for Organic Chemistry II Spring , 2008 Text: Morhig, Hammond, Schatz, and Morrill, Modern Projects and Experiments in Organic Chemistry, Freeman, New York, 2003. Instructors: Thomas S. Straub, Ph.D., William A. Price, Ph.D., Michael J. Prushan, Ph.D. Date Experiment Jan. 16-17 EXP 19 Diels-Alder Reaction Jan. 23-24 EXP 20 Selectivity in the Bromination of Acetanilide Jan. 30-31 EXP 21 Acylation of Ferrocene Feb. 6-7 EXP 21 continued Feb. 13-14 PROJECT 5.2 Grignard Synthesis of Secondary and Tertiary Alcohols Feb. 20-21 PROJECT 5.2 continued Feb. 27-28 PROJECT 4 Interconversion of 4-tert-Butylcyclohexanol and 4-tert-Butylcyclohexanone. 4.1 Green Chemistry: NaOCl Oxidation March 6-7 SPRING BREAK March 13-14 PROJECT 4 4.2 Sodium Borohydride Reduction March 20-21 EXP 18 Phase Transfer Catalysis: Synthesis of Butyl Benzoate March 27-28 Exp 28.2 Synthesis of a Mosquito Repellant: N,N-Diethyl- meta-toluamide (DEET) April 3-4 EXP 28.2 continued April 10-11 PROJECT 11 Aldol-Dehydration Chemistry Using Unknown Aldehydes and Ketones. 11.1 Preparation and Characterization of Aldol-Dehydration Condensation Product April 17-18 PROJECT 11 11.2 Preparation and Characterization of Solid Derivatives of the Unknown Aldehyde and Ketone April 24-25 Check-out. All laboratory reports due!
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