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TAG cal std.xls

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TAG cal std.xls Powered By Docstoc
					Retention Time (min)Compound                                                    Target m/z:
       <18.5        Dihydro-3-methyl-2(3H)-furanone                                 56
        22.6        g-Heptalactone or Dihydro-5-propyl-2(3H)furanone (?)            85
        23.05       Naphthalene-d8                                                  136
        23.1        Naphthalene                                                     128
        23.5        n-Dodecane                                                      57
        24.87       Benzeneacetic Acid (Phenylacetic Acid)                          91
        25.2        2-Methylnaphthalene                                             142
         27         n-Tetradecane                                                   57
        27.5        Acenaphthylene-d8                                               160
        27.6        4-methyl-1,2-Benzenedicarboxylic Acid                           118
        27.7        Acenaphthylene                                                  152
        27.9        Spirodilactone or 1,6-dioxaspiro[4.4]nonane-2,7-dione           112
        28.05       g-Decalactone or 5-hexyldihydro-2(3H)-furanone                  85
        28.23       Acenaphthene                                                    153
        28.3        Acetovanillone or 1-4(hydroxy-3-methoxyphenyl)-ethanone         151
        29.5        n-Dodecanoic Acid                                               60
        29.55       g-Undecalactone or 5-heptyldihydro-2(3H)-furanone               85
        29.6        Fluorene                                                        166
        29.86       n-Hexadecane                                                    57
        30.3        Benzophenone                                                    105
        30.55       3,4-Dimethoxybenzoic Acid                                       182
        30.8        1,3,5-tri-2-propenyl-1,3,5-triazine-2,4,6-(1H,3H,5H)-trione     249
         31         g-Dodecalactone or 5-octyldihydro-2(3H)-furanone                85
        31.2        2-Pentadecanone                                                 58
        31.7        Acetosyringone or 1-(4-hydroxy-3,5-dimethoxyphenyl)-ethanone 181
        31.9        Myristoleic Acid                                                55
        32.05       n-Tetradecanoic Acid                                            60
        32.14       Phenanthrene-d10                                                188
        32.2        Phenanthrene                                                    178
        32.3        Anthracene                                                      178
        32.4        n-Octadecane                                                    57
        33.6        n-Nonadecane                                                    57
        34.13       cis-9-Hexadecenoic acid (Palmitoleic Acid)                      55
        34.35       n-Hexadecanoic Acid                                             60
        34.74       n-Eicosane                                                      57
        35.2        cis-10-Heptadecenoic Acid                                       55
        35.4        Fluoranthene-d10                                                212
        35.45       Fluoranthene                                                    202
        35.95       Pyrene-d10                                                      212
         36         Pyrene                                                          202
        36.2        (Z,Z)-9,12-Octadecadienoic Acid (Linoleic acid)                 67
        36.25       (Z)-9-Octadecenoic acid (Oleic Acid)                            41
        36.5        n-Octadecanoic Acid (Stearic Acid)                              60
        36.85       n-Docosane                                                      57
        38.8        n-Tetracosane                                                   57
        39.3        Benz(a)anthracene                                               228
        39.4        Chrysene                                                        228
        40.6        n-Hexacosane                                                    57
        42.1        Benzo(b)fluoranthene                                            252
   42.15       Benzo(k)fluoranthene                                         252
   42.3        n-Octacosane                                                 57
   42.76       Benzo(a)pyrene-d12                                           264
   42.81       Benzo(a)pyrene                                               252
   43.9        n-Triacontane                                                57
   45.2        Indeno(1,2,3-cd)pyrene                                       276
   45.3        Dibenz(a,h)anthracene                                        278
   45.65       Benzo(g,h,i)perylene-d12                                     288
   45.7        Benzo(g,h,i)perylene                                         276
   48.3        n-Hexatriacontane                                            57

Not detected
     ND        4-Heptanone (RT<18.5 min)
     ND        1,4-Benzenediol
     ND        4-hydroxy-3-methoxy-Benzeneacetic Acid (Homovanillic Acid)   137
     ND        2,5-Dihydroxy-4-Benzenedicarboxylic Acid                     162
     ND        Isoprimaric Acid                                             289
     ND        cis-5,8,11,14,17-Eicosapentaenoic acid                       67
     ND        cis-11-Eicosenoic Acid
     ND        n-Docosanoic Acid                                            60
     ND        (z)-13-Docosenamide                                          59
     ND        n-Tricosanoic Acid
     ND        n-Tetracosanoic Acid
     ND        cis-15-Tetracosenoic Acid (nervonic acid)
     ND        n-Pentacosanoic Acid
     ND        n-Hexacosanoic Acid                                          60
     ND        n-Heptacosanoic Acid                                         60
     ND        n-Octacosanoic Acid
     ND        n-Nonacosanoic Acid
     ND        n-Triacontanoic Acid
Confirmation m/z's Mass loading for 5uL injection (ng)
     41,85,100                    120
         56                       120
                                   25
                                   25
       71.85                       25
        136                       140
      115,141                      25
       71,85                       25
         80                        25
     162,89,90                    140
         76                        25
     56,84,101                    120
  41,55,100,128                   120
      152,154                      25
      123,166                     120
  73,129,157,200                  144
  41,55,100,128                   120
         83                        25
       71,85                       25
     51,77,182                    120
167,77,111,121,139                140
  83,125,208,234                  120
  41,55,100,128                   120
     43,59,71                     120
      153,196                     120
 69,83,97,208,226                 144
  73,129,185,228                  144
         94                        25
      89,152                       25
      89,152                       25
       71,85                       25
       71,85                       25
   69,83,97,236                   144
  73,129,213,256                  144
       71,85                       25
     69,83,251                    144
        106                        25
        101                        25
        106                        25
        101                        25
     81,95,280                    144
 55,69,83,264,282                 144
  73,129,241,284                  144
       71,85                       25
       71,85                       25
                                   25
                                   25
       71,85                       25
        126                        25
         126             25
        71,85            25
         132             25
         126             25
        71,85            25
         138             25
         139             25
         144             25
         138             25
        71,85            25


                         120
                         120
         182             140
180,198,53,78,106,134    140
275,304,121,87,243 (?)   140
   79,91,105,119,..      140
                         144
       73,129            144
     72,127,337          144
                         144
                         144
                         144
                         144
       73,129            144
       73,129            144
                         144
                         144
                         144

   Total mass (ng)       6464

				
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posted:4/19/2014
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