George M. Whitesides Department of Chemistry and Chemical Biology

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George M. Whitesides Department of Chemistry and Chemical Biology
Opportunities for Materials Science

in Energy, Sustainability, and Global

Stewardship



George M. Whitesides

Department of Chemistry and Chemical

Biology

Harvard



gwhitesides@gmwgroup.harvard.edu

Outline

• Introduction (from Geosynchronous Orbit)

• Production and/vs. Conservation

• Some energy production technologies

– Combustion of fossil fuel and CO2

management

– Nuclear

– Biomass

– Solar

– Wind

• Personal Perennial Technical Favorites

• Issues in Technology Transfer and Policy

Energy, Climate, Water,

Sustainability

Technology provides options to society

Energy

Wellbeing ≈

People

Options.

•Generate more energy

•Conserve the energy we now generate.

•Have fewer people

Constraints

• Energy and Climate

– Climate change may limit the combustion

of fossil fuel





• Energy and Water

– Water production may become a major use

of energy





• Energy and Nuclear

– Weapons proliferation

Scale and Units



• Energy: the ability to do work–

Joules (J)

• J = Volt·Coulomb

• Power: 1 W = 1 J s-1

• World: 14 TW = 14 x 1012 W =

3 x 1017 BTU/year

• United States usage = 3.3 TW

• Hoover Dam electricity

production = 2 GW

• China: +1 GW/week, coal-

burning

Some Systems Aspects of the Problem

• 14 TW (now) 30 TW (2050)

• Energy, Power, Climate, Water, Sustainability are linked

• What counts is function and price (along several

dimensions), not energy or power.

• Only a part of the problem is technical

• Radical social change may be part of the

“solution/resolution”

• Other possible technical contributors: IT, biotechnology,

nanotechnology, catalysis, materials

• All plausible solutions are capital intensive; the world

economy is largely capitalist. What about social return?

• Developed and developing economies often in conflict

Risk-Discounted Cash Flow-The Standard

Capitalist Model

Profits

(per year)

Research Costs

(per year)









Total Cash Flow



Is there any economic model that

justifies long-term/non-product

related research in industry?

Warning



• This area is complicated: the answer you get

depends on the question you ask, and what

system/part of a system you are considering.

• There may be an objective truth scientifically,

but not societally.

• Everyone has opinions/prejudices.



• …including me.

Production of Energy: No Free Lunch



• Hydrocarbons

• Coal Climate Change:

CO2, NOx, CH4, SOx

• Gas

• Nuclear Proliferation, Waste, U/Th Supply

• Hydroelectric

• Biomass NOx, Food, Water, Soil

• Geothermal

• Wind

• Solar Dilution, Efficiency



• H2 (from shift-gas reactions; electrolysis)

Conservation of Energy

• Tribology, Substantially more than 50

Corrosion, Wear % of produced energy is

• New materials to lost, somewhere.

prevent resistive

heating losses in

power distribution

systems

• Lighting: compact

fluorescents, LEDs

Combustion of Carbon-Containing Fuels

• >80% of Energy derived from carbon fuels

– Petroleum (40.1%), natural gas (22.7%), coal (22.9%)



Light-duty vehicle: 16.7

Other* Industrial: 9.5

14.2% Freight: 7.0

Aircraft: 3.4

Petroleum

Coal 40.1%

22.9%





Natural Gas

22.8%

Electricity generation: 20.8 Industrial: 8.0

Industrial: 2.0 Electricity generation: 6.0

Commerical: 0.1 Residential: 5.0

Residential: 0.01 Commerical: 3.2

Freight: 0.6



*Hydroelectric (2.7), biomass (2.8), geothermal (0.31), wind (0.15), solar (0.006), nuclear (8.13)

Combustion of Carbon-Containing Fuels:

Examples of Materials Issues



• CO2 Management

• Catalysis

• Fuels (low sulfur diesel, Fischer-Tropsch-derived fuels)

• Emissions (NOx, SOx)

• High Temperature Materials

• Efficiency, NOx/SOx control

• Separations

• CH4/CO2; O2/N2; H2/CO/CO2/H2S; …

• Machinery

• Tribology, wear, corrosion

Internal Combustion of Hydrocarbons:

An Example of Tradeoffs

• CnH2n + O2 CO2 + H2O

• Higher T

– Greater Carnot efficiency

– More demanding on materials

– The basis for Diesel engines

– More NOx

N2 + O2 NOx

NOx is a pollutant (oxidant)

NOx is also a green house gas

• Higher T thus requires after-treatment

– …which lowers efficiency

Carbon Management

• CO2 Sequestration (“minerals as materials”)

• Carbon Trading Credits

• CO2 Utilization

• CO2 Separation

• Biomass Production and Conversion

CO2 Utilization: The Chemistry of CO2 has

not been a hot topic



• Assume: Oxygen-fired coal plants

relatively clean, hot CO2; then ?

• Sequestration: Geochemistry and long-term

fate?

• Photosynthesis

• Other chemistry (carbon source with

negative price)

Reinventing the Chain



CH3CH3







CH2=CH2







HOCH2CH2OH



?

CO2

“Geoengineering”

• Sulfuric Acid Sols

– Tambora (1815) and the “year without a summer”



• CO2 for control

– Inject CO2 into atmosphere for “feedback” climate

control

Nuclear



• Regulatory Approval/Public Perception

• Proliferation

• Waste/Decommissioning

• U/Th Supply

Photosynthesis

Conceptually some similarity to

semiconductor pn photovoltaic

cells: separate charge (“H-”, H+)

Biomass

• Biomass to ???

– Shift gas (for H2 and synthetic fuels synthesis)

– Ethanol

– Biodiesel

• Fertilizer (Haber Process is energy intensive)

N2 + H2 → NH3 → HNO3 → NH4+NO3-

• Topsoil (soil is a material, and a limited

resource)

• Biomaterials

CH3 O

BioPDO

HO OH



O

Array of Photovoltaic Modules









Berkeley, CA: www.nrel.gov

Solar

• Photovoltaics (inorganic or organic)

• Solar Water Splitting

• Furnaces (Solar Thermal)

• Artificial Photosynthesis

• (Biomass Production)

The Heterojunction Solar Cell



1 Light absorption, exciton migration

n-type









cathode

material

anode





Band diagram of

charge-separated state

p-type

excitons

material

anode p-type n-type cathode

2 Charge separation material material

+ -- -

+ - - - +- -

+

cathode



+ +- --

anode









+ EF

+- + + -

-

EF

+ -- -

++

+ -

3 Charge transport, collection at electrodes

+ ++ - - --

- -

cathode









+ -- -

anode









+ +

++ -

-

- -

++ -

+ + - -

Order Correlates with Performance in Photovoltaics:

Cost vs. Efficiency Tradeoff









NREL

Options for Energy Storage



•Pumped water

•Compressed Air

•Thermal Energy

•Batteries

•Flywheels

•Capacitors

•Superconducting Grand Coulee Dam

Columbia River, WA

Magnets

•Redox Fuel Cells

Wind

Fuel Cells (and H2)



• Bypass Carnot thermo limitations (but have

others)

• Very materials intensive

• Fuel ? (H2, CH3OH)

– (H2: Generation? Transportation?

Storage?)

• High temperature (SOFC) materials?

– Can use hydrocarbons without reforming

• Catalysis – Design of new catalysts

Proton Exchange Membrane Fuel Cells



Nafion® Membranes









Anode: 2H2 4H+ + 4e-

Cathode: O2 + 4H+ + 4e- 2H2O

Overall: 2H2 + O2 2H2O + energy



www.fuelcelltoday.com Dupont

Supported Nanoparticles to Catalyze Reduction of O2 in

Proton Exchange Membrane Fuel Cells







O2 reduction is the rate-limiting step…



…Catalyst: Pt nanoparticle on

e- e- mesoporous carbon support

H+

H+ O2

H+

H+

H2 H+ H+



H+ H2O

H+



anode H+ cathode

H+



2H2 4H+ + 4e- O2 + 4H+ + 4e- Ferreira, et al. J. Electrochemical Soc.

2H2O 2005, 152(11), A2256.





Polymer membrane “electrolyte”

(doped perfluorocarbon)

The Oxygen Electrode

Kinetics of cathode reaction are much slower than the anode reaction

and limit economic viability of low temperature fuel cells



Cathode reaction: 4e- + O2 + 4H+ slow

2H2O



Periodic trends in oxygen reduction activity Alloying leads to oxygen reduction

activity enhancements



Pt3M single crystal surfaces

Pt is the best!









Pt3Co

oxygen binding energy



Volcano relationship between activity

and oxygen binding energy suggest

alloying improve activity



Nørskov et al. J. Phys. Chem. B 108 (2004) 17886

The Special Problem of H2



• Production:

– Electrolysis (nuclear or fossil)

– Shift gas (CHx + H2O H2 + CO2)

– Future direct solar?

• Storage

– Hydrides? Pressure?

• Transportation or on-site generation?

• Platinum? Alloys?

Conservation



A few examples of materials in a very rich field:



• New materials to prevent resistive heating

losses in power distribution systems

(electrical, gas, ..)

• Materials for reduction of friction, wear

• Corrosion resistance

Efficient Use of Energy

spiral type compact fluorescent light bulb









Plasma Display









Diesel Fuel http://www.de.nec.de/

Strategies for Materials Scientists in

Energy

• Try to solve problems relevant to

energy/sustainability involving materials.

• Work on what you were doing anyway, and

relate it to (or call it) “energy.”

• Join an ideological crusade around a

particular energy.

• Focus on technology transfer and startups

The Logic of University Research



• We have an energy/environmental problem

now.

• Urgency demands an immediate solution:

hence, engineering is the answer.

• Engineering is the application of existing

knowledge to the solution of practical

problems; science is the creation of

knowledge.

• …but what if the knowledge does not exist?

Research Universities: Some Generalities

• Energy/climate/water will be problems forever. Like

mortality.



• Universities must do long-term research: understanding

and radical invention.

------------------------ Profits

Energy Production: (per year)

Thermal (high T is good) Research Costs

(per year)

Electrochemistry (P = I2R = IV;

tradeoff between voltage

and current)

Sunlight is abundant but dilute

Rock, soil, and biomass are

materials (inter alia)

Energy Conservation

Light weight, strong, Total Cash Flow

corrosion resistant

Water, Climate, Sustainability

University Policy



• Education in the systems approach

• Multidisciplinarity

• Emphasize long-term and radical research

(universities bring freedom to explore

different options very inexpensively)

• Design of career paths for energy scientists

and engineers (including unconventional—

industry, foreign, foundation—support).

• Define objectives of tech transfer (solve the

problem; jobs; money for the university?)

Perennial Personal Favorites

• Catalysis as materials science

• Materials with extreme properties: low

corrosion/friction, high temperature stability,

durability, low weight,

• Mobile electrons in matter: Superconductivity,

Band-gap Engineering, photon-electron

interconversions…

• Separations

• Biomimetic and biological materials

• Nanotechnology (catalysis, membranes,

solar…small dimensions)

• “Impossible materials”

Technology Transfer in Energy…



• The historical templates—biotechnology and

information technology—don’t fit.

• The area is capital intensive, and although

there is capital, it is expensive

• Small companies will generally provide only

a part of a solution.

• Define the endpoint: independent company?

IPO? Acquisition?

Recognizing a Product Comes from:





• Extensive and joint (BusDev and Tech)

contact with potential customers.

– Difficult in a commoditized world, where only cost

counts

-----------------

• Symptoms of a Product:

Recognizing a Product Comes from:



• Extensive and joint (BusDev and Tech)

contact with potential customers

-----------------

• Symptoms of a Product:



– Someone will pay you for it.

– It’s technically a pretty sure thing



Scarcity and momentum:

Threaten and entice.

The “Product Arc”







REVENUE









TIME

National/International Science Policy



• Agreed on framework for carbon management

and climate change



• Agreed on policies for nuclear technology



• Broaden the technological base through

international collaboration

Conclusion



• Energy/climate/water/sustainability are

entwined, enormous problems for society

• No single solution will suffice. Probably a

combination of everything together will not

suffice.

• Unlimited opportunity, from radical invention

to engineering development.

• Funding and career track are still uncertain.

• Understanding the systems will help to avoid

wasting time.


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