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STUDY PROFILE





Name of Chemical/Technical





Study Type: Other Genotoxicity: Unscheduled DNA Synthesis in Primary Rat Hepatocytes /

Mammalian Cell Culture





OPPTS Guideline Number: 870.5550





Title of the Study:





Study Identification:





Prepared for:





Health Effects Division

Office of Pesticide Programs

U.S. Environmental Protection Agency







Prepared by:



Name of Registrant/Sponsor/Company





Study Report Date:

Unscheduled DNA Synthesis Assay (year of study) / Page 2 of 4

[NAME OF TECHNICAL/PC Code] OPPTS 870.5550

Study Profile version 07/04









STUDY PROFILE

prepared by [name of submitting company/lab]





STUDY TYPE: Other Genotoxicity: Unscheduled DNA Synthesis in Primary Rat Hepatocytes /

Mammalian Cell Cultures; OPPTS 870.5550 (in vitro)[§84-2].



TEST MATERIAL (PURITY): [use name of material tested as referred to in the study

(common agency chemical name in parenthesis)]



SYNONYMS: [other names and code names]



CITATION: Author [up to 3] (Date) Title. Laboratory name (location if needed). Laboratory

report number, full study completion date. MRID [no hyphen]. Unpublished (OR

if published, list Journal name, vol.:pages)



SPONSOR: (Name of Study Sponsor - indicate if different from Applicant).



INVESTIGATORS’ EXECUTIVE SUMMARY:



In an unscheduled DNA synthesis assay (MRID [number]), primary rat hepatocyte cultures were

exposed to [Chemical name, (% a.i., batch/lot #), include solvent if appropriate] at

concentrations of 0, x, x, or x g/mL for (duration of exposure).



Chemical name was tested [up to cytotoxic or precipitating concentrations, or limit

concentration, 5000 g/mL. (include other details as appropriate, quantitation if positive e.g.

there was a significant increase in number of cells in repair (60% at top concentration vs 1% in

controls))]. The positive controls induced (did not induce) the appropriate response. There was

(no) evidence (or a dose related positive response) that unscheduled DNA synthesis, as

determined by radioactive tracer procedures [nuclear silver grain counts] was induced.

Unscheduled DNA Synthesis Assay (year of study) / Page 3 of 4

[NAME OF TECHNICAL/PC Code] OPPTS 870.5550

Study Profile version 07/04



I. MATERIALS AND METHODS



A. MATERIALS:



1. Test Material: [as named in study]

Description: [e.g., technical, nature, color, stability]

Lot/Batch #:

Purity: % a.i.

Compound Stability:

CAS # of TGAI:

[Structure]

Solvent Used:





2. Control Materials:

Negative control: [e.g., culture medium]

Solvent: Concentration:

Positive control /solvent: Concentration:





3. Test compound concentrations used: [for preliminary cytotoxicity test, if performed, and

main assay]



4. Media: [Identify]



5. Test Cells: Mammalian cells in culture/primary rat hepatocytes. Describe cell line, cell strain

or primary cell culture [if primary cell culture, identify organ, animal] used:



6. Cell Preparation:



a. Perfusion Technique:



b. Hepatocyte Harvest/Culture Preparation:





B. TEST PERFORMANCE [(NOTE: If cells other than hepatocytes are tested, information

regarding the S9 activated phase of testing must be included)]



1. Cytotoxicity Assay: [if conducted, briefly describe procedure]



2. UDS Assay:



a. Treatment:



b. Preparation of Autoradiographs/Grain Development:

Unscheduled DNA Synthesis Assay (year of study) / Page 4 of 4

[NAME OF TECHNICAL/PC Code] OPPTS 870.5550

Study Profile version 07/04



c. Grain Counting: [include number of cells scored per dose, derivation of net nuclear grains,

whether % cells in repair were scored]



e. Evaluation Criteria: [describe]



f. Statistical Analysis: [list parameters that were analyzed and the statistical methods]





II. REPORTED RESULTS [Report results of analytical determination if performed]



A. PRELIMINARY CYTOTOXICITY ASSAY: [include concentration ranges; reported

results, e.g., cytotoxicity and solubility, rationale for dose selection for main study]



B. UDS assay: [reported results, e.g., net nuclear grain counts and/or summary;

appropriateness of positive controls and background levels (concurrent and/or historical);

number of concentration levels evaluated; number of replicates -- 100 cells/group (50

cells/slide); include representative table, if appropriate]





III. INVESTIGATORS’ DISCUSSION AND CONCLUSIONS: [Note any deficiencies and

how they impact on the study results and interpretation, if at all]



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