galtr ra nJJt \-l'Ll|-€)'
182OO West Highway 72
Gder\ Colrado 8O4Ol
(gB) 425'€021
.&Yenber 14, 1985
l,lr. L. J. Libby
?rpcess Engineer
Stone & l,ebster Engineering Corp. Title: Analysis
€reenrood Pl aza
P. 0. Box 5406 Reference:
&nver, C0 8A?f7
lbar Len,
Enclosed ane results on your Sample Nurber 46, submitted
-Itstober 29, 1985. Also enclosed is a copy of your cover letter
of the same date. t{e vill retain the whole sampl e and the
dlstillation fractions in case further analyses are required.
Very truly yours,
C?L #
CARL I'I. SMITS
Laboratory Supervisor
{l{S/eac
Encs.
cc: tlr. G. l{. Brown (slfEc)
Dr. il. T. Atnood (J e A Associates)
Dr. J. G. Huntington (J & A Associates)
Ffle Copies
tl
ra{5€ | ()r. J
*t t- -'
& WEBSTER ENGINEENING CORPONATION
STONE
Catalvtlc Craeklng Feedstock Analysls Request and Results
^ CLIart Code qL
&b [o. .//
Date Seut /O9-S-
Fccdstock Date Rectd
Retaln sanples of tbe overhead and bottous
or :rny requested aqarysls of those cuts.
FT'I.L SAI{PLE
Yolune I Overhead 0verhead Tenp. € IATM Actual Kettle Tenp.
IBP 626"F 330
5.0 690 365
10.0 729 393
15.0 766 T
20.0 794 -.ao-_
6.O 817 460
I
i 30.0 842 480
I
.i.a 35.0 - 868 501
i 40.0 890 524
'l
3
45.0 - 922 - 5s6
50.0 9s6 595
.56.t 54.9 - 1000 - 648
60.0 -
65.0 - -
Volt€lOOOoFOverhead 54.9 vol ? ,
52.3 wr
olPr c"""tt" eozOo s.G. 60/50
---- 20.4 --- 0.9317
27.9
r- 0.8878
-----_
Lt.7
--
0.9878
c (nrt)
t{L (vol t)
^
L
@"t
JF=fr66-.o-F--
€o"r * Resld
Recovered
,--/
_:7.s
18s.
186.3
87. s
a
rroor
1s2.J
47 .4
(se. I
tu; 89. 0
198.8
(44. s)
(se.4)
-
Full Sanple Gas 011 Cut Resld Cut
cravLtv e eooglropr) l/20-4
y' zz.s ,,/t, .t
Uol l{t.
Coposltlon -
Sol3ur (lwtf) /t.tz
toCal l{ltrogen (wppn) v? 0.87
Baslc Nttrogen (wppn) t/ 0.24
Bydrogen (wtt) 11.89 t/ Lz.7s t/
Carbon
Mctals
(:rtf) 85.28 G
-TO-oJs-
10.90
99.35
lftckel (wppn) / :ttt t/ 48.4
Vanadfu:n (wppn) t/ Nil
Sodtr:ra (sppn) t'/4.2 G '/
t/
s.4
1-8
Potasslum (wppu)
Conradson Carbon (rrtt)
ln{llne Polnt (oF) t/ rtt
4_v/ 204.6 -
,/tt
"
Bcptane rnsolubres
(1) Too viscous 1or anilinc pt. detm.
:
(Aphaltenes) (wtt)
Pcntane Insolubles (wel)
L- -/
.tj.6
I
I
Refractlve Index
lA Vlscoslty cs e 15ool/21ooP
Pour Polnt (or')
L'/- "- L--'
Parafflns - 44.3 7?.5
-a1 i
Cycloparaflnns Lr.a 11 .8
18. 8 ?3.1
Condensed Cycloparafflns
All^n-7t' ."*--d ttbg g
/ ,
/+oc/+-
5 TONE 8 WEBSTER ENCIXEEFIING CONPORATION
A
qFIG
C{tr xLL. *J
DENVER OPERATIONS CENTER
GneeNwooo pLAzA. Dexven. CotoRnoo
AOOR€SS ALL CORR€SPONO€NCE TO eo.aox 5406. OENVER. coLoRAoO 8O2t7-5406
tfLfq tr3-t rr&
rrvEt wu Y€L€r.5-..or
{rtLr;
qYLN EG
ic{N.*^grcrG
ssiQ OC
J+A
Dr. Mark T. Atwood October 29, f985
Vice President
J & A Assocl-ates
f8200 West Highway 72
Golden, Colorado 80401
Dear Mark:
Enclosed ls one (l) feedstock sample for your attention. please refer
to
the enclosed foms for the requested laboratory work. The type sampre and
code number are lLsted below:
Code No. Description
46 Fresh Feed
This wqrk should be bllled agalnst Stone & Websrer Blanket purchase order
No' EPR-BL-340-64-00198. Please include the sarnple number
tests in your Lnvoice. "rra """o.i";;;
Very truly yours,
2
d'e"-
"/'
L. J. Llbby l9 ,:
Process Engineer
b
LJL:JMG
Enclosures
f ULIATe,&
4h, fr fun+,frur,A uJ
+ +
( {,u .€ Lt&,
r'irtq
^
tq #4 / o { ,7 ,oJ tt:nqJ.
Table 2
liNT RES'LTS ON ATMOSPHERIC RESIDS,
SINGLE TESTS, GAS YIELD BY DIFFERENCE
Catalyst c-3 c-3 c-3 l,l-1407 1't-1407 t{-1407
Al tanont slrEc 16 (Ztnntni)
slrEc 17 Al tamnt sr{Ec 16 s}tEc I 7
Feed Yel I ow (Shengli) Yell ow (Shensl l) (Zhenal )
Tests at 900"F
T€mp, "F 902 904 902 900 903 n2
C/0 Ratio 3.2 2.9 2.9 3.2 2.8 2.9
xHs v 14.9 16.8 16.4 15.2 17.0 16.5
lttX Yield
Gas, By diff. 21.9 18.6 16.8 29.7 l4.t 16.0
0ll (C5+) 74.8 66.4 69.3 66.4 73.9 71.9
Coke, Total 3.3 15.0 3.9 3.9 12.0 12.3
3 on Catalyst 100 86 t00 100 80 75
% above bed 0 1400 20 25
Tests at 975"F
Temp, "F 976 976 974 978 972 972
C/0 Ratlo 3.2 2.9 3.0 3.2 2.8 2.9
ltHsv 15.2 16.4 16.0 15.2 17.3 15.6
l{t% Yields
Gas, By dfff. 4l .0 26.8 28.2 42.5 20.2 23.2
0t I (Cs+) 55.1 57.3 60.0 55.1 70.8 71.7
a Coke, Total 3.9 15.9 ll.8 2.4 9.0 5.1
% on Catalyst t00 59 50 95 50 67
% above bed 0 4I 50 5 50 at
clavtty (olpr)
FuII Sanple
-1Tf w @)
C 6oop
Conposlblon
Sulfur (wtf) U/ ' l-tT l. trr
W,+7"
Total Nltrogen 14pc) 0.lo L 0-6 o
Baslc Nltrogen ,.,ir, o')-'c a).o
Hydrogen (wtt) ll,L8
Carbon (wtl) I (,. zs 8t.s{@
MetaIs :fl
11 3TW
Nlckel
Vanadil:n (wppn)
Sodlun (wppn)
(wppn)
Potasslum (wppn)
Conradson Carbon (wbf)
4
ua
r/
-o3
, 2^r. +
cc)
J'l
_
+ 2+?
_-_-
5-+
Anlllne Potnt (oF) L23 2-L 2-
Heptane Insolubles
(Aphaltenes) (wtt) t/ 0.oL
Pentane Insolubles (wtl)
Refractlve Index ( to '(-)
Vlscoslty CS € l5OoF/21OoF
Pour Point (oF)
t/
re l.fo-o9
'lof
t.e"L
o /fr
' lo3
r'^ tt oF
l,lass Spectroscopy Analysls Method Q ru+'+ry h ,*',n .* tse
(ConPosltlon. wt1)
parafflns
/,'^\.-rt (^
t'tl
\7ffi
?7,
4F lill,-rl ,/r- c+ x
t/
Cycloparaflnns
Condensed Cycloparafflns
Allcy1 Benzenes (Mono-Aronatlcs) ,/ -s/z4t
Benzo Cyclo Parafflns a-/
Benzo D Cycloparafflns l/
TOTAL
Dlaronatlcs L- -
Trlaronatlcs I
Tetra-Aronatlcs L-
Penta-Arooatlcs
PoIy-Aronatlcs
Sulfur Aronatlcs t/
Furans
Not' Analyzed tr
TOTAL
78 0.5578 o.@79 0.0302 0.0097 0.627 o.o2s7 0.0699
z 104 0.0536 o.1gs7 0.0524 0.0017 0.0007 0.@75 0.0342
> 129, 130 o.m36 0.0613 0.M35 0.0133 0.0009 0.@25 0.0098
z r28 0.cxE8 0.0260 0.1142 0.5192 0.0057 0.@19 0.00CI
D 154 o"@05 0.0016 0.0212 ' 0.0357 '- 0.5075 0.0152 0.m26
> 166 o"{it004 0.0005 0.0060 0.0063 0.0452 0.4910 o.0226
I178. 0.0009 0.0005 o.@34 0.0023 0.0064 0. lo34 0.5073
." ? ''r1 E 78: 78+ 92+106+120+..'....toend
;1 !: --dltl.
+ 9f + 105 + ll9 + .:... toend(monoisotopic)
2 104 : 104 + ll8 + 132 + 146 + .,... toend
+ ll? + l3l + 145 + ..... to end (monoisotopic)
2 129 - l3O + t44 + 158 + 172 + ..... to end
+ 129 + 143 + 157 + l7l +..". toend(monoisotopic)
2 t28 - t28 + 142+ 156 + l7O + ..... tocnd
+ l4l + 155 + 169 + ' '... to end (monoisotopic)
2 154 - 154 + 168 + 182 + 196 + ..... to end 't
+ 167 + l8l + 195 + .. '.. to end (monoisotopic)
2 166 : 166 + l8o + 194 + 208 + .... ' to end .,
+ 179 + 193 + 2O7 + .. '.. to end (monoisotopic)
E 178 - 178 + 192 + 206 + 22O + ..... to end
+ l9l + 2OS + 219 + '.... to end (monoisotopic)
Table IV. Calculation Matrix-Inverse of Calibration Matrix
l{ominal type t78 > 104 zl?9 2 r28 > 154 t 166 X 178
Begtnes r .8904 -0.1601 -0.0942 -0.0290 -0.0021 -0.0421
+0.m25
-0.2345
Na$lhenebenzenes -0.1952 2.M79 -o.2284 +0.0016 -0.m)3 -0.1069
Dincphthencbenzencs +0.0124 -0.2806 2.3p.24 -0.0579 -0.0026 -o.00r8 -0.0266
Nap&thalenes -a.m.27 -o.ol02 -o.4937 l .9106 -0.0r95 -0.0151 -0.0020
Accoaphtlienes -0.0015 +0.0081 -0.0({o -0.1339 1.9773 -0.0584
2.0165 -0.0057
Fluorenes -0.001I +0.0011 -0.0154 -0.0r l6 -0. t822 -0.0904
Pheunthrenes -0.0029 +o.finl -0.0088 -q.w4 +0.012t -0.4192 I .9904
214. If the observcd height at 2W is lcss than the pcaks in a scries are plottL'd versus thcir masses' the curve is
186 end
catsdarcd height, thc observed hcight is rctained. Sinlilarly, non-linear and, if no ovcrlapping types arc prc:'ient, srnoothly
the orrcctcd hcight at 213 is the averagc of heiS,hts at 199 and approaches zcro as thc mass incrcascs. This is illustrated in
227. The corrcctcd hcight at mass 175 is the height at 16l Figure I for alkylbenzcncs in fractions isolated from a virgin
gas oil. Howcvcr. if the square root of pcak hcight is plottcd
less are-third thc algebraic dilltrence bctween hcights at 16l
and 203 again, if thc obscrvcd height at 175 is lcss than the as a function 106/massz, the plots are cssentialiy lincar at the
;
calcuhted hcight, the observed hcight is retained. The same higher masses, and dcviate only at thc lowcr masscs' Figure 2
prostdure is used at mass 176 using basc points at 162 and 2A4' shows the lincarity achicved for alkylbcnzcnes.
Finalty, heights at 189 arrd 190 are the avcrages of heights at A characteristic of distillation fractions is that thc highesl
175 and 203 and at rcspectively. The prcviously
176 and 204, molecular weight compounds will gcncrally hrve the fewcst
calculated or rctaincd values at 175 and 176 ate uscd in these rings and double bonds. Hcrtce, within a class lhe molecular
calculations. ions ncar the end of thc spcctrum will result only from tltr:
Tables III and IV give details of the pcak sunrmations, the nominal types, bccause thc llrst and sccond ovcrlap com-
pounds will have lower molccular weights. Similarly at the
original calibration data, and the inverse matrix ttscd in the
tlass anulysis. Although two scts of valucs are shown ior iow ttrott trnd o[ the spectrum thcre will be peaks relatively
benzencs in Table II, thc value based on the higher'molccular-
lit:e of contributions from the first and second ovcrlap types'
becausc the condcnscd aromatic nuclci do not liagment to any
weight benzencs was chosen, as thc molccular wcight range
approximates that of the majority of samplcs of intcrcst to our large extent. Thcreforc, base lincs constructt'd on the squarc-
laboratorics. Multiplication of peak-height summations by root plots can distinguish bctwcen contributiolrs o[ the nom-
the inverse matrix yiclds total-ionization values for cach class' inal and overlapping typcs. In ovcrlapping rcgions, from thtr
Because total ionization is approximately proportional to the
lowcst mass whcrc overlap can occur to thc cnd of thc (M-l)'
liquid volume of sample chargcd to the mass spcctromctcr (/'l), serics, pcak heights rcpresentc - f(P)
,YX
4
-j---*r
5
rDN/\-O
,' r4.
6
7
SAA/LEL" 4a VGD' a:tr.4€+ t/\q-A-.{
(t-)
J,\ ". Q9
8
9
---H G (LLg *o cUr*^ -e't-- F"t + ,\_ Clr-^--={
to
/L)
tl a-------> t
t2
t3
,l
t4
z
l5
l6 D
l7
t8
t9
Ce',a'J = pGnY 1a,4 3
-(
t' '7*
?o
2l L
h".^-0-- L.t o-(zt L)^J 4--'tut
5 5^ -]5,, 88 C',O13
22
3.35 n-' 4 * fo-
23
24
25
26
n/e\
LI
sL- | /
l+ae't ffif ft#)"-
27
,/'
?8
29
(a'tIY - A
1 &, +5 )/(*r, - ffi"t + ffi=,,")
30
:7.)
l/^
[ + ?c L
44
-..-- - Il -
45 A(
46
STONE A WEBSTER ENGINEERING CORPORATION
CALCULATION SHEET
a 5010.65
CALCULAT ION IDENTIFICATION NUMBER
J.O. OR W.O. NO. DIVISION O GROUP CALCULATION NO. OPTIONAL TASK CODE PAGE
-
( (. r,rr) + t,()
o
6 .o r
6
.1EsR - ,ot1 R-- ,136
?
A(fis: -.or-t la) - .1jG
I
n_ /
R (^) \)
9
lo 6 - ,13G f, il'r
Uctoc
eETT€RIT
/t
II 1
C?o46 '. 'lesps
t2 q A,G
"1d ?
23
?6 Y= e+ bY
?7 a y=4 xt$x)
28 X y:o-+Lr
q(P-G)
,1
=?P- G e --"(q - r) l
q!-a =
te-r)P € - p (- t,..r,o 1
a.4r5 (i",)+ r'bb*"f
G
1( R'= '18=
i? -:-
"o7-"t'
P
y-e
I/=
t-
3
.r
STONE A WEESTER ENGINEERING CORPORATION
CALCULATION SHEET
a s010.85
CALCULATION IDENTIFICATION NUMBER
,r.o. oR w.o. No. DIVISION A GROUP CALCULATION NO. OPTIONAL TASK CODE paee&o
/v757, /8 3l 86oz- G
I
-
2
3
E-qgMArLLt q
4 cAse L o Coan- Z Can-e
6
5
*{ ,oG
Tro--
. o: ;-oq- E 757 J[m
|tr-29
7s
l.oo
r.\Ff ND M
l,l? 8L
7 'S
8
C,-Cz 3,V6 ,3.q S1 a'qS t. o tl €,3 t,o t,3s
9
to ' QS- C,t tsjl 'n 1 t,6z 15/:(+ le.5s ?r to.95 l+.fl, 73
tl
l2 e"nrL* 53 54 53. ? t91 48.?+ qq.60 o.?2 4s.63 +.+.49 /,.&
t3
l4
t5
Leo n-qs 12 .oL t,o{ ILN ts.f7 t.o? 'lg ,o0 I ,0( ,.oJ
t6 Dg-rrO.i.Q s.zs L. o gs ufl3 -?. tg ,1 | 1 ,tt 1.+Lr I,
t7
t8
aD6€ U.69 6,V t.o+ 6.98 1'oo .11 7'71- 7-O l.o:
l9
20
R+{- 96 .a 9q,8 /,ol ,6.s 9l ,192 , T,LT t8 ,113
2l
22
23
?4
25
lLoo* }lv"in€.rror l.ol l.os l,lt
?6 -+ l,oG'LLrnor
27
2A
L U; I,U l,/+
?9
30
3l
52
35
34
55
56
57
l8
39
40
4l
,t.l 42
43
44
45
46
sIUNE tl WTASILR INGINEI.RING CORPORATION
CALCULATION SHEET
CALCULATION IDENTIFICATION NUMBER
/
J.O. OR W.O. NO. DIVISION A GROUP CALCULATION NO. OPTIONAL TASK CODE ,ourfuD
t+'771.lY . to, s? t l,qg 1,
9 ?- ?7. t8 L t12{ 7,175 )+-13 7'/f l€,78
{ )
ro
ll 3 6q 16 l,-111 a.?q1 tz,rt',5 0,5+ I | 1..+
(D
l:
t2 6 c \c/r2,9
l3
t4
t5
r6
t?
r8
b
a:
c7 / rr^t Qs =--------=- t--\
-l ,/ . \..
e/B- fc"lru 4.-l
r9
20 c AseF r- n t^?G
2_ :i/-c
.'1oL\ Z,V3 3,16
+
^
N 2l
22
D tD,51 ,)
\
2l 2 ?,/{ .6gc \ 6'37 e.78 ./
)
?4 l
23 3 6.aV e,Oq- ,j
26
A
27
?a
29
30
I c* /ren
3l
32
Ctsv
^
Fqf ^LPC
C+
r\ /
-*/'(C+ ( ot( ---.-,/
a
-- n(+ i Cr
53
34
I 3 \.?-5 t?'99 L'r
\,
en;'/oLv A n t 'bLu
.+9Q -e,ot/ru l,q1
35
56 z ?? .l a {5,7 8 7.to L.OI
\
{,v }
37
38
3 6+ 1t- tf . *1 ,+1L ) t'X'g
5.39 4'tqr
39 b i' t24v 1C. , fl €,N-C-D
ft \_=?
40
4l
,\\ 42
45
a1
J I Ullc, (a YILDJ I C.f\ C.ttloilrEC'nltre vvnrvnAr rvrr
'l--
-4.,.:!I-3tr CALCULATION SHEET
!iat): a s010.65
CALCU LAT ION IDENTIFICATION NUMBER
,r.o. oR w.o. No. DtvtstoN o GRoUP CALCULATION NO. OPTIONAL TASK CODE eaaeSdko
(?797,I3 2P BD o---
5
4
a
=
(c *ro) = cvf (a,+er'/rqr a,.f
5 F.s/s, ? .1G -.oosol| :-eP
6
6
7
clsE %
tt
C
.31
Faf
il, e{
@
,0'01
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FC
Fi- ,lL
t|,94 'llrS
rea
9
2 7? , ul- ?7, lg 1,75 L.87 ,LT ,31 688
to
ll
3 72.66 6Y.16 t'A:7 L S,5F 4,27 .rf J ,g a3
t2 +
r3
t4
r5 q
r6
t7
4 'fr?T G.^"&r^^.e : A(",gY- t.-s(+)r rr3(+^f-o,srz(rcpn) a ,*u ftf
t8
l9
PLZ6 '&- FaP
89,'59 9(.25
't!g- 6C
20
I 59,17- ,1+6
zl
2?
7 ?9.t+ 1-1, tt s7.rg --7€o
2f,
?4
? \7,bL b+,16 s4.87 o,759
23
26
27
toW Oit- | revpl Hco/rco -- .qar-.adsK6 -s (re- ro)tr
2A
.CAsr ^L .Kr Se % Te,o Hco v(o
29
50
I at,q t{.sq -lt .A6a lb,("\ +,q1 ra. le
3l
32
"- 79.|q t.1.{5 .Z* .aZS at.86 L,6l tS.f,5
33 3 7 2.6C tz q\ a'at '3r 3
54
35
,3] "'* -.!:7& l3" lJ. "
36
il- tll 7. YtE uus b)Fr.o= Ft..tl "ftoo (L,s-. oor=.)X**+- $S(r.e6- ,ozzaqg)]
6T t.o = L^(?l_-.ooott5C,FeP - lO,t9Z t .l\B f- *, r1r fOe]
37
38
39
ao
cts? l_( q,P
-i c-o
'ArlP S 0-b
G- NPf s kfCmo 6G u.o asY- Tco cr:l
4l
42
t gg.31 8t'?{ t.tt .i& t,z> s's,3 2't'( ?la, 177 ,12/ IL,LI w1
4a
44
2 77. /+ t z,tg t.q,.17 56.-r;
.1*Q 6a *L/ 52.3L
e$&b
9 /.
\\(
(
ro
ll
z .12-6 ,1v1 s,{( tL,zv 23,n: 6,?s i ..)to 67,t3 ,
+o.# !
t2 3 '?3* .1+g 6.t s
(-r+ og3zvt> i.-q,!ti cf5.63
-:158 {c.
r3
9 C l"ac/A e t-D=F T=aH/n
l4
r3
r6
t7
_12
t8
.-?l
S..kc = [=-..S.- i+. t2 1.115 )1 TorE
t9
20
eAs€ jls- LCou) 5;ro\
G 2l
22
| ,lC t2.66 fr/\ E.2e Hc991 Ft
.o56
r-S- cog{
L.68 sfii
L \ I
2' ,?+ l6'Lv g,3l , b.q3 ,o89 6. 8e .'75"/o
24
25
3 aa'8 e52-l q .f8 ,1.e3 7.zz- +.7r1 {
26 A/i'
27
fr ,c.2t t
2A
29
30
3l
Itr-% Roulcl,= .oo,31C.fQf-.03&tC - .Btfe? + tot,3
$^olJfl,; .'11t RpDCJ.- + ).5
52
53
Rvf , a.sKt *.3q-13.r
,-J-*-'*_-z*--z''-J, _,J' -- .- _/y--_:
r4_l qe€ E-N (Wz
\ I ^tt \
34 C AEU TL Ss-
f5
56
I t?,5t ,lb tt2{,) q?.s z-iE ffi,
\
, 1,+ )) -2. + ,,8, ll 77.t? (_qr.,3
57
2 te.v{ ) 8t,3 Xt,g
38
59
z l|7, t+l
\,r (
a.?s q)5j2 7z.ec 6+.1eL1z.q tr.8 tz
5
40 .-
4l -
\(\ 42
43
44
45
46
I
i
i l--l
ilr)
I
I
-'.l -- -!.-. -- +t- :i-ql
I
I I
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I
t--
I
I
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