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X-Ray Spectroscopy

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X-Ray Spectroscopy
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X-Ray Spectroscopy

The need for high resolution

X-ray spectroscopy 1 eV



Astrophysical Plasmas:



Simulation of the emission from

a gas at T = 107 K with normal

abundances of elements.





An energy resolution of ~ 10 eV

is required to begin serious 10 eV

X-ray spectroscopy and a resolution

of ~ 1 eV is required for complete 100 eV

plasma diagnostics and velocity

measurements.



Energy (keV)

What’s a milliCrab?



• The second brightest X-ray (1-10 keV)

source in the sky is the Crab nebula

• Its photon intensity at the top of the

atmosphere of the Earth is ~ 10 cm-2 s-1

• There are about 1000 AGN (“quasars”) at

a level of about .01 cm-2 s-1 = 1 mC

Oxygen Shock-Heated to kT ~ 0.3 keV





ionized



H-like







He-like





Ionization

age

X-Ray Spectrum with 100 eV Resolution









4-6 keV





Cassiopeia A ACIS spectrum

Estimates of H- and He-Like Energies vs Atomic Number

X-Ray Spectrometers - I



• Proportional counters have

– High efficiency

– Imaging capability

– Multiplex spatial/spectral without confusion



But resolving power ≡ E/(δE) ≈ 6√E(keV)

X-Ray Spectrometers - II

• Bragg crystal spectrometers

– Dispersive, so they can use any detectors

– Can achieve R > 103

– Can have high efficiency (at one E at a time)



But no imaging or multiplexing capabilities

(i.e. can look at only one E at a time)

X-Ray Spectrometers - III

• Gratings

– Dispersive

– Can have moderate (few %) efficiencies

– Can multiplex (all E at the same time)

– Can have R > 103/√E(keV) (better for low E)



But image and spectral orders are mixed

Capella

Chandra HETG

X-Ray Spectrometers - IV

• Solid State (including CCDs)

– High efficiency (>90%)

– Non-dispersive, can multiplex all E

– Imaging capability without confusion with E



But cannot achieve better than R ≈ 25√E(keV)

(Resolution ≈ 40√E(keV) eV)

The need for high resolution

X-ray spectroscopy 1 eV



Astrophysical Plasmas:



Simulation of the emission from

a gas at T = 107 K with normal

abundances of elements.





An energy resolution of ~ 10 eV

is required to begin serious 10 eV

X-ray spectroscopy and a resolution

of ~ 1 eV is required for complete 100 eV

plasma diagnostics and velocity

measurements.



Energy (keV)

X-Ray Spectrometers - V



• Cryogenic Microcalorimeters

– High efficiency (>90%)

– Non-dispersive, can multiplex all E

– Imaging capability without confusion with E



And can achieve R > 103 √E(keV)

Physical Conditions Through X-Ray Spectroscopy

Fe-K lines provide very clean diagnostics.

w

He-like Fe “triplet” He-like Fe Expected

y, x with XRS

z

(12 eV)

Neutral Fe



w x









Counts

H-like Fe

y z





Chandra

HEG

(~ 60 eV)









Energy (keV)



One such diagnostic: excellent density-independent

temperature sensitivity in the range 107–108 Kelvin.

The X-ray Microcalorimeter

Features high resolution, non-dispersive spectroscopy with high quantum

efficiency over K- and L- atomic transition band.









Moseley, Mather and McCammon 1984

Simple Energy Resolution Argument

• δT = E/C (temperature rise for E deposition)

• C ≈ N(kT)/T (N = # of phonons with )

• N ≈ C/k (fluctuation in N is the “noise”)

• ΔN = √N (Poisson statistics)

• R = E/(ΔE) (resolving power)

• ΔE ≈ kT√N ≈ kT√(C/k) ≈ √(kT2C)

• More carefully, ΔE = 2.35 ζ √(kT2C)

Spectral Resolving Power:

Doped semiconductor

Depends on thermometer technology









R (ohms)

Temperature-sensitive resistance



Resolution limited by thermal

fluctuations between sensor and heat

bath and Johnson noise.

Temperature

E  2.35 kT 2C

T = operating temperature (50-100 mK)







R (ohms)

C = heat capacity

Superconducting

 ~ 2 - 4 for doped semiconductors Transition

~ 0.2 for transition edge sensors

For both thermometer schemes a spectral

resolution of few a eV is possible! Temperature

Basic requirements:

• Low temperature

• Sensitive thermometer

• Thermal link weak enough that the time for restoration of the base

temperature is the slowest time constant in the system yet not so

weak that the device is made too slow to handle the incident flux.

• Absorber with high cross section yet low heat capacity

• Reproducible and efficient thermalization







Types of thermometers:

• resistive

• capacitive

• inductive

• paramagnetic

• electron tunneling

Microcalorimeter Arrays

Implanted Traces

X-Ray Absorber

(HgTe)



Implanted Thermistor

Silicon Spacer



Silicon Pixel

Silicon Support Beams

.

.

.









XQC Array: 36 array of

0.5  2 mm pixels.

X-Ray Quantum Calorimeter Dewar

Deep implants using

silicon-on-insulator wafers.



625 m pixels



GSFC

Fit Parameters

200

6.4 eV FWHM

FWHM: 6.40 ± 0.15 eV

E_shift: -19.95 ± 0.069 eV



Mn Ka1

Amplitude: 208.8 ± 4 counts

y0: 0.0 ± 0 counts

150  2: 1.43

Ion beam









Counts

100





1.5 m Mn Ka2

50

E

0



40

Residual







20

0

(after anneal) -20

-40

5860 5870 5880 5890

Energy [eV]

~ 6 times deeper Energy (keV)

thermometer

RTS – Rotating Target Source

X-ray lines









continuum

X-ray source





X-ray continuum









rotating target

wheel



targets (one is open

for continuum)

motor









target wheel


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