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Solid-state Raman lasers: a tutorial

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Solid-state Raman lasers: a tutorial
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Solid-state Raman lasers: a tutorial

Jim Piper

Professor of Physics

Centre for Lasers and Applications, Macquarie University, Sydney

(Carnegie Centenary Professor, Heriot-Watt University, Edinburgh)









Acknowledgements: H Pask, R Mildren, H Ogilvy, P Dekker

Australian Research Council, DSTO Australia









Solid-state Raman lasers

Overview of presentation

• Introduction to Stimulated Raman Scattering (SRS),

crystalline Raman materials, and solid-state Raman

lasers (SSRL)

• Raman generators (picosecond pulse conversion)

• External-cavity SSRLs (nanosecond pulse conversion)

• Intracavity (including self-Raman) SSRLs

• Intracavity frequency-doubled SSRLs for visible outputs

• CW external-cavity and intracavity SSRLs

Note excellent recent reviews of solid-state Raman lasers are given by:

Basiev & Powell Handbook of Laser Techn. & Applns B1.7 (2003) 1-29

Cerny et al Progress in Quantum Electronics 28 (2004) 113-143

Pask Progress in Quantum Electronics 27 (2003) 3-56



Solid-state Raman lasers

Stimulated Raman Scattering

Spontaneous Raman scattering was first reported by Raman and

Krishnan (also Landsberg and Mandel’shtam) in1928.

Stimulated Raman Scattering (SRS) arises from the third order

nonlinear polarisability P3 = eoc3E3, which gives rise to various

nonlinear optical phenomena, including also two-photon absorption,

stimulated Brillouin scattering and self-focussing.

Photons passing through a Raman-active

medium are inelastically scattered, leaving the

molecules of the medium in an excited

wP wS1

(usually ro-vibrational) state:

wS1 wS2

wS1 = wP - wR (first-Stokes generation)

wS2 wS3

wS2 = wS1 - wR (second-Stokes generation)

wS3 = wS2 - wR (third-Stokes generation)

wR

SRS does not require phase matching.

Solid-state Raman lasers

SRS theory*

* Penzkofer et al Progress in Quantum

Electronics 6 (1979) 55-140.



In the “steady-state” regime, where the pump duration tP is long

compared to the Raman dephasing time TR, the Stokes intensity

IS(z) grows as:

IS(z) = IS(0) exp (gR IP z)

where IP is the pump intensity, the steady-state Raman gain

coefficient is gR = 8pc2 N . ds in units cm/GW,

2w 3 G dW

hmS S

and the integral Raman scattering cross-section is introduced as

ds = wS4mS . h . da 2



dW c4 mL 2mwR dq

Here da/dq is the derivature of the normal-mode polarisability (the

square is proportional to c3), G is the Raman linewidth, the inverse of

the dephasing time i.e. G = TR-1, and small-signal conditions are

assumed. Typically TR ~ 10ps , G ~ 1011 s-1 or DnR ~ 5 cm-1.

Solid-state Raman lasers

SRS theory (cont.)

In the steady-state regime, gR scales with the Raman (Stokes)

frequency wS and the integral Raman scattering cross-section

ds/dW , and inversely as the Raman linewidth G = cDnR .

Raman media of choice for this regime have small Raman linewidth

(30. Thus for a high gain

crystal with gP ~10 cm/GW, and a crystal length 30mm, the pump

intensity needs to be IP >1GW/cm2. This is above the damage

threshold of many materials!



Solid-state Raman lasers

SRS theory (cont.)

In the transient Raman regime, where tP 10 ps.

Raman crystals are chosen for high Raman gain and damage threshold (e.g.

BN, KGW, BW). First-Stokes pump thresholds are typically ~0.5-1GW/cm2.

For ultra-short pulses 1

input output

R1 , R2 reflectances at first-Stokes

mirror 1 mirror 2



Resonating the first- and higher-order-Stokes fields effectively reduces the

Raman threshold: for a 50mm-long BN crystal the calculated threshold for

first-Stokes from a 1064nm, nanosecond pump is ~10 MW/cm2 compared

with ~300 MW/cm2 for single-pass Raman generation*.



Achieving high conversion efficiency requires matching of the pump

mode to the Raman Stokes mode in the resonator. At (Stokes) average

powers > 1W this is likely to require consideration of thermal lensing in

the Raman crystal due to heat deposition by the Raman process itself.

* HM Pask Prog. Quantum Electron. 27 (2003) 3-56.



Solid-state Raman lasers

External-cavity (resonator)

Raman lasers

Basiev et al, OSA Advanced Solid-State Photonics 2004, TuB11



High average power

8 x 145mJ, 50ns, 50ms BaWO4 95mm

30 Hz at 1064nm





Nd:YAG 35W

85%T 1064nm 3.2mm 77% R, pump

HR 1st-3rd Stokes 55% T 1st-3rd Stokes





High energy

50 x 380mJ, 50ns BaWO4 95mm

20 kHz at 1062nm





Nd:GGG 19J

85%T 1064nm 3.2mm 77% R, pump

HR 1st-3rd Stokes 55% T 1st-3rd Stokes





Solid-state Raman lasers

External-cavity (resonator)

Raman lasers

180mJ, 20ns Ba(NO3)2 70mm Ermolenkov et al, J. Opt.

10 Hz at 532nm Technol. 72 (2005) 32.

35mJ, 10Hz 1st-Stokes at

90%T 532nm HR, pump

HR 1st-Stokes

5mm

70% T 1st-Stokes

563nm (20% eff.) external

SHG 4.2mJ at 281nm

176mm unstable







Takei et al, Appl. Phys B

140mJ, 20ns Ba(NO3)2 58mm

20 Hz at 1064nm 74 (2002) 521.

11mJ, 20Hz 3rd-Stokes at

HR pump 1598nm (eyesafe region) after

HT 1064nm 5mm

HR 1st-3rd Stokes HR 1st-2ndStokes compensation for strong

71% T 3rd-Stokes thermal lensing in BN

200mm







Solid-state Raman lasers

External-cavity Raman lasers

Mildren et al, OSA Adv. Solid-State Photonics 2006, MC3

*also Mildren et al, Opt. Express 12 (2004) 785; Pask et al, Opt. Lett. 28 (2003) 435.





2.4W at 532nm KGW 50mm

10ns, 5kHz 100 100









Output Coupler Transmission (%)

Fraction of Output (%)

80 80



90%T 532nm HR pump, 1st-Stokes

160mm 60 60

HR 1st-2nd Stokes 50-60% 2nd-Stokes

40 40

52mm mode-matched

1.6 20 20



1.4 KGW E//Nm

0 0

1.2 (588nm)

OUtput Power (W)









560 580 600 620

1.0 Wavelength (nm)



0.8

KGW E//Ng

0.6 (579nm) Conversion efficiency into 2nd-Stokes

0.4 at 588nm: 64% (slope eff. 78%);

0.2 at 579nm: 58% (slope eff. 68%).

0.0

0.0 0.5 1.0 1.5 2.0 2.5

Input Power (W)



Solid-state Raman lasers

Intracavity Raman lasers

Intracavity Raman lasers allow for both the pump and the

Stokes wavelength(s) to be resonated, substantially reducing

the effective Raman threshold (~MW/cm2)

Nd3+ laser

Intracavity Raman

diode

crystal

* Raman crystal

*including coupled-cavity

pump



Mirror 1 Q-switch Mirror 2

HT pump HR pump/ fundamental

HR fundamental/Stokes Stokes coupling



Nd3+ laser/

Raman crystal



Intracavity self-Raman

Mirror 1

Q-switch Mirror 2

HT pump HR pump/fund

HR fund/Stokes Stokes coupling



Solid-state Raman lasers

Intracavity crystalline

Raman lasers

Effects of thermal lenses on resonator design

Pask & Piper, IEEE J. Quantum Electron. 36 (2000) 949.

*also Pask, Prog. Quantum Electron. 27 (2003) 3.



Resonator mode 1.0









stability parameter g2

1. I=0 4. I=32A unstable

size taking account 0.8 2. I=11A 5. I=38A region

of LIO3 thermal lens 3. I=14A 6. I=40A 6

Plane HR mirror

Nd:YAG LiIO3

0.6

Plane OC mirror 45



1000 0.4

900

instability

1

800 0.2 2

3

unstable region stable region

beam waist (µm)









700

0.0

600

-3 -2 -1 0 1 2 3

500

400 stability parameter g1

300

200

100

0

0 5 10 15 20 25 30 35 40 45 50 55

Mode size taking pump mode size

position (cm)

account of Nd:YAG

thermal lens only

Solid-state Raman lasers

All-solid-state intracavity

Raman lasers

Nd:YAG Raman crystal

diode

pump



HT pump Q-switch HR pump/ fund

HR fund/Stokes Stokes coupling



Diode Raman l first t pulse/prf Stokes Reference

power crystal Stokes power/eff

5W CaWO4 1178nm 6ns/10kHz 0.5W/9% Murray et al, OSA TOPS 19

(1998) 129

30W Ba(NO3)2 1197nm 15ns/10kHz 3W/10% Pask & Piper, IEEE JQE 36

(2000) 949

30W LiIO3 1156nm 20ns/10kHz 2.6W/9% Pask & Piper, IEEE JQE 36

(2000) 949

23W KGd(WO4)2 1158nm 30ns/15kHz 4W/17% Mildren et al, Opt.Lett. 30

(2005) 1500

10W BaWO4 1181nm 24ns/20kHz 1.6W/17% Chen et al, Opt. Lett. 30 (2005)

3335



Solid-state Raman lasers

Intracavity Raman lasers

Spatial and temporal characteristics

Raman beam clean-up is

observed for intracavity

Raman lasers. Despite

poor mode quality on the

fundamental, the Stokes

field grows in the lowest

order (TEM00) mode*#.

* Murray et al, Opt. Mater. 11 (1999) 353, #Band et al, IEEE JQE 25 (1989) 208.



The Stokes output is commonly observed

to be strongly modulated at the cavity

round-trip time. This is due to self-

modelocking, which arises from the

dynamics of energy transfer between

fundamental and Stokes fields (analogous

to synchronous pumping)#.



Solid-state Raman lasers

(Intracavity) self-Raman lasers

Andryunas et al, JETP Lett, 42 (1985) 410 first reported self-Raman

conversion in Nd3+ doped tungstates. Grabtchikov et al, Appl. Phys. Lett. 75

(1999) 3742 a self-Raman laser operation based on a 1W-diode-pumped

Nd:YVO4 / Cr4+:YAG microchip, giving 15mW 1st -Stokes at 1181nm in sub-ns

pulses at 20kHz. Subsequently there have been numerous reports of diode-

pumped, Q-switched self-Raman lasers based on Nd:SrWO4, Nd:BaWO4,

Nd:PbMoO4, and Yb:KLu(WO4)2.

Chen, Opt. Lett. 29 (2004) 1915 has

demonstrated a diode-pumped, Q-

switched Nd:YVO4 self-Raman laser

giving 1.5W on first-Stokes at 1176nm

(20kHz) from 10.8W pump (13.9%).

Using mirrors coated for 1342nm

fundamental and1525nm first-Stokes,

1.2W is obtained in the eyesafe region

from 13.5W pump (at 9% diode-S1)

Chen, Opt. Lett. 29 (2004) 2172

Solid-state Raman lasers

Intracavity frequency-doubled

Raman lasers

The high intracavity fluences which can be achieved if the fundamental

and Stokes wavelengths are resonating in high-Q cavities are well-

matched to intracavity sum-frequency/second harmonic generation.



Nd:YAG

Pask & Piper, Opt.Lett. 24

Raman crystal LBO

(1999) 1492 reported 1.2W

at 578nm from an

intracavity frequency-

HR end doubled, crystalline LI laser

input

mirror Q-switch mirror based on Q-switched

(10kHz) Nd:YAG laser.

Nd:YAG LBO dichroic 1.7W at 579nm has been

turning/

output

reported subsequently for

mirror KGW at diode-yellow

efficiencies ~ 9.5%*

*Mildren et al, OSA Adv. Solid-

State Photonics 2004, TuC6.

Solid-state Raman lasers

Intracavity frequency-doubled

Raman lasers

At the design operating point, the laser resonator must be optically stable

and give the optimum mode sizes at the fundamental laser crystal, Raman

crystal and SHG crystal, to give maximum extracted power and avoid

optical damage to the components*.

* Design of intracavity frequency-doubled cyrstalline

Raman lasers subject to USA Patent No. 6901084









Nd:YAG Raman crystal Q-switch M2 flat LBO M3 (R=300mm)



M1

flat



250mm overall resonator length

Solid-state Raman lasers

Discretely tunable visible

all-solid-state laser

Mildren et al, Opt. Lett. 30 (2005) 1500 demonstrated that intracavity

SFG/SHG can be used in combination with intracavity SRS in crystalline

materials to select one of a wide range of visible outputs from the

second-harmonic of the fundamental, to various combinations of sum-

frequency and second-harmonic of the various cascading Stokes orders.

1st 2nd

Using angle- or temperature-tuning of Fund Stokes Stokes

the nonlinear SFG/SHG crystal, the

fundamental or Stokes field can be

dumped by way of the nonlinear

coupling through a dichroic cavity

optic. To avoid cavity mis-alignment

issues with angle tuning, or large

temperature ranges in tuning a single SHG SFG SHG SFG SHG SFG

532 555 579 606 636 nm :768cm-1

NL crystal, a second temperature- 532 559 589 622 658 nm :901cm-1

tuned NL crystal can be introduced. KGW





Solid-state Raman lasers

Discretely tunable visible

all-solid-state laser

ANGLE-TUNING TEMPERATURE-TUNING

resonator LBO 1 LBO 2

a axis =90, =90,

=0 =11.6



TEC TEC



LBO1 Wavelength Output Temp Temp Wavelength Output

Angle (nm) power (W) LBO1 LBO2 (nm) power

(W)

0 579 1.8

19 C (52 C) 606 0.25

11  555 0.95

48 C (52 C) 579 0.57

17  532 1.7

95 C (52 C) 555 0.52

- 25 C 532 1.5

• beam displacement

• phase-matching limits possible •temperature range too big for single stage TEC

wavelengths •low powers due to insertion loss of 2nd crystal

•dual crystals reduce switching times

Solid-state Raman lasers

CW crystalline Raman lasers

Reaching threshold for CW operation of Raman lasers requires small mode

sizes to achieve pump intensities high enough for sufficient Raman gain, and

low-loss (high-Q) resonators.

Grabtchikov et al, Opt. Lett. 29 (2004) 2524 reported the first CW crystalline

Raman laser using BN in an external-resonator pumped by an argon ion laser.

Ar+ pump BN, l =68mm

5W, 514nm 164mW, 543nm ( ~3% pump-1st Stokes)









Demidovich et al, Opt. Lett. 30 (2005) 1701 subsequently demonstrated a

(long-pulse) CW Raman laser at 1181nm based on self-Raman conversion in a

diode-pumped Nd:KGW laser (intracavity self-Raman gives reduced losses).



diode pump Nd:KGW, l =40mm

2.4W, 808nm 9(54)mW, 1181nm ( ~2.5% diode-1st Stokes)



1067nm





Solid-state Raman lasers

CW crystalline Raman lasers

Pask, Opt. Lett. 30 (2005) 2454 recently 2000

TEM22









Threshold power (W)

calculated pump (fundamental) power 1500

237µm

threshold for CW intracavity KGW Raman

laser: 1000 TEM00

R2 (1  L) exp( 2 g R I L l )  1 500

136µm



L =total non output coupling losses at the

0

Stokes wavelength (1%)

0 1 2 3 4 5

R2 = reflectivity of mirror M2 (0.25%)

total cavity loss (%)





Nd:YAG KGW 800mW









1176nm power (mW)

800

diode 1176nm

600

pump 400

unstable

200

Maximum stable CW Raman output power

was 800mW for 20W diode pump power at 0

0 10 20 30

diode-1st Stokes (1176nm) efficiency ~4%*

diode input power (W)



Solid-state Raman lasers

A CW intracavity frequency-doubled

crystalline Raman laser?

Efficient, high-power CW operation of intracavity crystalline Raman lasers

offers the prospect of using intracavity SFG/SHG to make simple, compact

and efficient CW visible sources:









Instantaneous 588 nm power ( mW )

Nd:YVO4 KGW LBO 1600

CW (100% duty cycle)

22W diode 1400 Modulated (50% duty cycle)

1200

1000

800

Dekker, Pask and Piper (submitted to 600

Optics Letters) report 700mW CW output 400

at 588nm by intracavity SHG of 1196nm 200

1st -Stokes of KGW pumped intracavity by 0

1064nm from diode-pumped Nd:YAG, at 2 4 6 8 10 12 14 16 18 20 22 24 26

diode-yellow efficiency ~5%. Instantaneous incident pump power ( W )



Improved resonator design and thermal management are expected to

result in ~2W cw yellow output at ~8% diode-yellow. A miniature

(25mm) intracavity frequency-doubled Nd:GdVO4 self-Raman laser has

already demonstrated >100mW cw yellow for a 3W diode pump!



Solid-state Raman lasers

Solid-state Raman lasers: a tutorial



Thank you for your attention!









jim.piper@vc.mq.edu.au



Solid-state Raman lasers


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