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ESM 282

INTRODUCTION

Mercury is present in the environment as a result of both natural and anthropogenic activities. A

persistent bioaccumulative toxic metal, the amount of mercury released into the environment has

increased significantly since pre-industrial times (see Figure 1). It‟s low boiling point allows

mercury to move freely through the environment and for the transformation from one chemical

compound to another (Ayres & Ayres, 147).



Most of the mercury present in the atmosphere is elemental mercury vapor, with only a small

fraction of it bound to airborne particles. This form may circulate in the atmosphere for up to a

year, resulting in the wide dispersal and transport of mercury up to thousands of miles away from

its source (EPA). In contrast, most mercury present in water, soil, sediment or plants and

animals is in the inorganic form of mercury salts and organic forms of mercury (e.g.,

methylmercury). Inorganic mercury is readily removed from the atmosphere by precipitation

and dry deposition (EPA). The methylation of mercury (i.e., the organic form) makes it

available for uptake by organisms such as bacteria, which are consumed by fish. Via this route,

mercury slowly makes it‟s way up the food chain, where it bioaccumulates in animal tissues.

Most of mercury‟s chemical compounds are in a form that is toxic to higher animals, resulting in

a variety of debilitating health effects.



Several studies have suggested that the relative contribution of mercury loadings to land and

water from atmospheric deposition can be substantial (EPA). However, there are few, if any,

permanent environmental sinks for mercury, resulting in indefinite environmental residence

times. Mercury is most persistent in sediments (~2.5*108 yr. residence time), followed by the

ocean and soils with residence times in the 1,000s of years. Mercury may be present in the

atmosphere for up to a year, although the average is only an ~11 day residence time. In addition,

mercuric species are subject to much faster atmospheric removal than elemental mercury (EPA).

Due to the properties of bioaccumulation and „biorecycling‟ of methyl mercury, environmentally

accumulated mercury will be available for many years (Ayres & Ayres, 147).

Figures 1a-1d: Pre-man versus 1978 flows of total mercury. (Ayres & Ayres, 150-151).





Atmosphere Terrestrial



80 70,000

70 60,000

60 50,000

kMT per ye ar









kMT per ye ar

50

40,000

40

30,000

30

20 20,000

10 10,000

0 0

Pre- 1978 Pre- 1978

man man









Ocean Sediment



41,900 330,000

41,800

kMT per ye ar (in millions)









328,000

41,700

kMT per ye ar









326,000

41,600

324,000

41,500



41,400 322,000



41,300 320,000

Pre- 1978 Pre- 1978

man man

ANTHROPOGENIC SOURCES

Mercury (Hg) has been mined for industrial uses for more than a century, and yet only a few

decades ago was it recognized to be a major environmental hazard. Today textbooks revere it as

a classic example of a toxic metal, which has the ability to bioaccumulate in the tissues of

animals of higher trophic levels. However, before the adverse environmental effects of mercury

were known, it was mined extensively due to its ability to conduct electricity, and the ability to

form amalgams with other precious metals (Ayres & Ayres, 147). The U.S.G.S. and the U.S.

Environmental Protection Agency (EPA) estimated that ~158 metric tons of mercury are emitted

annually into the atmosphere by anthropogenic sources in the United States. Of these 158 tons,

87% (137.4 tons) is from combustion point sources, 10% (15.8 tons) is from manufacturing point

sources, 2% (3.16 tons) is from area sources, and 1% (1.58 tons) is from miscellaneous sources

(EPA).

U.S. Anthropogenic Emissions









manufacturing

10%



area

2%

miscellaneous

1%



combustion

87%









Four specific source categories account for approximately 80% of the total anthropogenic

emissions—coal-fired utility boilers (33%), municipal waste combustion (19%),

commercial/industrial boilers (18%), and medical waste incinerators (10%) (EPA). These four

most significant sources represent high temperature waste combustion or fossil fuel processes.

For each of these operations, the mercury is present as a trace contaminant in the fuel or

feedstock. Because of its relatively low boiling point, mercury is volatized during high

temperature operations and discharged to the atmosphere as exhaust gas (EPA). Thus the main

environmental concern with anthropogenic mercury concerns emissions into the atmosphere.





Mercury Uses and Emissions Breakdown

Man first mined mercury in the form of the red colored mineral cinnabar for use as a pigment in

cosmetics and paints. A more profitable purpose for mercury arose in the nineteenth century

when it was used extensively to separate grains of gold and silver from riverbed gravel and

alluvial deposits (Ayres & Ayres, 160). Today the mining of silver and gold has replaced the use

of mercury as an amalgam with a process using cyanide. However, small mines that continue to

utilize mercury still exist (mostly in developing countries), as 1990 figures reported the

production of ~448 metric tons (Ayres & Ayres, 161).



The next major use of mercury (311 tons used in 1987) came during the first part of the twentieth

century, when its catalysts were used to manufacture acetic acid, acetaldehyde, and other

chemicals (Ayres & Ayres, 161). This use of mercury was again replaced, this time by ethylene.

The most consistent use of mercury, according to Ayres & Ayres, during the last century has

been in the manufacture of chlorine via the electrolytic process, hence the „mercury cell‟. Since

the 1940s chlorine production has steadily risen spurred by growing demands for elemental

chlorine as a germicide or bleach, polyvinyl chloride, chlorinated solvents, and many other uses,

all of which require mercury in the manufacturing processes. Tighter regulations and

bookkeeping over the latter half of the century have reduced the emissions of mercury per ton of

chlorine produced from 300mg/kg of product to 150mg/kg (Ayres & Ayres, 165). Mercury

emissions via the electrolytic process thus account for roughly 77 metric tons per year.



The largest single use of mercury has been in battery manufacturing, using approximately 250

tons in 1990 (EPA). Mercury has two main purposes for the production of batteries. The first

use is as a component in the zinc-mercury amalgam used as the anode in mercury oxide and

alkaline batteries and as a component in the cathode of mercury oxide batteries (EPA). The

second use serves to inhibit side reactions and corrosion of the battery casing material in carbon-

zinc and alkaline batteries (EPA). Before the 1980s, most batteries and some storage batteries

contained mercury in the form of mercuric oxide (HgO), zinc amalgam (Zn-Hg), mercuric

chloride (HgCl2), or mercurous chloride (Hg2Cl2) (EPA). Technological improvements made by

the battery industry within the last couple of decades are resulting in a phase out of mercury in

battery production. These improvements have shown to be successful, as the 1992 estimate of

mercury emitted from the production of batteries was 0.02 tons.



Approximately half of the batteries used in the United States end up in landfills or are dissipated

and/or incinerated, resulting in significant mercury emissions to the environment (see Figure 2).

The electrical industry also produces components using mercury such as florescent lamps, and

wiring devices and switches (fever thermometers and thermostats). These uses require roughly

141 tons of mercury annually (Jasinski), and emit less than 1 ton of Hg in the manufacturing

process. The emissions of mercury from these sources are more likely to occur when the product

is broken and/or discarded; hence the majority of these emissions end up in landfills and/or

incinerators as well.



Dental preparations (amalgams in fillings), and laboratory uses annually require roughly 57 tons

of mercury. Most of this mercury is captured in the use of the products manufactured; however

the end fate of these products is either incineration or landfilling, resulting in respective

emissions of 35 and 4 tons to the environment. Anti-fungal paints, measuring and control

instruments, and other miscellaneous uses comprise the remaining sources for mercury.

Together, these sources amount to approximately 16 metric tons of mercury lost to the

environment annually. The majority of losses occur via the manufacture of paints using mercury

as a paint additive. Current regulations however, have called for the elimination of mercury in

this process and emission levels are expected to reflect this decrease in future studies. A more

comprehensive and „outlined‟ diagram depicting all of these sources, uses, and emission figures

are found in Figure 2. (Note that more detail is depicted in the diagrams than is discussed.)





LEAKS TO ENVIRONMENT

Current emissions of mercury from manufacturing sources are generally low compared to

combustion sources (with the exception of chlor-alkali plants). The EPA identified that the

largest source of emissions is fossil fuel combustion (163 tons annually) by utility boilers

(particularly coal combustion). The other significant sources of mercury emissions are from

municipal waste combustors and medical waste incinerators. Because the vapor pressure of

mercury metal is strongly dependent on temperature, and it vaporizes readily under ambient

conditions, most of the mercury emissions are found in the atmosphere as mercury vapor.



Approximately 96 tons of mercury lost to the environment, mostly as mercury vapor, are from

area source manufacturing (Jasinski). The majority of losses, and these include losses to the

atmosphere (by incineration and/or dissipation) as well as to landfills occur post-production. As

stated earlier, these emissions are the result of products being discarded or broken. Intuitively

speaking, we can assume that if future consumption of mercury remains constant, emissions

from these manufacturing sources will remain constant as well. To combat emissions from fossil

fuel combustion, innovative ideas to increase fuel efficiency, as well as new technological

advancements, must be actualized by the utility industry, depending greatly on the nation‟s

future fuel energy needs. These leaks to the environment from each sector are shown in Figure

2.





Missing Mercury

As is demonstrated in Figure 2, the annual consumption of mercury in the US is greater than the

annual release. This results in a large quantity of „missing‟ mercury. The US Bureau of Mines

and the EPA (under the Toxic Release Inventory, or TRI) provide comparison data on mercury

consumption by the US chlor-alkali industry vs. mercury emissions in Table 1. The data

reported regarding „releases and transfers‟ for the production, consumption and major uses of

mercury indicate that inflows do not equal outflows for the mercury system. Apparently, a

significant portion of the mercury consumed by the chlor-alkali industry (which is all for

replacement uses) has mysteriously disappeared from these statistics. Thus, most of the mercury

being consumed is unaccounted for in the TRI (Ayres & Ayres, 167). This is a large discrepancy

that has only a handful of explanations.



One possibility is that the emissions reports are falsely generated (either intentionally or not),

due to a lack of information on the part of chlorine manufacturers. A second possibility lies in

the interpretation of the discrepancy between consumption and emission rates. It may be

assumed that the reported emissions rates refer only to air and process water, while most of the

mercury is probably accumulated in semi-solid or solidified sludges from process water

treatment. This sludge may be stored or buried on site or shipped to a landfill, and thus not

accounted for under the typical reporting framework. A third possibility lies in the fate of

mercury as a contaminant of the chlor-alkali products. Mercury contamination in caustic soda (a

Table 1: Mercury in chlorine production in the US (tonnes).

USBM Minerals EPA US Bureau of Mines

Yearbook

Year Consumption EPA OPPT* Releases Releases Transfers Total



1987 311 23.7

1988 455 15.7

1989 381 10.7 11.3 52.9 64.2

1990 247 11.0 11.0 58.5 69.5

1991 184 7.9 8.5 56.0 64.5

1992 209 6.3 4.5 8.7 13.2

* USEPA Office of Pollution Prevention and Toxics Releases

Source: Ayres & Ayres, 167.



product of chlor-alkali processing) has appeared as a significant contaminant; however, this

would only account for about 4.3 tonnes of missing mercury in the US (Ayres & Ayres, 168).



The most likely explanation for the missing mercury revolves around EPA mandated disposal

techniques. In 1992, the EPA banned the disposal of mercury-containing sludge produced at

chlor-alkali factories. In addition, at about this time the TRI was expanded to include reports for

„Source reduction and recycling‟. Thus, in 1992, 40 tonnes of mercury were released while 160

tonnes were recovered on site from chlor-alkali facilities (Ayres & Ayres, 168). This was

equivalent to 2.5 times the amount of mercury consumption reported for that year, suggesting

that the missing mercury had been accumulating in mercury-bearing waste sludges on site at the

chlorine plants (Ayres & Ayres, 168). These accumulations were not reported until 1992 when it

became illegal to continue their storage, prompting the need for recycling and thus reporting.





BIOGEOCHEMICAL FLOWS

Almost every part of the Earth‟s ecosystem contains some mercury. Due to its high vapor

pressure at normal atmospheric temperatures, mercury is constantly emitted from the earth

(although it rarely occurs in toxic concentrations) (Jasinski). Natural sources of significant

mercury emissions to the atmosphere may be classified as follows:



 degassing from natural mineral deposits;

 volcanic emissions;

 photo-reduction of divalent mercury in natural waters;

 biological demethylation of methyl or dimethyl mercury (Ayres & Ayres, 155).



In addition, the following sources serve as minor sources of mercury emissions:



 geothermal sources (submarine volcanoes and faults and fractures in the earth‟s crust)

 seismic activities (such as earthquakes);

 erosion of mercury-bearing soils and rocks;

 evaporation of mercury-containing water;

 volatilization from soil;

 animal excretions;

 forest fires (Ayres & Ayres, 155).



All totaled, these sources account for the annual, global emission of approximately 317.0 kMT of

mercury into the atmosphere (Ayres & Ayres, 13), and are fairly comparable to anthropogenic

emissions. Approximately 2/3 of mercury emissions are thought to be attributable to natural

sources (oceanic and terrestrial), with the remaining 1/3 resulting from anthropogenic activities

(Ayres & Ayres, 155). Atmospheric additions of gaseous mercury have nearly doubled since the

nineteenth century (Ayres & Ayres, 156), with approximately 90 percent of these increases

attributed to anthropogenic activities. Natural water fluxes of mercury to water are not well

known, although a 1977 study estimated an annual, global discharge of mercury into the oceans

(due to natural weathering processes) of 3000 tonnes (Ayres & Ayres, 156).



Natural sources of mercury emissions result in the cycling of mercury through the biosphere,

with the concentration of natural mercury emissions at any one location generally found to be

quite low. However, anthropogenic sources often enhance these natural sources, resulting in

higher than normal localized levels (Jasinski). For example, the flooding of vegetated areas can

release a considerable quantity of soluble methylmercury into the water from the natural stock of

insoluble inorganic mercury (Baird, 361). This methylmercury may then enter the food chain,

resulting in elevated mercury levels in organisms.







Global sour ce s for air bor ne me rcur y.





Other

an th ro poge ni c

source s





Oceans









Worl d fo ssil fu el

co mbustion









Na tural te rrestri al

source s

The ratio of anthropogenic to natural sources of mercury is currently estimated at 6.5, with more

mercury being mined than resides in the topsoil (Ayres & Ayres, 156). In addition, the

mobilization rate of natural sources of mercury emissions into surface waters is very low

compared to anthropogenic sources (Ayres & Ayres, 157). The anthropogenic culprit here is

industrial water emissions. These emissions constitute a relatively small fraction of total

anthropogenic emissions, yet they may have a disproportional impact on biota (Ayres & Ayres,

157).





INTERACTIONS AND RESPONSES

The most significant sources of mercury emissions are industrial atmospheric emissions

(primarily chlor-alkali production), energy production and continental „degassing‟. Sources such

as natural geological processes and emissions from coal combustion and phosphate fertilizers

release significant amounts of mercury into the atmosphere, where it is often transferred to

waterways. Here, the biological transformation of inorganic to organic mercury (CH3Hg+) is

increased with the increased availability of organic matter. In this organic form, mercury is

available for uptake and it bioaccumulates in animal tissues, due to the high rate of mercury

uptake relative to elimination.



Bioaccumulation is more significant in aquatic systems than in terrestrial systems. Once

mercury enters the soil, it is strongly bound in the clays and other particles, resulting in a low

transfer to plants and herbivores. However, when organic mercury is uptaken, the effects may be

significant and irreversible. Detrimental health effects associated with mercury exposure include

the following:



 deterioration of the nervous system (cellular damage);

 impairment of hearing, speech, vision and gait (dulled senses);

 involuntary muscle movements (affects motor skills);

 corrosion of skin and mucous membranes;

 difficulty chewing and swallowing.



Mercury present in fish is passed along to consumers of fish with increasingly greater toxicity, as

mercury is bioconcentrated and longer-lived organisms typically accumulate more.



Mercury does not appear to have any significant interactions with other metals, nor is there any

evidence pointing towards significant interactions between the natural and anthropogenic cycles.

A 1994 EPA report stated that natural sources of mercury emissions registered at approximately

1,000,000 Kg/year for both pre-industrial and current times (EPA). Thus, no increase was noted

in natural mercury fluxes as a result of increased anthropogenic emissions.



Substitutes for mercury are abundant and in strong demand. Public awareness regarding mercury

has increased in recent years due to several factors. One such factor lies in evidence stating that

mercury levels in the atmosphere of the industrial Northern Hemisphere are much higher and

rising than in the non-industrialized Southern Hemisphere (Ayres & Ayres, 152). This has led to

widespread concern regarding anthropogenic sources of mercury emissions, and a move towards

the reduction of mercury in consumer products. For example, mercury-amalgams are currently

being investigated for use in dental fillings. As was previously noted, the extensive use of

mercury in mining gold and silver has been phased out and replaced by the more efficient

cyanide process (Ayres & Ayres, 161). The use of mercury in batteries is being phased out as

well, due to concerns about landfill leakage of mercury into groundwater aquifers. These

batteries are now being replaced by rechargeable nickel-cadmium cell batteries. Lastly, mercury

once heavily used in fluorescent lamps is now being replaced by sodium vapor, which presents a

lesser toxicity hazard and is a more efficient light source.





Recycling of Mercury

Mercury consumption has rapidly declined since the late 1980s, with the most dramatic drop

noted in the case of electronic goods (especially in batteries and anti-fungal paint) (Ayres &

Ayres, 160). However, large quantities of these goods still remain, with primary disposal via

landfills. This is a potentially significant hazard as was previously noted (i.e., leakage if mercury

into ground water). A large number of mercury uses are potentially recyclable, including

industrial catalysts, mercury electrolytic cells (for chlorine production), electrical equipment and

instruments (Ayres & Ayres, 160). Unfortunately, much of the mercury present in these uses is

not recycled, but is instead dissipated into the environment.



Mercury recycling in the US is a relatively small-scale operation, with only five small chemical

companies that routinely process mercury-containing scrap (Ayres & Ayres, 178). Most „scrap‟

recycled includes fluorescent tubes, mercury vapor lamps, batteries, switches, electrical relays

and dental amalgam. However, current technologies do not allow for the recycling of mercurous

wastes from the chemical industry, a major producer. In addition, most mercury in consumer

products cannot be recycled economically, leading to the general discharge in landfills (all from

Ayres & Ayres, 178).



As was previously mentioned, mercury is extremely mobile due to its high vapor pressure and

low affinity for oxygen. Thus, landfill or sediment deposition is not a guarantee of long-term

immobilization. In addition, mercury‟s failure to oxidize rapidly in either the atmosphere or in

water points to the inevitable remobilization from virtually any use or waste. It seems quite

likely that all mercury that has been mined in the past will be, or has been, released into the

environment. This is a serious factor for consideration, as such losses are raising the

environmental background level of mercury.



Sources of mercury could be effectively controlled (or „plugged) via three primary routes:

product substitution, process modification, and materials separation. Product substitution, as was

previously mentioned, has already started to soar via the reduced use of and substitutes for

mercury. Process modification would be used primarily at chlor-alkali plants, removing mercury

with ~100% efficiency. Firms could also enjoy additional savings here as a result of reduced

recycling or disposal needs (~$4,590 per pound of mercury removed cost-effectiveness) (EPA).

Materials separation, the separation of low-volume materials containing high mercury

concentrations, could reduce mercury input to a combuster without removing energy content of

the waste stream (EPA). Such programs have been successfully implemented for household

batteries and at hospitals. All of these techniques will aid in the plugging of environmental leaks

for mercury.

CONCLUSION

Current information available for both natural and anthropogenic mercury cycles is seriously

flawed by a lack of reliable data on emission levels, trade, consumption and industrial uses of

mercury, especially outside of the US (Ayres & Ayres, 179). Estimates of flows for either cycle

vary significantly depending on the source. Thus, the statistical information presented in this

report is an approximation at best. While numerous sources of data exist for anthropogenic

flows of mercury, little to no data is available for natural mercury emissions beyond a composite

measure.



In addition, current measurement methods administered under the EPA‟s TRI fail to account for

large quantities of „missing‟ mercury. The inclusion of all sectors of the economy and a

modification requiring firms to account for all of their inputs and outputs of toxic materials (via a

demonstrated materials balance) would potentially eliminate this problem. It would also be

useful to gather emissions data for a number of source categories, including secondary mercury

production (recycling), commercial and industrial boilers, landfills, electric lamp breakage, and

iron and steel manufacturing (EPA). This would provide better estimates of mercury fluxes and

disposal techniques. Lastly, an accurate determination of the mercury flux from natural sources

would aid in determining the impact of US anthropogenic sources on the global mercury cycle,

as well as the impact of all mercury emissions in the US (EPA).



Anthropogenic activities have been identified as a significant source of mercury leaks to the

environment. These leaks may be significantly plugged in the future through government

regulations and innovative ideas for new technologies from the utility industry. Both of these

potential “plugs” have the capability for reducing the negative impacts associated with indefinite

mercury cycling by reducing overall atmospheric emissions. No significant interaction between

natural and anthropogenic mercury cycles was discovered.



The current analysis suggests that anthropogenic sources of mercury emissions are significant

but decreasing. EPA estimates for the future predict a significant decrease in mercury emissions

over the next 10 years as a result of new regulations. An increase in secondary production of

mercury is also expected as more recycling facilities commence operation to recover mercury

form discarded products and wastes. Lastly, mercury used in conjunction with manufacturing is

expected to decline, while chlorine production from mercury cell chlor-alkali plants is expected

to continue to account for most of the mercury use in the manufacturing sector (EPA).

REFERENCES

1) Ayres & Ayres. “Accounting for Resources”, Volumes I & II.



2) Baird, Colin, Environmental Chemistry (New York: W.H. Freeman and Company, 1995).



3) Environmental Protection Agency. “Mercury Study Report to Congress”, Volumes I & II.

Document # 452/R-97-004, 1997. Website: http://nsdi.epa.gov/ttn/uatw/112nmerc/mercury.html



4) Jasinski, Stephen M. “The Materials Flow of Mercury in the U.S.”, Volume 1.

U.S. Bureau of Mines Information Circular #9412, 1989. Website:

http://greenwood.cr.usgs.gov/pub/min-info-pubs/usbm-ic/ic-9412/



5) U.S.G.S. Website: http://minerals.usgs.gov/minerals/pubs/myb.html



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