Table 1-Discharge (Jan-Apr 14)

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					                                                            Table 1 (Revised*--Effective 7/01/03)
                                                              Outfall 003 Discharge Volumes
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex

                Column 1     Column 2A      Column 2B        Column 3       Column 4        Column 5       Column 6        Column 7             Column 8            Column 9

               Well Water                                       Total      Aerated, Lime
               Diluent to     U.S. Filter   Florida Pines   Well Water +   Treated Water     Discharge     Shipments       Shipments            Shipments            Total
              Mixing Tank,   RO Permeate    RO Permeate     RO Permeate,    Discharged,     Measured at        to               to                  to              Offsite
  Date           gallons       gallons         gallons         gallons        gallons        Outfall 003     Tampa         Cargill & CF         Counties (1)      Consumption
 1-Jan-04            0         835,700                        835,700         984,503        1,628,900      159,000           36,599                0               2,015,802
 2-Jan-04            0         384,100                        384,100        1,165,385       1,273,630      166,200           36,629             125,700            1,878,014
 3-Jan-04            0         777,500                        777,500        1,390,415       1,714,400      157,900           73,408              75,000            2,474,223
 4-Jan-04            0         780,600                        780,600        1,443,600       1,803,220      159,000           73,419                0               2,456,619
 5-Jan-04           110        798,800                        798,910        1,381,028       1,947,050      158,000           73,518              75,000            2,486,456
 6-Jan-04            0         810,000                        810,000        1,346,660       2,003,330      162,400           73,514              75,000            2,467,574
 7-Jan-04            0         823,600                        823,600        1,416,240       2,145,740      164,600           36,810              75,000            2,516,250
 8-Jan-04            0         788,700                        788,700        1,567,137       2,303,430      162,800           36,673              75,000            2,630,310
 9-Jan-04            0         738,700                        738,700        1,723,486       2,563,900      149,400           36,592              75,000            2,723,178
10-Jan-04            0         765,900                        765,900        1,389,684       2,152,910      159,000           73,679              75,000            2,463,263
11-Jan-04            0         821,600                        821,600        1,155,743       1,788,240      159,000           73,322                0               2,209,665
12-Jan-04           120        790,200                        790,320         995,211        1,659,930      164,500           36,702             150,000            2,136,733
13-Jan-04            0         811,700                        811,700         915,109        1,445,200      162,400           73,451             150,000            2,112,660
14-Jan-04            0         848,600                        848,600         789,160        1,399,750      156,900           74,016             150,000            2,018,676
15-Jan-04            0         801,200                        801,200        1,011,431       1,672,900      159,000           36,813             150,000            2,158,444
16-Jan-04            0         845,800                        845,800         766,146        1,657,800      159,000           72,846             150,000            1,993,792
17-Jan-04            0         824,500                        824,500         727,573        1,573,250      156,900           73,670             150,000            1,932,643
18-Jan-04            0         850,300                        850,300         762,962        1,661,700      158,900           55,175                0               1,827,337
19-Jan-04            0         756,400                        756,400         576,780        1,432,840      159,000              0               150,000            1,642,180
20-Jan-04            0         828,200                        828,200        1,266,125       2,127,970      159,000              0               150,000            2,403,325
21-Jan-04           130        734,200                        734,330        1,326,463       2,239,180      153,400           36,972             150,000            2,401,165
22-Jan-04            0         681,200                        681,200         949,816        1,662,970      146,000           36,822             150,000            1,963,838
23-Jan-04            0         770,000                        770,000         714,595        1,345,910      151,000           73,453             150,000            1,859,048
24-Jan-04            0         807,600                        807,600         730,012        1,416,300      156,300           73,598             150,000            1,917,510
25-Jan-04            0         812,900                        812,900         648,830        1,303,570      142,900           73,600                0               1,678,230
26-Jan-04            0         796,000                        796,000         660,250        1,242,700      146,100              0               150,000            1,752,350
27-Jan-04            0         802,700                        802,700        1,236,312       2,059,170      146,000              0               150,000            2,335,012
28-Jan-04            0         781,400                        781,400         956,632        1,947,870      146,400           36,813             150,000            2,071,245
29-Jan-04            0         793,000                        793,000         934,475        1,877,190      146,200           73,627             150,000            2,097,302
30-Jan-04            0         824,100                        824,100        1,148,151       2,102,800      145,200           73,335             150,000            2,340,786
31-Jan-04            0         821,200                        821,200        1,472,095       2,484,440      153,600           73,553             150,000            2,670,448
1-Feb-04             0         778,800                        778,800        1,421,120       2,199,920      155,300           73,522                0               2,428,742
2-Feb-04             0         818,300                        818,300         941,330        1,759,030      146,100           36,692             150,000            2,092,422


  Printed On: 11/22/2011                                                     Page 1 of 30                        C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                            Table 1 (Revised*--Effective 7/01/03)
                                                              Outfall 003 Discharge Volumes
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex

                Column 1     Column 2A      Column 2B        Column 3       Column 4        Column 5       Column 6        Column 7             Column 8            Column 9

               Well Water                                       Total      Aerated, Lime
               Diluent to     U.S. Filter   Florida Pines   Well Water +   Treated Water     Discharge     Shipments       Shipments            Shipments            Total
              Mixing Tank,   RO Permeate    RO Permeate     RO Permeate,    Discharged,     Measured at        to               to                  to              Offsite
  Date           gallons       gallons         gallons         gallons        gallons        Outfall 003     Tampa         Cargill & CF         Counties (1)      Consumption
 3-Feb-04           0          827,000                        827,000         839,580        1,667,180      146,000           73,493             150,000            2,036,073
 4-Feb-04          180         786,100                        786,280        1,147,720       1,933,820      145,800           67,391             150,000            2,297,191
 5-Feb-04           0          824,800                        824,800        1,528,830       2,353,630      145,600           55,055             150,000            2,704,285
 6-Feb-04           0          662,100                        662,100        1,295,493       2,233,390      125,600           73,223             150,000            2,306,416
 7-Feb-04           0          802,300                        802,300        1,661,605       2,769,330      145,400           61,197             150,000            2,820,502
 8-Feb-04           0          803,000                        803,000        1,799,466       2,938,890      166,900           61,317                0               2,830,683
 9-Feb-04           30         763,100                        763,130        1,784,102       2,697,430      145,300           61,162             150,000            2,903,694
10-Feb-04           20         714,000                        714,020        1,196,773       1,964,340      145,700           61,126             150,000            2,267,619
11-Feb-04           20         764,000                        764,020         720,200        1,422,010      145,800              0               150,000            1,780,020
12-Feb-04           20         743,300                        743,320         704,751        1,303,380      145,700           18,420             150,000            1,762,191
13-Feb-04           0          832,900                        832,900        1,095,630       1,738,180      148,600           30,032             150,000            2,257,162
14-Feb-04           0          831,300                        831,300        1,192,640       1,818,270      149,100           54,969             150,000            2,378,009
15-Feb-04           0          831,600                        831,600        1,372,740       2,204,340      144,800           30,937                0               2,380,077
16-Feb-04           30         793,200                        793,230        1,535,060       2,624,010      145,100              0               150,000            2,623,390
17-Feb-04           10         819,700            0           819,700        1,549,920       2,369,620      103,700           61,585             150,000            2,684,905
18-Feb-04           20         828,500            0           828,500         757,050        1,585,550      145,200           18,456             150,000            1,899,206
19-Feb-04           20         621,500        187,682         809,182         724,978        1,534,160      145,200              0               175,000            1,854,360
20-Feb-04           0          785,500         53,000         838,500         679,760        1,518,260      145,200           36,828              75,000            1,775,288
21-Feb-04         17,150       761,200         30,876         792,076         363,774        1,155,850      116,000           49,195              75,000            1,396,045
22-Feb-04           0          815,700            0           815,700         584,410        1,400,110      107,600           61,935                0               1,569,645
23-Feb-04           10         744,000        206,980         950,980         465,320        1,416,300      145,200           61,007              75,000            1,697,507
24-Feb-04           0          821,400        387,374        1,208,774       1,111,826       2,320,600      145,300           61,220              75,000            2,602,120
25-Feb-04           0          809,800        289,227        1,099,027       1,434,673       2,533,800      141,000           38,504              75,000            2,788,204
26-Feb-04           0          762,700        366,868        1,129,568       1,589,632       2,719,200      140,100           35,656              75,000            2,969,956
27-Feb-04           0          804,000        322,178        1,126,178       1,408,122       2,534,300      145,090           73,269              75,000            2,827,659
28-Feb-04           0          833,200          7,166         840,366        1,081,434       1,921,800      73,200            54,349              75,000            2,124,349
29-Feb-04           0          836,500        315,584        1,152,084        927,316        2,079,400      97,600            43,254                0               2,220,254
 1-Mar-04           0          803,300        366,443        1,169,743        986,057        2,155,800      144,900          268,654              75,000            2,644,354
 2-Mar-04           0          832,300         88,530         920,830        1,248,070       2,241,900      116,100          243,948              75,000            2,603,948
 3-Mar-04           0          717,800         30,289         748,089         889,711        1,637,800      150,200          360,053              75,000            2,223,053
 4-Mar-04           0          781,200        388,675        1,169,875       1,475,025       2,663,900      145,200          329,908              75,000            3,195,008
 5-Mar-04           0          671,500        320,407         991,907        1,157,393       2,189,300      145,400          316,007             175,000            2,785,707
 6-Mar-04           0          756,600        423,033        1,179,633       1,495,267       2,674,900      117,400          289,461             175,000            3,256,761


  Printed On: 11/22/2011                                                     Page 2 of 30                        C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                            Table 1 (Revised*--Effective 7/01/03)
                                                              Outfall 003 Discharge Volumes
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex

                Column 1     Column 2A      Column 2B        Column 3       Column 4        Column 5       Column 6        Column 7             Column 8            Column 9

               Well Water                                       Total      Aerated, Lime
               Diluent to     U.S. Filter   Florida Pines   Well Water +   Treated Water     Discharge     Shipments       Shipments            Shipments            Total
              Mixing Tank,   RO Permeate    RO Permeate     RO Permeate,    Discharged,     Measured at        to               to                  to              Offsite
  Date           gallons       gallons         gallons         gallons        gallons        Outfall 003     Tampa         Cargill & CF         Counties (1)      Consumption
 7-Mar-04           0          815,400        479,094        1,294,494       1,201,306       2,495,800      73,000           269,341                0               2,838,141
 8-Mar-04           0          783,200        101,932         885,132        1,499,368       2,412,500      145,400          236,195             175,000            2,941,095
 9-Mar-04           0          808,700        371,686        1,180,386       1,114,414       2,294,800      125,500          306,461             175,000            2,901,761
10-Mar-04           0          761,000        228,274         989,274         922,926        1,912,100      153,200          335,358             175,000            2,575,758
11-Mar-04           0          676,200        249,131         925,331         817,069        1,742,400      158,400          359,798             175,000            2,435,598
12-Mar-04           0          757,600        367,811        1,125,411        826,989        1,952,400      146,900          298,941             175,000            2,573,241
13-Mar-04           0          795,800        358,775        1,154,575       1,204,525       2,359,100      118,200          255,150             175,000            2,907,450
14-Mar-04           0          818,300        365,033        1,183,333       1,120,067       2,303,400      87,600           271,125                0               2,662,125
15-Mar-04           0          811,800        401,236        1,213,036        884,964        2,098,000      145,200          308,118             175,000            2,726,318
16-Mar-04           0          823,800        405,038        1,228,838       1,034,562       2,263,400      145,200          345,383             175,000            2,928,983
17-Mar-04           0          822,300        412,281        1,234,581       1,164,519       2,399,100      145,200          394,072             175,000            3,113,372
18-Mar-04           0          738,800        417,729        1,156,529       1,179,071       2,335,600      145,200          405,068             175,000            3,060,868
19-Mar-04           0          276,800        406,817         683,617        1,180,783       1,864,400      145,200          337,997             175,000            2,522,597
20-Mar-04           0          300,500        372,030         672,530        1,260,670       1,933,200      93,800           214,084             175,000            2,416,084
21-Mar-04           0          790,700        180,789         971,489        1,146,511       2,118,000      97,200           145,933                0               2,361,133
22-Mar-04           0          789,500        198,917         988,417        1,359,983       2,348,400      135,600          224,631             175,000            2,883,631
23-Mar-04           0          737,000        394,143        1,131,143       1,160,957       2,292,100      145,200          292,033             175,000            2,904,333
24-Mar-04           0          783,700        400,730        1,184,430       1,012,670       2,197,100      145,200          311,940             175,000            2,829,240
25-Mar-04           0          821,500        405,311        1,226,811       1,116,789       2,343,600      145,100          283,951             175,000            2,947,651
26-Mar-04           0          778,100        400,741        1,178,841        304,859        1,483,700      141,900          253,512             175,000            2,054,112
27-Mar-04           0          814,500        383,001        1,197,501        961,999        2,159,500      77,000           196,756             175,000            2,608,256
28-Mar-04           0          813,000        107,496         920,496        1,091,104       2,011,600      66,400            86,294                0               2,164,294
29-Mar-04           0          765,700        329,226        1,094,926        956,874        2,051,800      98,700           176,749             175,000            2,502,249
30-Mar-04           0          711,900        428,770        1,140,670       1,235,430       2,376,100      54,400            48,740             175,000            2,654,240
31-Mar-04           0          688,400        418,355        1,106,755       1,072,945       2,179,700      47,800            24,245             175,000            2,426,745
 1-Apr-04           0          753,500        413,670        1,167,170        280,730        1,447,900      48,000               0               175,000            1,670,900
 2-Apr-04           0          769,500        411,611        1,181,111        199,889        1,381,000      48,000            42,423             175,000            1,646,423
 3-Apr-04           0          737,800        399,122        1,136,922        533,178        1,670,100         0              36,200             175,000            1,881,300
 4-Apr-04         10,060       768,700        401,874        1,170,574         15,226        1,185,800         0                 0                  0               1,185,800
 5-Apr-04         12,950       623,000        315,667         938,667         566,433        1,505,100      48,000            30,480             175,000            1,758,580
 6-Apr-04         13,010       717,700        405,797        1,123,497        802,803        1,926,300      48,000            18,282             175,000            2,167,582
 7-Apr-04         12,900       676,200        433,525        1,109,725        586,475        1,696,200      47,800            12,206             175,000            1,931,206
 8-Apr-04         13,000       698,900        440,571        1,139,471        563,429        1,702,900      48,000            36,454             175,000            1,962,354


  Printed On: 11/22/2011                                                     Page 3 of 30                        C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                              Table 1 (Revised*--Effective 7/01/03)
                                                                Outfall 003 Discharge Volumes
                                                                 Emergency Order No. 02-1054
                                                               Piney Point Phosphates Complex

                 Column 1     Column 2A       Column 2B        Column 3       Column 4        Column 5       Column 6        Column 7             Column 8            Column 9

                Well Water                                        Total      Aerated, Lime
                Diluent to     U.S. Filter    Florida Pines   Well Water +   Treated Water     Discharge     Shipments       Shipments            Shipments            Total
               Mixing Tank,   RO Permeate     RO Permeate     RO Permeate,    Discharged,     Measured at        to               to                  to              Offsite
    Date          gallons       gallons          gallons         gallons        gallons        Outfall 003     Tampa         Cargill & CF         Counties (1)      Consumption
  9-Apr-04         13,100       768,000         439,240        1,207,240        454,360        1,661,600      24,500               0               100,000            1,786,100
 10-Apr-04           0          737,800         246,650         984,450         613,750        1,598,200        0                  0               100,000            1,698,200
 11-Apr-04           0          763,200            0            763,200         541,700        1,304,900        0                  0                  0               1,304,900
 12-Apr-04           0          566,900            0            566,900         864,200        1,431,100      24,500            73,452             100,000            1,629,052
 13-Apr-04           0          604,700            0            604,700         968,200        1,572,900      24,500               0                  0               1,597,400
 14-Apr-04           0          743,300            0            743,300        1,014,200       1,757,500      24,500               0               100,000            1,882,000

Total              92,890      80,102,000     16,276,385       96,379,045    108,554,714      203,687,190    13,010,690      11,391,806          12,325,700          241,661,955

Notes:         TBR = Data not yet available.
            * Revised as of 04/01/03 Third Modification.
           (1)
               Shipments to Manatee County.




   Printed On: 11/22/2011                                                      Page 4 of 30                        C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                   Table 1 (Revised*--Effective 7/01/03)
                                     Outfall 003 Discharge Volumes
                                      Emergency Order No. 02-1054
                                    Piney Point Phosphates Complex

                     Column 1       Column 2       Column 3         Column 4            Column 5             Column 6

                     Well Water                       Total        Aerated, Lime
                     Diluent to     U.S. Filter   Well Water +     Treated Water        Discharge             Total
                    Mixing Tank,   RO Permeate    RO Permeate,      Discharged,        Measured at           Offsite
        Date           gallons       gallons         gallons          gallons           Outfall 003        Consumption
    15-Apr-04               0        775,600        775,600          1,136,000           1,911,600           1,911,600
    16-Apr-04               0        797,400        797,400           768,500            1,565,900           1,565,900
    17-Apr-04               0        790,100        790,100           821,200            1,611,300           1,611,300
    18-Apr-04               0        670,900        670,900          1,027,300           1,698,200           1,698,200
    19-Apr-04               0        781,300        793,861           972,939            1,766,800           1,766,800
    20-Apr-04               0        704,100       1,101,247          708,453            1,809,700           1,809,700
    21-Apr-04             500        794,700       1,237,803          774,597            2,012,400           2,012,400
    22-Apr-04               0        784,100       1,238,024          834,976            2,073,000           2,073,000
    23-Apr-04               0        748,900       1,292,274          829,226            2,121,500           2,121,500
    24-Apr-04               0        725,200       1,238,352          814,428            2,052,800           2,052,780
    25-Apr-04               0        740,600        999,102          1,104,798           2,103,900           2,103,900
    26-Apr-04               0        717,200        952,180          1,143,820           2,096,000           2,096,000
    27-Apr-04               0        646,500       1,153,053         1,115,047           2,268,100           2,268,100
    28-Apr-04               0        673,100       1,214,962         1,187,838           2,402,800           2,402,800
    29-Apr-04               0        756,300       1,220,451          909,649            2,130,100           2,130,100
    30-Apr-04               0        796,000       1,228,727          365,873            1,594,600           1,594,600
    1-May-04                0        810,000       1,234,257          338,143            1,572,400           1,572,400
    2-May-04                0        763,800       1,188,911          346,689            1,535,600           1,535,600
    3-May-04                0        759,300        784,998           361,502            1,146,500           1,146,500
    4-May-04                0        755,800        944,937           370,563            1,315,500           1,315,500
    5-May-04                0        728,300       1,169,458          423,842            1,593,300           1,593,300
    6-May-04                0        686,800       1,095,690          451,810            1,547,500           1,547,500
    7-May-04                0        569,900        849,370           461,630            1,311,000           1,311,000
    8-May-04                0        449,600        744,937           491,363            1,236,300           1,236,300
    9-May-04                0        515,800        515,800           490,000            1,005,800           1,005,800
    10-May-04               0        636,900        636,900           395,000            1,031,900           1,031,900
    11-May-04               0        675,000        793,261           403,439            1,223,700           1,196,700
    12-May-04               0        449,300        903,300           515,800            1,419,100           1,419,100
    13-May-04               0        590,600       1,023,979          415,321            1,439,300           1,439,300
    14-May-04               0        728,600        728,600           546,700            1,275,300           1,275,300
    15-May-04               0        733,200        733,200           384,400            1,179,600           1,117,600
    16-May-04               0        740,300        968,038           509,062            1,477,100           1,477,100
    17-May-04               0        676,700       1,095,741          554,359            1,650,100           1,650,100
    18-May-04               0        624,600       1,298,191          512,809            1,811,000           1,811,000
    19-May-04               0         78,700        405,422           578,178             983,600             983,600
    20-May-04               0        154,300        519,217           605,483            1,124,700           1,124,700
    21-May-04               0            0          768,040           653,960            1,422,000           1,422,000
    22-May-04               0            0          590,433           683,367            1,273,800           1,273,800
    23-May-04               0            0          579,028           643,672            1,222,700           1,222,700
    24-May-04               0            0          111,087           508,113             619,200             619,200
    25-May-04             230        213,800        563,768           349,732             913,500             913,500
    26-May-04             810        272,100        690,171           210,629             900,800             900,800
    27-May-04            27,910      237,900        695,837           495,763            1,191,600           1,191,600
    28-May-04             340         33,100        532,331           460,869             993,200             993,200
    29-May-04               0        321,600        756,215           432,685            1,188,900           1,188,900
    30-May-04               0        352,700        784,245           478,755            1,263,000           1,263,000

Printed On: 11/22/2011                              Page 5 of 30   C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                   Table 1 (Revised*--Effective 7/01/03)
                                     Outfall 003 Discharge Volumes
                                      Emergency Order No. 02-1054
                                    Piney Point Phosphates Complex

                     Column 1       Column 2       Column 3         Column 4            Column 5             Column 6

                     Well Water                       Total        Aerated, Lime
                     Diluent to     U.S. Filter   Well Water +     Treated Water        Discharge             Total
                    Mixing Tank,   RO Permeate    RO Permeate,      Discharged,        Measured at           Offsite
        Date           gallons       gallons         gallons          gallons           Outfall 003        Consumption
    31-May-04             0          354,500        716,583          535,817             1,252,400           1,252,400
     1-Jun-04             0          355,700        600,307          624,493             1,224,500           1,224,800
     2-Jun-04             0          345,100        745,200          673,400             1,418,600           1,418,600
     3-Jun-04             0          233,900        648,333          427,567             1,075,900           1,075,900
     4-Jun-04             0          365,000        936,386          414,314             1,350,700           1,350,700
     5-Jun-04             0          445,800       1,093,218         493,982             1,587,200           1,587,200
     6-Jun-04             0          136,200        660,846          605,354             1,266,200           1,266,200
     7-Jun-04             0             0            14,528          797,672              812,200             812,200
     8-Jun-04             0             0           638,573          443,478             2,615,800           1,082,051
     9-Jun-04             0          153,200        876,409          533,296             1,535,900           1,409,705
    10-Jun-04             0          360,200        912,197          532,223             2,013,000           1,444,420
    11-Jun-04             0          249,100        486,680          535,053             1,557,000           1,021,733
    12-Jun-04             0             0           513,839          529,557             1,415,200           1,043,396
    13-Jun-04             0             0           225,621          289,680              670,800             515,301
    14-Jun-04            290           900          245,564          380,225              506,300             625,789
    15-Jun-04             0          299,000        617,208          416,550             1,677,800           1,033,758
    16-Jun-04             0          336,500        791,807          463,820             1,736,400           1,255,627
    17-Jun-04             0          379,700        860,574          453,920             2,168,000           1,314,494
    18-Jun-04             0          563,400       1,120,343         539,537             1,659,880           1,659,880
    19-Jun-04             0          496,300       1,055,549         519,678             1,575,227           1,575,227
    20-Jun-04             0          683,700        849,767          558,339             1,408,106           1,408,106
    21-Jun-04             0          650,600       1,167,246         524,503             1,691,749           1,691,749
    22-Jun-04             0          398,000        987,128          491,218             1,478,346           1,478,346
    23-Jun-04             0          561,600       1,225,927         510,109             1,736,036           1,736,036
    24-Jun-04             0          524,400       1,295,440         489,797             1,785,237           1,785,237
    25-Jun-04             0          578,300       1,151,866         522,342             1,674,208           1,674,208
    26-Jun-04             0          599,000       1,077,551         421,093             1,498,644           1,498,644
    27-Jun-04             0          630,400       1,162,959         536,191             1,699,150           1,699,150
    28-Jun-04             0          593,500       1,260,246         513,533             1,773,779           1,773,779
    29-Jun-04             0          501,000       1,086,604         512,302             1,598,906           1,598,906
    30-Jun-04             0          645,600       1,149,255         511,153             1,660,408           1,660,408
     1-Jul-04             0          539,300        539,300          526,627             1,065,927           1,065,927
     2-Jul-04             0          623,100        623,100          510,992             1,134,092           1,134,092
     3-Jul-04             0          577,300        577,300          530,227             1,107,527           1,107,527
     4-Jul-04             0          595,100        595,100          462,449             1,057,549           1,057,549
     5-Jul-04             0          429,300        429,300          376,810              806,110             806,110
     6-Jul-04             0          530,500        530,500          452,930              983,430             983,430
     7-Jul-04             0          165,400        165,400          505,330              670,730             670,730
     8-Jul-04             0          406,500        406,500          537,050              943,550             943,550
     9-Jul-04             0           1,200           1,200          551,732              552,932             552,932
     10-Jul-04            0          170,600        170,600          487,905              658,505             658,505
     11-Jul-04            0          380,100        380,100          529,491              909,591             909,591
     12-Jul-04            0          392,300        392,300          504,691              896,991             896,991
     13-Jul-04            0          384,700        384,700          517,325              902,025             902,025
     14-Jul-04            0          203,200        203,200          528,041              731,241             731,241
     15-Jul-04            0          173,800        173,800          526,989              700,789             700,789

Printed On: 11/22/2011                              Page 6 of 30   C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                   Table 1 (Revised*--Effective 7/01/03)
                                     Outfall 003 Discharge Volumes
                                      Emergency Order No. 02-1054
                                    Piney Point Phosphates Complex

                     Column 1        Column 2        Column 3         Column 4            Column 5             Column 6

                     Well Water                        Total         Aerated, Lime
                     Diluent to      U.S. Filter   Well Water +      Treated Water        Discharge             Total
                    Mixing Tank,    RO Permeate    RO Permeate,       Discharged,        Measured at           Offsite
        Date           gallons        gallons         gallons           gallons           Outfall 003        Consumption
     16-Jul-04             0          462,700         462,700          528,905              991,605             991,605
     17-Jul-04             0          457,900         457,900          528,343              986,243             986,243
     18-Jul-04             0          447,900         447,900          522,803              970,703             970,703
     19-Jul-04             0          487,900         487,900          545,630             1,033,530           1,033,530
     20-Jul-04             0          490,800         490,800          605,385             1,096,185           1,096,185
     21-Jul-04             0          492,600         492,600          478,680              971,280             971,280
     22-Jul-04             0          510,900         510,900          484,411              995,311             995,311
     23-Jul-04             0          525,100         525,100          504,353             1,029,453           1,029,453
     24-Jul-04             0          520,800         520,800          530,621             1,051,421           1,051,421
     25-Jul-04             0          446,600         446,600          544,475              991,075             991,075
     26-Jul-04             0          402,000         402,000          499,274              901,274             901,274
     27-Jul-04             0          228,000         228,000          419,077              647,077             647,077
     28-Jul-04             0          509,100         509,100          515,519             1,024,619           1,024,619
     29-Jul-04             0          455,700         455,700          528,050              983,750             983,750
     30-Jul-04             0          514,700         514,700          536,725             1,051,425           1,051,425
     31-Jul-04             0          519,000         519,000          482,597             1,001,597           1,001,597

   Total                 30,080      49,945,400      79,627,252       60,191,915         145,057,813          139,819,167

   Notes:            TBR = Data not yet available.
                  * Revised as of 04/01/03 Third Modification.
                 (1)
                     Shipments to Manatee County.




Printed On: 11/22/2011                                Page 7 of 30   C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                              Table 2
                                        Ammonia Loading
                                   Emergency Order No. 02-1054
                                 Piney Point Phosphates Complex

                                   Measured Flow @   Ammonia @ 003         Total Ammonia
                          Date          003 (1)        (mg/L) (2)              (lb/day)
                    1-Jan-04          1,628,900            18.90                256.89
                    2-Jan-04          1,273,630            13.10                139.22
                    3-Jan-04          1,714,400            19.90                284.68
                    4-Jan-04          1,803,220            16.70                251.28
                    5-Jan-04          1,947,050            16.30                264.82
                    6-Jan-04          2,003,330            14.50                242.39
                    7-Jan-04          2,145,740            18.10                324.08
                    8-Jan-04          2,303,430            11.10                213.35
                    9-Jan-04          2,563,900            13.90                297.38
                    10-Jan-04         2,152,910            20.90                375.46
                    11-Jan-04         1,788,240            22.80                340.22
                    12-Jan-04         1,659,930            19.00                263.17
                    13-Jan-04         1,445,200            21.20                255.66
                    14-Jan-04         1,399,750            25.30                295.50
                    15-Jan-04         1,672,900             0.00                  0.00
                    16-Jan-04         1,657,800            25.70                355.52
                    17-Jan-04         1,573,250            26.10                342.63
                    18-Jan-04         1,661,700            20.40                282.86
                    19-Jan-04         1,432,840            13.60                162.60
                    20-Jan-04         2,127,970            12.60                223.73
                    21-Jan-04         2,239,180             8.69                162.37
                    22-Jan-04         1,662,970            14.20                197.05
                    23-Jan-04         1,345,910            20.70                232.48
                    24-Jan-04         1,416,300            17.20                203.27
                    25-Jan-04         1,303,570            22.50                244.74
                    26-Jan-04         1,242,700            16.10                166.95
                    27-Jan-04         2,059,170            11.00                189.01
                    28-Jan-04         1,947,870             8.05                130.84
                    29-Jan-04         1,877,190             5.89                 92.26
                    30-Jan-04         2,102,800            11.20                196.52
                    31-Jan-04         2,484,440            15.40                319.26
                    1-Feb-04          2,199,920            22.00                403.85
                    2-Feb-04          1,759,030            19.40                284.75
                    3-Feb-04          1,667,180            11.50                159.98
                    4-Feb-04          1,933,820             8.82                142.32
                    5-Feb-04          2,353,630             8.68                170.47
                    6-Feb-04          2,233,390             6.58                122.63
                    7-Feb-04          2,769,330             5.95                137.49
                    8-Feb-04          2,938,890             4.97                121.88
                    9-Feb-04          2,697,430            10.90                245.34
                    10-Feb-04         1,964,340            21.00                344.21
                    11-Feb-04         1,422,010            25.60                303.76
                    12-Feb-04         1,303,380            14.70                159.88
                    13-Feb-04         1,738,180            11.50                166.80
                    14-Feb-04         1,818,270            10.30                156.27
                    15-Feb-04         2,204,340             7.36                135.38
                    16-Feb-04         2,624,010             7.17                156.99
                    17-Feb-04         2,369,620             7.88                155.81
Printed On: 11/22/2011                              of 30
                                             Page 8 C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                              Table 2
                                        Ammonia Loading
                                   Emergency Order No. 02-1054
                                 Piney Point Phosphates Complex

                                   Measured Flow @   Ammonia @ 003         Total Ammonia
                          Date          003 (1)        (mg/L) (2)              (lb/day)
                    18-Feb-04         1,585,550            12.40                164.06
                    19-Feb-04         1,534,160            11.40                145.94
                    20-Feb-04         1,518,260            20.20                255.91
                    21-Feb-04         1,155,850            19.20                185.18
                    22-Feb-04         1,400,110            15.20                177.58
                    23-Feb-04         1,416,300            17.20                203.27
                    24-Feb-04         2,320,600            13.10                253.67
                    25-Feb-04         2,533,800            11.20                236.80
                    26-Feb-04         2,719,200             6.56                148.85
                    27-Feb-04         2,534,300             7.42                156.91
                    28-Feb-04         1,921,800             8.31                133.26
                    29-Feb-04         2,079,400             9.47                164.32
                    1-Mar-04          2,155,800            11.10                199.68
                    2-Mar-04          2,241,900            10.70                200.17
                    3-Mar-04          1,637,800             9.69                132.43
                    4-Mar-04          2,663,900             6.87                152.71
                    5-Mar-04          2,189,300             6.62                120.94
                    6-Mar-04          2,674,900             7.31                163.16
                    7-Mar-04          2,495,800             7.96                165.77
                    8-Mar-04          2,412,500             8.54                171.92
                    9-Mar-04          2,294,800             6.98                133.66
                    10-Mar-04         1,912,100             9.88                157.64
                    11-Mar-04         1,742,400            10.60                154.12
                    12-Mar-04         1,952,400             8.48                138.15
                    13-Mar-04         2,359,100             8.81                173.43
                    14-Mar-04         2,303,400             9.96                191.44
                    15-Mar-04         2,098,000            10.80                189.07
                    16-Mar-04         2,263,400             6.97                131.64
                    17-Mar-04         2,399,100            11.30                226.21
                    18-Mar-04         2,335,600             9.46                184.37
                    19-Mar-04         1,864,400            10.50                163.35
                    20-Mar-04         1,933,200            10.20                164.54
                    21-Mar-04         2,118,000             8.70                153.76
                    22-Mar-04         2,348,400             8.57                167.94
                    23-Mar-04         2,292,100             9.13                174.62
                    24-Mar-04         2,197,100             8.60                157.67
                    25-Mar-04         2,343,600             6.28                122.81
                    26-Mar-04         1,483,700             4.64                 57.45
                    27-Mar-04         2,159,500             4.57                 82.35
                    28-Mar-04         2,011,600             3.32                 55.73
                    29-Mar-04         2,051,800             4.52                 77.39
                    30-Mar-04         2,376,100             4.58                 90.81
                    31-Mar-04         2,179,700             6.53                118.77
                    1-Apr-04          1,447,900             9.06                109.46
                    2-Apr-04          1,381,000             4.59                 52.89
                    3-Apr-04          1,670,100             4.71                 65.64
                    4-Apr-04          1,185,800             6.39                 63.23
                    5-Apr-04          1,505,100             2.08                 26.12
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                                              Table 2
                                        Ammonia Loading
                                   Emergency Order No. 02-1054
                                 Piney Point Phosphates Complex

                                   Measured Flow @   Ammonia @ 003         Total Ammonia
                          Date          003 (1)        (mg/L) (2)              (lb/day)
                    6-Apr-04          1,926,300             4.20                 67.51
                    7-Apr-04          1,696,200             5.68                 80.39
                    8-Apr-04          1,702,900             5.93                 84.26
                    9-Apr-04          1,661,600             7.88                109.26
                    10-Apr-04         1,598,200             8.28                110.42
                    11-Apr-04         1,304,900             9.80                106.71
                    12-Apr-04         1,431,100             7.40                 88.37
                    13-Apr-04         1,572,900             6.45                 84.66
                    14-Apr-04         1,757,500             4.37                 64.09
                    15-Apr-04         1,911,600             3.79                 60.45
                    16-Apr-04         1,565,900             3.82                 49.91
                    17-Apr-04         1,611,300             4.30                 57.81
                    18-Apr-04         1,698,200             4.66                 66.03
                    19-Apr-04         1,766,800             4.41                 65.02
                    20-Apr-04         1,809,700             3.80                 57.38
                    21-Apr-04         2,012,400             4.64                 77.92
                    22-Apr-04         2,073,000             5.65                 97.73
                    23-Apr-04         2,121,500             7.94                140.56
                    24-Apr-04         2,052,800             6.27                107.40
                    25-Apr-04         2,103,900             3.75                 65.83
                    26-Apr-04         2,096,000             3.31                 57.89
                    27-Apr-04         2,268,100             5.02                 95.01
                    28-Apr-04         2,402,800             4.73                 94.84
                    29-Apr-04         2,130,100             2.52                 44.79
                    30-Apr-04         1,594,600             1.88                 25.02
                    1-May-04          1,572,400             1.09                 14.30
                    2-May-04          1,535,600             1.54                 19.73
                    3-May-04          1,146,500             0.95                  9.07
                    4-May-04          1,315,500             0.96                 10.50
                    5-May-04          1,593,300             0.73                  9.71
                    6-May-04          1,547,500             0.55                  7.13
                    7-May-04          1,311,000             0.44                  4.82
                    8-May-04          1,236,300             0.46                  4.72
                    9-May-04          1,005,800             0.62                  5.21
                    10-May-04         1,031,900             0.78                  6.68
                    11-May-04         1,223,700             0.58                  5.94
                    12-May-04         1,419,100             0.65                  7.73
                    13-May-04         1,439,300             0.54                  6.45
                    14-May-04         1,275,300             0.21                  2.23
                    15-May-04         1,179,600             0.09                  0.89
                    16-May-04         1,477,100             0.64                  7.89
                    17-May-04         1,650,100             0.60                  8.28
                    18-May-04         1,811,000             0.50                  7.56
                    19-May-04          983,600              0.70                  5.75
                    20-May-04         1,124,700             0.90                  8.45
                    21-May-04         1,422,000             0.90                 10.68
                    22-May-04         1,273,800             1.10                 11.69
                    23-May-04         1,222,700             1.90                 19.39
Printed On: 11/22/2011                              of 30
                                             Page 10C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                              Table 2
                                        Ammonia Loading
                                   Emergency Order No. 02-1054
                                 Piney Point Phosphates Complex

                                   Measured Flow @   Ammonia @ 003         Total Ammonia
                          Date          003 (1)        (mg/L) (2)              (lb/day)
                    24-May-04          619,200              2.20                 11.37
                    25-May-04          913,500              2.10                 16.01
                    26-May-04          900,800              1.60                 12.03
                    27-May-04         1,191,600             2.70                 26.85
                    28-May-04          993,200              6.40                 53.04
                    29-May-04         1,188,900             7.20                 71.43
                    30-May-04         1,263,000             4.40                 46.37
                    31-May-04         1,252,400             3.10                 32.40
                    1-Jun-04          1,224,500             3.16                 32.29
                    2-Jun-04          1,418,600             5.82                 68.89
                    3-Jun-04          1,075,900             4.75                 42.64
                    4-Jun-04          1,350,700             3.95                 44.52
                    5-Jun-04          1,587,200             3.18                 42.12
                    6-Jun-04          1,266,200             1.86                 19.65
                    7-Jun-04           812,200              1.22                  8.27
                    8-Jun-04          2,615,800             1.61                 35.14
                    9-Jun-04          1,535,900             1.25                 16.02
                    10-Jun-04         2,013,000             0.77                 12.92
                    11-Jun-04         1,557,000             1.45                 18.84
                    12-Jun-04         1,415,200             3.29                 38.85
                    13-Jun-04          670,800              5.43                 30.39
                    14-Jun-04          506,300              2.05                  8.66
                    15-Jun-04         1,677,800             2.69                 37.66
                    16-Jun-04         1,736,400             0.68                  9.85
                    17-Jun-04         2,168,000             0.77                 13.93
                    18-Jun-04         1,659,880             0.52                  7.20
                    19-Jun-04         1,575,227             0.72                  9.46
                    20-Jun-04         1,408,106             0.46                  5.40
                    21-Jun-04         1,691,749             1.19                 16.80
                    22-Jun-04         1,478,346             9.16                113.00
                    23-Jun-04         1,736,036             2.83                 41.00
                    24-Jun-04         1,785,237             2.62                 39.03
                    25-Jun-04         1,674,208             2.15                 30.04
                    26-Jun-04         1,498,644             1.31                 16.38
                    27-Jun-04         1,699,150             1.32                 18.72
                    28-Jun-04         1,773,779             0.76                 11.20
                    29-Jun-04         1,598,906             0.45                  6.00
                    30-Jun-04         1,660,408             0.25                  3.46
                    1-Jul-04          1,065,927             0.43                  3.86
                    2-Jul-04          1,134,092             0.63                  5.99
                    3-Jul-04          1,107,527             0.69                  6.34
                    4-Jul-04          1,057,549             0.67                  5.91
                    5-Jul-04           806,110              0.29                  1.95
                    6-Jul-04           983,430              0.32                  2.60
                    7-Jul-04           670,730              1.02                  5.71
                    8-Jul-04           943,550              4.73                 37.24
                    9-Jul-04           552,932              4.61                 21.27
                    10-Jul-04          658,505              7.23                 39.73
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                                             Page 11C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                   Table 2
                                             Ammonia Loading
                                        Emergency Order No. 02-1054
                                      Piney Point Phosphates Complex

                                          Measured Flow @     Ammonia @ 003         Total Ammonia
                             Date              003 (1)          (mg/L) (2)              (lb/day)
                    11-Jul-04                  909,591               3.95                 29.98
                    12-Jul-04                  896,991               1.03                  7.71
                    13-Jul-04                  902,025               0.74                  5.57
                    14-Jul-04                  731,241               1.17                  7.14
                    15-Jul-04                  700,789               8.12                 47.48
                    16-Jul-04                  991,605              10.50                 86.88
                    17-Jul-04                  986,243               6.83                 56.21
                    18-Jul-04                  970,703               5.09                 41.23
                    19-Jul-04                 1,033,530              3.74                 32.25
                    20-Jul-04                 1,096,185              1.01                  9.24
                    21-Jul-04                  971,280               1.36                 11.02
                    22-Jul-04                  995,311               0.58                  4.85
                    23-Jul-04                 1,029,453              0.75                  6.46
                    24-Jul-04                 1,051,421              0.45                  3.96
                    25-Jul-04                  991,075               0.77                  6.35
                    26-Jul-04                  901,274               0.34                  2.52
                    27-Jul-04                  647,077               0.26                  1.42
                    28-Jul-04                 1,024,619              1.01                  8.64
                    29-Jul-04                  983,750               0.92                  7.52
                    30-Jul-04                 1,051,425              0.95                  8.34
                    31-Jul-04                 1,001,597              0.26                  2.15

                    Total:                   348,745,003                                 21,530
                    Average per Day:          1,637,300

                    Notes:
                             mg/L = Milligrams per liter.
                             lb/day = Pounds per day.
                             TBR = To be reported, data not yet available.
                             (1)
                                 From Table 1, Column 5.
                             (2)
                                 From Table 3.




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                                                      Page 12C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                                                                                      Table 3
                                                                                                                       Daily Water Quality Monitoring Results
                                                                                                                            Emergency Order No. 02-1054
                                                                                                                         Piney Point Phosphates Complex

Parameter              Visual Observations                  Temperature (oC)                       Turbidity NTU)                      pH (Standard Units)                Dissolved Oxygen (mg/L)              Specific Conductance (µs/cm)                                Ammonia
Station       X-1      003    BR/41    X-2   AR    X-1    003   BR/41     X-2     AR    X-1    003     BR/41    X-2      AR    X-1     003    BR/41   X-2     AR    X-1     003    BR/41    X-2     AR     X-1     003    BR/41    X-2      AR           X-1        003     BR/41           X-2      AR
   1-Jan-04   DRY      CLR     CLR     CLR   CLR   DRY    18.8   19.0     18.9   18.2   DRY     0.3     0.9      0.9     0.6   DRY     6.73    6.75   6.71   6.47   DRY      7.0    6.9     6.5     5.8   DRY     4,575 4,642 4,638 4,645                DRY       18.90    15.80          15.90   16.60
   2-Jan-04   DRY      CLR     CLR     CLR   CLR   DRY    18.8   18.9     19.0   19.0   DRY     0.5     0.6      0.8     0.6   DRY     6.66    6.74   6.72   6.50   DRY      7.1    6.7     5.8     5.6   DRY     4,944 4,817 4,644 4,558                DRY       13.10    14.40          13.50   12.50
   3-Jan-04   DRY      N/A     N/A     N/A   N/A   DRY    19.1   18.8     18.0   18.8   DRY     1.3     1.3      1.3     1.4   DRY     6.76    6.77   6.85   6.61   DRY      6.6    6.4     6.6     4.6   DRY     5,070 4,956 4,986 5,330                DRY       19.90    16.70          16.60   17.50
   4-Jan-04   DRY      N/A     N/A     N/A   N/A   DRY    20.6   20.3     20.6   20.4   DRY     1.2     1.3      1.3     1.2   DRY     6.61    6.74   6.70   6.55   DRY      6.5    6.1     5.7     3.9   DRY     4,966 4,843 4,866 4,753                DRY       16.70    17.60          17.70   16.10
   5-Jan-04   DRY      N/A     N/A     N/A   N/A   DRY    20.7   20.7     20.8   20.1   DRY     1.2     1.3      1.2     1.4   DRY     6.52    6.48   6.38   6.29   DRY      6.1    5.7     5.6     3.8   DRY     4,885 4,784 4,777 4,721                DRY       16.30    16.30          16.30   16.20
   6-Jan-04   DRY      CLR     CLR     CLR   CLR   DRY    19.5   19.7     20.0   19.9   DRY     1.9     1.0      0.8     0.8   DRY     6.58    6.58   6.48   6.33   DRY      6.6    6.4     5.9     5.4   DRY     4,977 4,692 4,698 4,566                DRY       14.50    16.30          16.10   13.50
   7-Jan-04   DRY      CLR     CLR     CLR   CLR   DRY    16.6   16.1     16.6   16.6   DRY     0.9     0.9      1.4     1.0   DRY     6.43    6.58   6.54   6.31   DRY      7.8    6.9     6.2     6.6   DRY     4,783 4,700 4,716 4,408                DRY       18.10    14.40          14.80   15.30
   8-Jan-04   DRY      CLR     CLR     CLR   CLR   DRY    12.6   12.7     12.7   13.1   DRY     1.1     0.8      0.9     1.1   DRY     6.55    6.62   6.65   6.46   DRY      8.2    8.1     8.0     6.8   DRY     4,738 4,670 4,677 4,626                DRY       11.10    12.10          11.90   11.20
   9-Jan-04   DRY      N/A     N/A     N/A   N/A   DRY    13.6   14.5     13.8   14.2   DRY     1.2     1.3      1.3     1.4   DRY     6.64    6.61   6.69   6.89   DRY      8.6    7.8     7.8     7.2   DRY     5,120 4,865 4,910 4,947                DRY       13.90    19.20          18.90   18.90
 10-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY    16.2   17.3     17.1   16.2   DRY     1.0     1.0      0.0     1.2   DRY     6.70    6.86   6.59   6.45   DRY      6.9    7.6     6.6     4.9   DRY     5,280 4,911 5,120 5,140                DRY       20.90    23.40          24.70   23.90
 11-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY     9.7   10.4     11.4   10.5   DRY     0.9     1.1      1.2     1.4   DRY     6.59    6.64   6.63   6.53   DRY      9.4    8.5     7.8     6.4   DRY     4,732 4,751 4,710 4,710                DRY       22.80    19.40          18.90   19.10
 12-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY    12.4   11.9      0.0   12.0   DRY     1.4     1.1      1.0     1.2   DRY     6.70    6.59   6.60   6.42   DRY      9.2    8.1     7.5     5.9   DRY     4,563 4,561 4,510 4,484                DRY       19.00    17.80          17.60   16.80
 13-Jan-04    DRY      CLR     CLR     CLR   CLR   DRY    13.4   13.4     13.6   13.7   DRY     0.3     0.9      0.8     1.2   DRY     6.53    6.55   6.49   6.41   DRY      8.2    7.4     7.1     6.5   DRY     4,757 4,515 4,508 4,355                DRY       21.20    25.30          25.30   21.30
 14-Jan-04    DRY      CLR     CLR     CLR   CLR   DRY    13.9   13.5     13.6   13.7   DRY     1.0     0.6      1.6     0.5   DRY     6.64    6.61   6.50   6.37   DRY      8.1    8.1     7.3     7.2   DRY     4,343 4,284 4,276 4,219                DRY       25.30    33.90          32.70   28.20
 15-Jan-04    DRY      CLR     CLR     CLR   CLR   DRY    14.4   14.4     14.9   14.7   DRY     0.3     0.5      0.8     0.7   DRY     6.54    6.71   6.65   6.39   DRY      8.3    8.0     6.9     6.4   DRY     4,606 4,201 4,333 4,316                DRY        0.00    36.70          37.70   35.90
 16-Jan-04    DRY      CLR     CLR     CLR   CLR   DRY    16.6   16.1     16.2   15.9   DRY     0.5     0.8      0.9     0.7   DRY     6.69    6.80   6.74   6.50   DRY      7.7    6.7     6.9     6.0   DRY     4,338 4,477 3,935 4,285                DRY       25.70    36.10          31.00   34.70
 17-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY    14.4   14.9     15.0   14.9   DRY     1.0     1.3      1.3     1.2   DRY     6.72    6.55   6.56   6.44   DRY      8.0    7.0     7.1     4.6   DRY     3,941 4,075 4,104 3,913                DRY       26.10    23.20          22.80   23.10
 18-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY    17.7   18.0     17.8   17.3   DRY     1.2     1.0      1.0     1.3   DRY     6.64    6.54   6.56   6.51   DRY      7.2    5.9     5.4     4.3   DRY     3,817 3,910 3,917 3,898                DRY       20.40    18.20          17.70   18.30
 19-Jan-04    CLR      CLR     CLR     CLR   CLR   16.6   19.4   18.4     18.2   18.2    5.2    0.4     1.2      1.8     2.1   7.07    7.13    6.88   6.80   6.72   7.5      7.6    6.8     6.7     5.7   1,571    149     1,706 3,160 3,486             4.93      13.60     5.45          10.40   11.80
 20-Jan-04    N/A      N/A     N/A     N/A   N/A   12.8   17.8   15.8     15.8   15.5    4.3    1.2     1.4      1.3     1.0   7.21    6.83    6.65   6.64   6.63   7.7      8.0    7.1     6.7     4.3   1,574    579     3,553 3,555 3,823             8.26      12.60     9.88           9.81   11.20
 21-Jan-04    CLR      CLR     CLR     CLR   CLR   10.9   13.2   12.9     13.2   14.3    5.9    1.5     0.8      0.8     1.1   7.35    7.21    7.05   6.93   6.68   8.4      8.4    8.0     8.3     6.9   1,627 4,467 4,245 4,226 4,255                  11.7       8.69     9.21           9.07    8.32
 22-Jan-04    CLR      CLR     CLR     CLR   CLR   11.6   13.2   14.0     14.5   14.7    4.9    0.4     0.8      1.1     1.3   7.36    6.83    6.74   6.70   6.56   8.6      8.2    7.9     7.3     6.9   1,589 4,707 4,596 4,565 4,541                  15.3      14.20    15.70          15.20   13.10
 23-Jan-04    CLR      CLR     CLR     CLR   CLR   11.7   14.5   14.3     14.9   14.7    4.3    1.2     0.7      1.3     1.2   7.43    6.69    6.64   6.60   6.52   8.6      8.3    7.9     7.7     6.5   1,706 4,273 4,157 4,146 4,238                  20.8      20.70    17.70          16.80   16.70
 24-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY    12.7   13.1     13.0   13.3   DRY     1.0     1.2      1.2     1.1   DRY     6.50    6.46   6.46   6.63   DRY      8.3    8.6     8.2     6.9   DRY     4,281 4,160 4,194 3,985                DRY       17.20    16.80          16.90   15.70
 25-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY    15.1   14.8     14.6   13.7   DRY     1.2     1.3      1.3     1.2   DRY     6.41    6.41   6.39   6.14   DRY      9.0    8.1     7.9     5.9   DRY     4,432 4,106 4,115 4,055                DRY       22.50    28.20          28.60   26.00
 26-Jan-04    DRY      N/A     N/A     N/A   N/A   DRY    18.4   18.3     18.4   17.1   DRY     1.0     1.2      1.2     1.3   DRY     6.51    6.51   6.49   6.22   DRY      7.8    6.0     6.5     5.6   DRY      130      734    771    4,356          DRY       16.10     2.93           2.91   20.80
 27-Jan-04    CLR      CLR     CLR     CLR   CLR   19.1   19.9   20.0     20.0   20.3   22.6   10.6     6.4      4.7     1.6   6.97    6.70    6.67   6.45   6.35   6.1      6.1    5.7     5.4     4.6    793    5,160 3,602 3,695 3,538                10.4      11.00    10.80          11.70   12.20
 28-Jan-04    CLR      CLR     CLR     CLR   CLR   14.2   16.8   16.0     16.3   17.0    3.2    2.1     2.1      1.9     1.6   6.95    6.77    6.72   6.68   6.62   7.7      7.2    6.7     7.4     6.6   1,306 4,330 4,165 3,335 2,718                  6.07       8.05     6.89           6.17    6.49
 29-Jan-04    CLR      CLR     CLR     CLR   CLR   16.3   14.5   14.4     14.7   14.8    3.1    0.9     1.0      1.0     1.3   6.67    6.71    6.81   6.76   6.60   8.3      8.0    7.1     7.1     5.2   1,540 2,918 2,502 2,535 2,707                  9.35       5.89     6.93           6.32    5.18
 30-Jan-04    N/A      N/A     N/A     N/A   N/A   13.7   14.9    0.0      0.0   14.9    3.1    1.0     1.2      1.2     1.5   6.77    6.82    6.70   6.74   6.64   7.1      8.4    7.3     7.7     6.2   1,657 4,424 4,037 4,055 3,987                   13       11.20    12.20          12.20   10.20
 31-Jan-04    N/A      N/A     N/A     N/A   N/A   14.5   15.9   15.9     15.6   16.2    4.2    1.0     1.3      1.3     1.5   6.87    6.91    6.85   6.83   6.78   7.2      7.7    7.1     6.9     5.7   1,489 4,433 4,295 4,320 4,025                  13.8      15.40    16.40          16.60   14.30
   1-Feb-04   N/A      N/A     N/A     N/A   N/A   16.5   16.2   15.9     N/A    16.0    5.1    1.0     1.2      1.2     1.3   6.70    6.81    6.83   6.84   6.79   6.3      7.7    6.3     6.7     5.3   1,346 4,644 4,363 4,235 4,311                  6.33      22.00    21.40          21.90   20.30
   2-Feb-04   N/A      N/A     N/A     N/A   N/A   16.7   18.4   18.2     18.2   17.7    4.2    1.2     1.3      1.2     1.5   6.81    6.80    6.88   6.85   6.68   6.3      8.2    7.0     7.1     5.8   1,456 4,428 4,096 4,083 4,029                  5.91      19.40    15.20          15.40   14.90
   3-Feb-04   CLR      CLR     CLR     CLR   CLR   16.4   18.1   18.2     18.0   18.1    2.9    0.6     0.8      5.4     2.4   6.88    6.96    6.97   6.89   6.85   6.9      6.8    7.1     6.6     6.1   1,531 2,455 2,320 2,277 2,277                  9.34      11.50     8.66           8.77    8.84
   4-Feb-04   CLR      CLR     CLR     CLR   CLR   16.1   18.4   17.9     18.3   18.2    2.6    0.7     1.2      0.9     1.1   6.80    6.96    6.93   6.89   6.78   6.9      6.8    7.2     6.4     5.3   1,686 4,018 4,162 4,073 3,827                  17.5       8.82    10.60          11.00    9.83
   5-Feb-04   CLR      CLR     CLR     CLR   CLR   16.3   19.0   18.9     18.9   18.7    1.9    1.1     0.9      0.6     0.9   6.85    6.91    6.97   6.95   6.79   6.2      6.7    6.7     6.4     5.1   1,636 4,453 4,273 4,185 4,182                  14.6       8.68     7.36           7.11    7.39
   6-Feb-04   CLR      CLR     CLR     CLR   CLR   19.4   20.7   20.6     20.9   20.9    2.3    0.9     0.8      1.7     1.0   6.72    6.70    6.68   6.55   6.48   5.4      5.9    6.0     5.9     5.0   4,534 4,513 4,534 4,491 4,491                  14.3       6.58     5.36           5.40    5.32
   7-Feb-04   N/A      N/A     N/A     N/A   N/A   17.8   21.4   20.7     20.5   20.9    2.4    1.0     1.2      1.2     1.4   6.68    6.79    6.54   6.60   6.46   4.3      6.7    6.0     6.8     4.7   1,678 4,729 4,548 4,408 4,612                  14.2       5.95     4.68           4.69    4.75
   8-Feb-04   N/A      N/A     N/A     N/A   N/A   11.5   13.8   14.0     13.8   12.8    6.6    1.0     1.0      1.2     1.4   6.69    6.64    6.57   6.64   6.50   7.1      9.5    7.8     8.3     7.2   1,761 5,030 4,514 4,527 4,725                  15.4       4.97     5.08           5.12    4.52
   9-Feb-04   N/A      N/A     N/A     N/A   N/A   12.1   12.1   13.8     12.3   12.7    3.4    1.5     1.2      1.2     1.4   6.76    6.56    6.68   6.72   6.57   7.1      9.3    8.3     9.1     6.9   1,662 5,090 4,935 4,921 4,921                  15.4      10.90    15.90          15.90   13.70
 10-Feb-04    CLR      CLR     CLR     CLR   CLR   15.5   16.5   16.5     16.6   16.7     2     1.4     0.8      0.8     0.9   6.87    6.76    6.81   6.75   6.61   6.3      8.3    6.9     6.7     5.9   1,700 5,350 5,190 5,180 5,080                  17.6      21.00    25.40          25.30   22.40
 11-Feb-04    CLR      CLR     CLR     CLR   CLR    17    18.6   18.8     18.8   19.0    2.6    0.8     0.5      0.8     1.1   6.83    6.85    6.79   6.70   6.56   6.0      6.4    6.4     6.1     5.1   1,599 5,120 4,520 4,489 4,454                  19.6      25.60    23.10          23.10   22.90
 12-Feb-04    CLR      CLR     CLR     CLR   CLR   18.5   20.6   20.5     20.5   20.2    1.9    0.5     0.7      1.2     1.3   6.94    6.71    6.71   6.58   6.60   5.9      5.8    6.4     5.8     6.5   1,645 3,597 3,739 3,653 3,149                  20.5      14.70    16.30          16.10   12.50
 13-Feb-04    CLR      CLR     CLR     CLR   CLR   20.5   22.3   22.3     22.3   22.3    1.8    0.6     0.8      1.1     0.9   6.91    6.61    6.53   6.58   6.60   5.6      5.7    5.7     4.7     4.0   1,551 3,566 3,430 3,606 3,755                   20       11.50     9.65          10.10   10.70
 14-Feb-04    N/A      N/A     N/A     N/A   N/A   19.1   20.7   20.4     21.4   20.7    3.1    1.3     1.3      1.3     1.2   6.83    6.77    6.57   6.65   6.36   3.9      6.9    5.1     6.5     3.6   1,682 4,250 3,987 3,986 3,903                  19.8      10.30     8.06           8.06    8.93
 15-Feb-04    N/A      N/A     N/A     N/A   N/A   19.8   20.0   20.3     20.5   19.9    5.4    1.3     1.2      1.2     1.0   6.82    6.80    6.67   6.67   6.64   6.3      7.3    6.7     6.5     4.4   1,321 4,166 3,852 3,848 3,618                  8.75       7.36     6.41           6.41    6.88
 16-Feb-04    N/A      N/A     N/A     N/A   N/A   15.1   18.0   17.5     16.4   17.5    4.6    1.3     1.2      1.2     1.3   6.94    6.76    6.72   6.74   6.59   7.2      7.8    7.4     6.7     6.6   1,463 4,443 3,984 3,905 4,010                  7.73       7.17     7.20           7.26    6.37
 17-Feb-04    CLR      CLR     CLR     CLR   CLR   15.6   16.0   16.3     16.6   16.7    3.4    1.3     1.0      0.8     0.1   6.98    6.67    6.68   6.67   6.56   7.0      7.3    6.8     7.1     6.4   1,602 4,719 4,517 4,463 4,452                  10.3       7.88     9.20           7.76    6.75
 18-Feb-04    CLR      CLR     CLR     CLR   CLR   11.8   13.2   13.4     13.7   13.7    3.5    0.7     0.4      0.7     0.6   7.01    6.85    6.79   6.73   6.61   8.5      9.2    7.9     8.0     6.8   1,657 4,828 4,306 4,305 4,262                  12.2      12.40    12.80          12.80   11.20
 19-Feb-04    CLR      CLR     CLR     CLR   CLR   11.3   13.6   13.0     13.4   13.6    4.2    1.0     0.7      0.7     0.6   6.99    6.85    6.70   6.70   6.60   8.6      8.4    7.7     7.7     7.3   1,626 4,128 4,016 4,001 3,644                  13.6      11.40    14.70          15.10   11.70
 20-Feb-04    CLR      CLR     CLR     CLR   CLR   11.6   14.3   14.7     15.0   14.3    4.2    0.4     0.7      0.3     0.6   7.01    6.75    6.66   6.66   6.53   8.2      7.6    7.0     7.8     6.3   1,676 4,663 3,165 3,187 3,735                  14.2      20.20    12.60          12.70   14.00
 21-Feb-04    N/A      N/A     N/A     N/A   N/A   16.5   16.4   16.4     17.4   17.2    3.7    1.0     1.3      1.2     1.2   6.99    6.59    6.64   6.65   6.47   6.1      7.9    6.3     6.1     5.1   1,648 4,798 3,643 3,620 3,764                  14.5      19.20    15.10          15.30   15.30
 22-Feb-04    N/A      N/A     N/A     N/A   N/A   17.4   18.8   19.2     19.0   18.3    2.4    1.0     1.2      1.2     1.0   6.87    6.61    6.53   6.56   6.38   4.9      7.0    5.1     5.8     4.2   1,614 4,577 3,304 3,299 3,070                  7.33      15.20     9.66          12.80   11.60
 23-Feb-04    N/A      N/A     N/A     N/A   N/A   15.7   17.8   18.1     17.7   16.7    2.5    1.2     1.2      1.3     1.4   6.89    6.51    6.50   6.56   6.50   6.8      7.2    6.2     6.2     5.2   1,522 4,816 3,649 3,635 3,486                   12       17.20    12.50          12.50   12.70
 24-Feb-04    CLR      CLR     CLR     CLR   CLR   19.7   21.2   21.6     21.6   21.5    1.5    0.6     0.7      1.2     0.7   6.97    6.44    6.44   6.49   6.44   5.7      6.4    5.9     4.8     4.3   1,575 3,791 3,213 2,624 2,546                  13.4      13.10     8.31           6.36    5.81
 25-Feb-04    CLR      CLR     CLR     CLR   CLR   18.9   19.9   19.9     19.8   20.1   31.5    4.5     1.9      1.8     2.9   6.85    6.78    6.80   6.79   6.67   6.2      6.4    6.5     6.2     4.8    733    4,295 3,223 3,235 2,942                5.39      11.20     5.98           6.05    5.88

              Printed On: 11/22/2011                                                                                                  Page 13 of 30                                                                      C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                                                                                     Table 3
                                                                                                                      Daily Water Quality Monitoring Results
                                                                                                                           Emergency Order No. 02-1054
                                                                                                                        Piney Point Phosphates Complex

Parameter              Visual Observations                  Temperature (oC)                      Turbidity NTU)                      pH (Standard Units)                Dissolved Oxygen (mg/L)              Specific Conductance (µs/cm)                                Ammonia
Station       X-1      003    BR/41    X-2   AR    X-1    003   BR/41     X-2     AR    X-1    003    BR/41    X-2      AR    X-1     003    BR/41   X-2     AR    X-1     003    BR/41    X-2     AR     X-1     003    BR/41    X-2      AR           X-1        003     BR/41           X-2     AR
 26-Feb-04    CLR      CLR     CLR     CLR   CLR   19.4   19.7   19.9     19.8   20.1    7.4   1.5     1.9      1.9     2.1   6.88    6.73    6.80   6.83   6.74   6.4      5.8    5.7     5.4     5.1   1,157 4,136 3,363 2,948 2,617                  3.12       6.56     4.00           4.02   3.06
 27-Feb-04    CLR      CLR     CLR     CLR   CLR   17.1   18.7   18.7     19.0   18.4    7.9   1.8     1.1      1.4     1.2   6.97    6.95    6.62   6.62   6.64   7.5      6.4    5.9     6.0     5.1   1,279 4,273 3,432 2,575 3,216                  6.54       7.42     5.91           4.54   5.40
 28-Feb-04    N/A      N/A     N/A     N/A   N/A   12.4   12.2   13.5     13.1   14.4    2.1   1.0     1.3      1.3     1.4   7.00    6.59    6.68   6.63   6.64   9.1      8.5    7.0     6.9     5.8   1,406 4,399 3,651 3,689 3,380                  9.74       8.31     6.37           6.50   5.66
 29-Feb-04    N/A      N/A     N/A     N/A   N/A   12.9   14.8   15.2     16.1   14.7    2.6   1.0     1.2      1.2     1.3   7.01    6.64    6.77   6.80   6.68   7.6      7.8    7.0     7.2     6.0   1,389 4,764 3,278 3,267 3,106                  12.6       9.47     7.66           7.55   6.44
   1-Mar-04   N/A      N/A     N/A     N/A   N/A   16.5   17.5   18.8     18.5   18.2    2.6   1.3     1.3      1.2     1.0   6.89    6.68    6.67   6.67   6.53   6.3      7.4    7.2     7.2     4.7   1,474 4,448 3,043 3,129 2,960                  14.1      11.10     7.11           7.03   6.21
   2-Mar-04   CLR      CLR     CLR     CLR   CLR    17    19.3   19.1     19.1   19.1    8.1   0.7     0.6      1.0     0.5   6.92    6.71    6.71   6.71   6.57   6.5      6.3    6.4     5.5     5.6   1,468 4,014 3,199 3,250 3,046                  14.3      10.70     6.85           6.99   6.28
   3-Mar-04   CLR      CLR     CLR     CLR   CLR   18.5   20.5   19.4     19.7   19.8    7.9   0.3     0.7      0.8     0.7   6.85    6.89    6.77   6.74   6.62   6.5      6.4    6.4     5.9     5.5   1,463 1,526 3,983 3,989 4,034                   14        9.69     7.29           7.18   6.66
   4-Mar-04   CLR      CLR     CLR     CLR   CLR   18.3   19.7   20.1     20.1   20.1    6.8   1.3     0.6      0.8     0.8   6.86    6.70    6.70   6.61   6.65   6.5      6.4    6.6     6.6     5.3   1,439 5,350 3,574 4,189 3,340                  13.7       6.87     5.10           5.83   4.96
   5-Mar-04   CLR      CLR     CLR     CLR   CLR   19.3   20.4   20.7     20.9   21.1    6.4   0.8     0.7      0.9     0.7   6.92    6.76    6.74   6.67   6.50   6.5      6.6    5.8     5.8     5.1   1,433 4,952 3,793 3,671 3,669                  13.3       6.62     4.97           4.97   4.31
   6-Mar-04   N/A      N/A     N/A     N/A   N/A   17.9   21.2   21.4     20.9   21.1    2.8   1.0     1.3      1.3     1.2   6.86    6.58    6.56   6.56   6.50   5.3      5.8    5.5     5.7     3.8   1,379 5,580 3,889 3,858 3,627                  12.2       7.31     6.00           5.95   7.37
   7-Mar-04   N/A      N/A     N/A     N/A   N/A   20.7   22.5   23.4     21.4   22.6    2.6   1.0     1.3      1.8     1.2   6.90    6.65    6.80   7.10   6.37   4.7      6.1    5.4     4.4     4.5   1,338 5,060 3,455 2,733 3,546                  10.7       7.96     5.61           8.41   5.44
   8-Mar-04   N/A      N/A     N/A     N/A   N/A    22    20.9   22.0     21.5   21.3    2.6   1.3     1.3      1.2     1.4   6.90    6.77    6.65   6.66   6.49   5.8      5.8    5.7     5.9     4.7   3,471 5,050 3,516 3,430 3,550                  12.1       8.54     6.35           6.23   5.55
   9-Mar-04   CLR      CLR     CLR     CLR   CLR   14.2   14.8   15.9     16.5   17.0    4.7   0.8     0.9      0.8     1.6   6.96    6.68    6.76   6.74   6.53   7.6      7.9    7.1     6.4     5.9   1,352 5,910 4,040 3,882 3,723                  9.84       6.98     5.19           5.86   4.31
 10-Mar-04    CLR      CLR     CLR     CLR   CLR   15.5   17.3   17.5     17.7   17.8    4.5   0.9     0.8      0.8     0.8   7.01    6.76    6.76   6.66   6.50   7.9      7.2    6.3     6.4     6.4   1,201 4,436 3,381 3,416 3,414                  8.56       9.88     8.39           8.56   6.71
 11-Mar-04    CLR      CLR     CLR     CLR   CLR   13.9   15.6   15.5     15.6   15.2   11.7   0.9     0.6      1.0     0.6   7.16    6.77    6.71   6.72   6.46   8.8      8.1    8.1     7.9     7.1   1,178 4,668 3,874 3,502 3,370                  7.49      10.60     7.26           6.58   6.05
 12-Mar-04    CLR      CLR     CLR     CLR   CLR   14.3   16.2   16.6     16.8   16.6   56.4   1.3     1.9      1.1     0.8   7.01    6.64    6.54   6.54   6.36   7.7      7.5    7.3     6.9     6.5   1,187 4,248 3,406 3,402 3,263                  6.51       8.48     6.18           6.50   5.16
 13-Mar-04    N/A      N/A     N/A     N/A   N/A   15.3   18.1   17.5     18.0   17.4    6.4   1.2     1.2      1.3     1.2   6.93    6.65    6.59   6.61   6.27   4.4      6.6    6.4     6.8     4.6   1,233 4,040 3,579 3,579 3,190                  7.22       8.81     7.05           7.16   5.40
 14-Mar-04    DRY      N/A     N/A     N/A   N/A   DRY    18.3   19.5     18.9   19.5   DRY    1.2     1.2      1.3     1.4   DRY     6.53    6.44   6.44   6.27   DRY      7.2    5.8     6.3     4.5   DRY     4,741 3,810 3,853 3,828                DRY        9.96     6.76           6.81   6.63
 15-Mar-04    DRY      N/A     N/A     N/A   N/A   DRY    20.3   20.1     21.0   20.9   DRY    1.0     1.2      1.2     1.3   DRY     6.42    6.49   6.44   6.25   DRY      6.5    5.4     5.2     3.9   DRY     4,617 3,340 3,347 3,428                DRY       10.80     6.18           6.35   6.48
 16-Mar-04    CLR      CLR     CLR     CLR   CLR   21.5   21.9   22.0     21.9   22.2    6.2   0.9     0.8      0.9     0.8   6.74    6.66    6.55   6.50   6.28   6.4      6.4    5.4     5.2     4.6   1,208 4,726 3,270 3,224 3,144                  13.4       6.97     7.06           6.68   5.81
 17-Mar-04    CLR      CLR     CLR     CLR   CLR   20.0   20.7   21.4     21.4   21.6   10.1   1.4     1.2      1.9     0.9   6.82    6.68    6.55   6.47   6.45   5.7      5.6    5.0     4.5     2.8   1,309 4,326 3,268 3,272            3066        10.7      11.30     8.11           8.34   7.26
 18-Mar-04    CLR      CLR     CLR     CLR   CLR   16.7   18.7   18.8     19.0   19.1    6.4   1.3     1.1      1.5     1.1   6.84    6.67    6.67   6.62   6.49   7.7      6.1    6.4     5.7     5.3   1,509 4,855 3,882 3,820            3603        11.6       9.46     7.43           7.52   6.87
 19-Mar-04    CLR      CLR     CLR     CLR   CLR   17.3   20.2   20.0     20.3   19.9    5.7   1.0     0.8      1.4     0.8   6.98    6.84    6.87   6.86   6.63   7.3      6.6    5.7     5.7     5.7   1,436 4,171 3,478 3,465            3481        12.1      10.50     7.50           8.42   6.92
 20-Mar-04    N/A      N/A     N/A     N/A   N/A   17.1   19.8   20.3     19.2   20.7    2.8   1.0     1.3      1.3     1.2   7.08    6.84    6.64   6.67   6.60   7.0      6.0    5.8     5.4     4.5   1,461 4,690 4,938 4,788            4550         15       10.20     9.90          10.10   9.10
 21-Mar-04    N/A      N/A     N/A     N/A   N/A   16.9   20.9    0.0     20.3   19.6    2.6   1.0     1.3      1.3     1.4   7.17    6.47    6.50   6.50   6.41   7.4      7.1    5.7     6.0     5.0   1,423 4,335 3,758 3,745            4169        14.3       8.70     5.20           5.10   6.00
 22-Mar-04    N/A      N/A     N/A     N/A   N/A   18.9   20.8   21.0     21.8   21.4    2.6   1.0     1.2      1.2     1.2   7.17    6.60    6.67   6.56   6.46   5.7      5.8    5.7     5.6     4.2   1,267 5,290 3,930 3,945            3693        13.7       8.57     7.88           7.88   6.26
 23-Mar-04    DRY      CLR     CLR     CLR   CLR   DRY    16.9   15.8     15.3   16.0   DRY    1.3     0.8      1.3     1.2   DRY     6.72    6.23   6.68   6.50   DRY      7.6    8.2     8.3     7.8   DRY     4,793 3,761 3,812          3726        DRY        9.13     5.78           5.82   5.51
 24-Mar-04    DRY      CLR     CLR     CLR   CLR   DRY    17.8   16.6     16.2   16.5   DRY    1.0     0.7      1.2     1.1   DRY     6.69    6.70   6.60   6.39   DRY      7.5    7.5     7.7     7.6   DRY     4,156 3,384 3,389          3582        DRY        8.60     5.77           5.74   5.44
 25-Mar-04    N/A      CLR     CLR     CLR   CLR   N/A    17.5   18.2     18.5   18.4   N/A    1.1     1.5      0.9     1.0   N/A     6.67    6.65   6.55   6.30   N/A      7.0    6.7     6.0     4.9    N/A    4,298 3,391 3,434          3350        N/A        6.28     4.18           4.27   4.23
 26-Mar-04    DRY      N/A     N/A     N/A   N/A   DRY    18.2   19.1     19.0   19.4   DRY    1.3     1.3      1.3     1.5   DRY     6.64    6.56   6.56   6.38   DRY      7.8    8.3     7.5     5.8   DRY     5,040 3,619 3,669          3607        DRY        4.64     3.05           2.98   2.94
 27-Mar-04    DRY      N/A     N/A     N/A   N/A   DRY    20.2   20.4     20.7   19.4   DRY    1.0     1.3      1.2     1.4   DRY     6.47    6.59   6.66   6.35   DRY      6.2    6.2     5.9     5.7   DRY     4,410 3,710 3,689          3750        DRY        4.57     2.64           2.79   2.90
 28-Mar-04    DRY      N/A     N/A     N/A   N/A   DRY    19.0   21.2     21.4   20.7   DRY    1.0     1.3      1.3     1.3   DRY     6.59    6.54   6.55   6.40   DRY      6.6    5.1     4.8     4.9   DRY     4,546 3,443 3,382          3248        DRY        3.32     2.69           2.55   2.15
 29-Mar-04    DRY      N/A     N/A     N/A   N/A   DRY    20.1   20.6     20.5   20.4   DRY    1.3     1.3      1.3     1.3   DRY     6.64    6.59   6.59   6.47   DRY      6.5    5.7     5.8     4.0   DRY     5,400 4,271 4,289          4254        DRY        4.52     3.94           3.93   3.53
 30-Mar-04    DRY      CLR     CLR     CLR   CLR   DRY    21.2   21.2     21.1   20.6   DRY    0.6     0.6      1.0     1.1   DRY     6.76    6.66   6.64   6.52   DRY      8.1    6.9     6.3     5.0   DRY     4,952 3,809 3,772 3,724                DRY        4.58     4.23           3.80   3.36
 31-Mar-04    DRY      CLR     CLR     CLR   CLR   DRY    22.4   22.5     22.7   22.9   DRY    0.8     1.0      1.1     0.7   DRY     6.88    6.72   6.68   6.52   DRY      7.9    7.2     6.3     4.8   DRY     5,040 4,566 4,159 3,758                DRY        6.53     7.38           7.53   4.83
   1-Apr-04   DRY      CLR     CLR     CLR   CLR   DRY    20.9   21.2     21.1   21.1   DRY    0.5     0.8      0.9     0.8   DRY     6.66    6.59   6.45   6.33   DRY      6.5    6.0     5.2     4.9   DRY     5,020 3,897 3,744 3,691                DRY        9.06     8.06           7.94   7.66
   2-Apr-04   DRY      CLR     CLR     CLR   CLR   DRY    20.3   19.8     20.3   19.4   DRY    0.2     1.0      1.0     0.8   DRY     6.76    6.58   6.49   6.24   DRY      5.9    5.5     5.2     3.3   DRY     2,655 2,211 1,973 1,939                DRY        4.59     3.65           3.23   2.71
   3-Apr-04   DRY      N/A     N/A     N/A   N/A   DRY    18.6   20.5     20.6   18.3   DRY    1.0     1.2      1.2     1.2   DRY     6.59    6.60   6.58   6.31   DRY      6.4    6.3     5.2     3.9   DRY     3,762 1,147 1,148 2,801                DRY        4.71     1.90           1.88   4.15
   4-Apr-04   DRY      N/A     N/A     N/A   N/A   DRY    21.9   20.5     20.5   20.0   DRY    1.0     1.2      1.2     1.3   DRY     6.65    6.57   6.57   6.37   DRY      6.0    5.2     4.9     4.8   DRY      157     3,170 3,180 3,305             DRY        6.39     4.57           4.58   4.20
   5-Apr-04   DRY      N/A     N/A     N/A   N/A   DRY    21.9   21.8     21.9   20.1   DRY    1.2     1.2      1.2     1.3   DRY     6.46    6.54   6.60   6.35   DRY      5.6    5.6     6.0     4.3   DRY      120      175    161      577          DRY        2.08     0.24           0.24   0.38
   6-Apr-04   DRY      CLR     CLR     CLR   CLR   DRY    17.8   17.9     17.7   17.4   DRY    0.4     0.4      1.7     0.9   DRY     6.70    6.75   6.72   6.45   DRY      7.1    6.8     5.9     6.3   DRY     5,010 3,731 3,822 3,538                DRY        4.20     4.51           5.21   3.63
   7-Apr-04   DRY      CLR     CLR     CLR   CLR   DRY    19.9   20.1     20.4   19.8   DRY    0.5     1.0      2.0     0.9   DRY     6.72    6.75   6.77   6.60   DRY      7.0    6.3     5.6     5.3   DRY     4,752 3,713 4,116 3,907                DRY        5.68     4.65           4.86   4.12
   8-Apr-04   DRY      CLR     CLR     CLR   CLR   DRY    21.6   21.9     21.8   22.0   DRY    0.4     0.6      0.5     0.8   DRY     6.65    6.68   6.64   6.51   DRY      7.1    6.0     5.5     5.2   DRY     5,250 3,701 3,676 3,549                DRY        5.93     5.59           5.52   4.77
   9-Apr-04   DRY      CLR     CLR     CLR   CLR   DRY    23.6   23.7     23.2   23.3   DRY    0.4     0.9      0.7     0.9   DRY     6.81    6.85   6.82   6.61   DRY      5.6    5.3     5.4     3.9   DRY     4,175 3,267 3,141 3,162                DRY        7.88     6.60           6.04   5.49
  10-Apr-04   DRY      N/A     N/A     N/A   N/A   DRY    23.2   22.5     23.3   22.7   DRY    1.2     1.3      1.3     1.2   DRY     6.66    6.37   6.39   6.33   DRY      6.6    4.9     5.3     4.2   DRY     4,160 3,812 3,710 2,681                DRY        8.28     8.58           8.21   5.15
  11-Apr-04   DRY      N/A     N/A     N/A   N/A   DRY    21.5   23.4     23.1   22.7   DRY    1.0     1.2      1.2     1.3   DRY     6.83    6.54   6.56   6.37   DRY      6.8    5.3     5.6     4.1   DRY     7,460 3,955 3,961 3,824                DRY        9.80     8.37           8.11   7.09
  12-Apr-04   DRY      N/A     N/A     N/A   N/A   DRY    22.6   22.8     23.0   22.3   DRY    1.0     1.2      1.2     1.3   DRY     6.73    6.55   6.60   6.51   DRY      5.3    5.5     5.8     3.3   DRY     4,889 3,815 3,752 3,499                DRY        7.40     5.57           5.42   5.23
  13-Apr-04   CLR      CLR     CLR     CLR   CLR   20.8   20.8   21.3     21.0   21.1    3.6   1.4     1.2      1.6     1.8   6.91    6.92    6.77   6.81   6.86   6.8      5.8    5.7     5.4     4.5   1,445 5,010 3,821 3,712 3,715                  1.81       6.45     3.71           3.71   3.82
  14-Apr-04   CLR      CLR     CLR     CLR   CLR   15.9   17.6   17.6     17.7   17.8    3.5   1.3     3.0      1.5     1.2   6.94    6.94    6.76   6.73   6.72   7.5      7.3    5.7     5.1     3.3   1,510 5,370 4,374 4,516 4,225                   6.1       4.37     4.16           3.97   3.27
  15-Apr-04   CLR      CLR     CLR     CLR   CLR   15.3   16.3   16.4     16.7   16.5    2.9   1.2     1.0      0.9     0.9   6.97    6.84    6.75   6.73   6.65   7.8      7.7    6.8     6.5     5.7   1,457 5,350 4,252 4,187 4,277                  5.43       3.79     2.84           2.62   2.50
  16-Apr-04   CLR      CLR     CLR     CLR   CLR   14.6   15.9   16.2     16.2   15.8    3.4   1.3     0.9      0.8     1.2   7.25    7.03    6.85   6.88   6.79   7.5      7.0    6.3     6.6     5.7   1,295 5,540 4,322 4,348 4,156                  5.86       3.82     3.58           3.56   2.68
  17-Apr-04   N/A      N/A     N/A     N/A   N/A    16    18.6   19.1     18.8   18.6     2    1.0     1.3      1.3     1.2   7.29    6.69    6.62   6.60   6.47   6.1      6.6    5.5     5.5     4.9   1,235 4,842 3,989 3,978 3,926                  8.19       4.30     3.37           3.54   3.53
  18-Apr-04   DRY      N/A     N/A     N/A   N/A   N/A    19.2   19.7     19.1   18.6   N/A    1.0     1.3      1.3     1.2   N/A     6.64    6.64   6.66   6.47   N/A      6.4    4.7     4.4     3.5    N/A    4,766 3,795 3,804 3,983                N/A        4.66     3.81           3.19   2.65
  19-Apr-04   DRY      N/A     N/A     N/A   N/A   N/A    17.6   18.9     18.8   19.2   N/A    1.0     1.2      1.2     1.2   N/A     6.84    6.72   6.70   6.58   N/A      7.0    5.3     5.1     2.7    N/A    7,320 6,130 6,130 4,436                N/A        4.41     4.74           4.59   3.08
  20-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A    19.9   20.2     19.9   20.1   N/A    0.8     0.7      1.0     0.8   N/A     6.68    6.60   6.58   6.48   N/A      6.3    5.5     5.8     5.1    N/A    5,800 4,422 4,424 4,310                N/A        3.80     2.90           3.21   2.45
  21-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A    21.5   21.9     21.8   21.8   N/A    0.8     1.1      1.2     0.9   N/A     6.77    6.66   6.65   6.57   N/A      6.7    4.6     4.0     2.6    N/A    4,812 3,690 3,659 3,341                N/A        4.64     5.26           5.20   5.12

              Printed On: 11/22/2011                                                                                                 Page 14 of 30                                                                      C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                                                                                   Table 3
                                                                                                                    Daily Water Quality Monitoring Results
                                                                                                                         Emergency Order No. 02-1054
                                                                                                                      Piney Point Phosphates Complex

Parameter              Visual Observations                 Temperature (oC)                     Turbidity NTU)                     pH (Standard Units)                Dissolved Oxygen (mg/L)               Specific Conductance (µs/cm)                                Ammonia
Station       X-1      003    BR/41    X-2   AR    X-1   003   BR/41     X-2     AR    X-1   003    BR/41    X-2      AR    X-1    003    BR/41   X-2     AR    X-1     003    BR/41    X-2     AR    X-1       003    BR/41    X-2      AR            X-1       003     BR/41          X-2     AR
  22-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A   21.7   21.5     21.0   21.1   N/A   0.8      0.7     0.9     0.7   N/A    6.84    6.62   6.52   6.49   N/A      6.1    5.7     5.4     5.3   N/A      4,827 3,774 3,713 3,768                 N/A       5.65     6.45          6.30   5.20
  23-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A   23.4   23.0     22.9   22.8   N/A   0.6      0.7     0.8     0.8   N/A    6.55    6.50   6.41   6.33   N/A      5.6    4.6     4.6     4.2   N/A      4,377 3,258 3,202 3,317                 N/A       7.94     5.35          5.35   5.12
  24-Apr-04   N/A      N/A     N/A     N/A   N/A   N/A   25.4   23.4     23.1   21.9   N/A   1.0      1.3     1.3     1.4   N/A    6.50    6.21   6.14   5.96   N/A      5.6    4.5     4.8     3.9   N/A      3,826 3,340 3,340 3,381                 N/A       6.27     3.39          3.32   3.78
  25-Apr-04   N/A      N/A     N/A     N/A   N/A   N/A   24.4   24.9     24.8   24.0   N/A   1.0      1.3     1.3     1.2   N/A    6.58    6.36   6.32   6.23   N/A      6.1    5.0     5.2     3.8   N/A      4,101 3,292 3,297 3,230                 N/A       3.75     2.07          2.04   2.31
  26-Apr-04   N/A      N/A     N/A     N/A   N/A   N/A   23.0   24.2     24.3   24.3   N/A   1.0      1.2     1.2     1.3   N/A    6.70    6.44   6.41   6.48   N/A      5.1    5.5     5.6     3.6   N/A      5,810 4,650 4,619 3,851                 N/A       3.31     4.32          4.20   2.13
  27-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A   24.7   24.4     24.7   24.6   N/A   0.6      0.9     1.0     1.0   N/A    6.60    6.50   6.48   6.25   N/A      5.5    4.6     4.4     4.0   N/A      4,885 3,756 3,753 3,815                 N/A       5.02     3.13          3.48   3.08
  28-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A   21.5   19.6     20.6   20.0   N/A   0.7      0.7     0.7     0.9   N/A    6.72    6.40   6.62   6.40   N/A      5.7    5.1     5.6     4.9   N/A      4,602 3,638 3,547 3,450                 N/A       4.73     2.42          2.46   2.52
  29-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A   21.8   22.4     22.1   21.8   N/A   0.6      0.7     0.9     0.9   N/A    6.88    6.81   6.77   6.55   N/A      6.2    5.6     4.8     5.0   N/A      5,430 4,125 4,097 3,636                 N/A       2.52     1.74          1.79   1.43
  30-Apr-04   N/A      CLR     CLR     CLR   CLR   N/A   24.0   24.1     23.7   23.7   N/A   0.9      0.7     0.8     0.8   N/A    6.81    6.79   6.73   6.57   N/A      5.7    4.6     4.5     4.0   N/A      5,030 3,691 3,624 3,628                 N/A       1.88     1.48          1.46   1.17
  1-May-04    N/A      N/A     N/A     N/A   N/A   N/A   25.8   24.8     24.6   24.5   N/A   1.0      1.3     1.3     1.2   N/A    7.19    6.81   6.81   6.69   N/A      5.4    4.6     4.3     3.2   N/A      126.1 328.9 280.8 843.0                 N/A       1.09     0.66          0.64   0.97
  2-May-04    N/A      N/A     N/A     N/A   N/A   N/A   26.1   26.3     26.5   25.3   N/A   1.2      1.3     1.3     1.2   N/A    6.90    6.71   6.66   6.54   N/A      3.9    6.2     5.4     4.2   N/A      2,646 2,202 2,195 2,307                 N/A       1.54     1.25          1.26   0.97
  3-May-04    N/A      N/A     N/A     N/A   N/A   N/A   27.1   27.3     27.2   26.2   N/A   1.0      1.3     1.3     1.2   N/A    6.98    6.71   6.67   6.39   N/A      4.8    4.0     4.2     5.3   N/A      2,998 2,322 2,332 2,230                 N/A       0.95     0.82          0.83   0.66
  4-May-04    N/A      CLR     CLR     CLR   CLR   N/A   23.2   22.5     22.1   21.4   N/A   0.7      1.1     1.1     1.7   N/A    6.81    6.82   6.79   6.75   N/A      4.7    4.6     4.4     4.1   N/A      3,228 2,687 2,654 2,413                 N/A       0.96     1.10          1.20   0.78
  5-May-04    N/A      CLR     CLR     CLR   CLR   N/A   23.1   22.4     21.7   21.1   N/A   0.6      0.9     0.9     1.0   N/A    6.84    6.75   6.67   6.58   N/A      5.1    5.2     5.4     4.5   N/A      2,982 2,369 2,237 2,419                 N/A       0.73     0.66          0.97   0.60
  6-May-04    N/A      CLR     CLR     CLR   CLR   N/A   23.6   22.5     21.8   21.3   N/A   0.6      0.8     1.1     1.1   N/A    6.82    6.77   6.74   6.61   N/A      5.3    5.0     5.2     4.8   N/A      2,773 2,194 2,131 2,274                 N/A       0.55     0.63          0.63   0.42
  7-May-04    N/A      CLR     CLR     CLR   CLR   N/A   23.3   22.8     22.8   22.5   N/A   1.2      1.5     1.9     1.2   N/A    7.03    7.01   6.88   6.73   N/A      5.6    5.2     4.6     4.4   N/A      4,673 3,077 2,895 2,373                 N/A       0.44     0.86          1.25   0.48
  8-May-04    N/A      N/A     N/A     N/A   N/A   N/A   24.6   23.8     23.6   22.8   N/A   1.0      1.3     1.3     1.2   N/A    7.05    6.86   6.81   6.59   N/A      5.2    4.7     4.5     4.4   N/A      3,159 2,418 2,491 2,565                 N/A       0.46     0.46          0.44   1.62
  9-May-04    N/A      N/A     N/A     N/A   N/A   N/A   23.6   23.6     23.8   23.4   N/A   1.0      1.2     1.2     1.3   N/A    6.68    6.59   6.56   6.52   N/A      5.1    4.1     4.4     3.2   N/A      4,856 4,034 4,036 2,819                 N/A       0.62     1.17          1.16   0.76
 10-May-04    N/A      N/A     N/A     N/A   N/A   N/A   24.1   24.2     24.2   23.3   N/A   1.0      0.0     1.3     1.2   N/A    6.69    6.59   6.60   6.50   N/A      5.1    4.3     4.5     3.3   N/A      3,824 3,144 3,145 3,941                 N/A       0.78     0.64          0.63   0.78
 11-May-04    N/A      CLR     CLR     CLR   CLR   N/A   23.9   23.9     23.7   23.3   N/A   0.9      1.0     1.4     1.5   N/A    6.80    6.91   6.91   6.79   N/A      4.8    4.7     4.3     4.1   N/A      4,406 2,999 2,192 1,708                 N/A       0.58     0.59          0.47   0.30
 12-May-04    N/A      CLR     CLR     CLR   CLR   N/A   24.4   24.0     23.8   23.2   N/A   0.8      1.1     1.2     1.5   N/A    6.67    6.56   6.46   6.45   N/A      4.3    4.6     4.4     4.8   N/A      3,048 2,366 2,424 3,328                 N/A       0.65     0.52          0.56   0.62
 13-May-04    N/A      CLR     CLR     CLR   CLR   N/A   23.6   23.4     23.4   23.2   N/A   1.0      1.0     1.3     1.3   N/A    7.25    7.17   7.06   6.89   N/A      4.4    4.6     4.9     4.9   N/A      5,560 4,143 4,155 3,343                 N/A       0.54     0.74          1.05   0.43
 14-May-04    N/A      CLR     CLR     CLR   CLR   N/A   24.3   24.2     23.7   23.4   N/A   0.8      1.0     1.5     1.4   N/A    6.91    6.81   6.76   6.53   N/A      4.8    4.8     4.6     4.4   N/A      4,204 2,967 2,921 2,387                 N/A       0.21     0.16          0.21   0.12
 15-May-04    N/A      N/A     N/A     N/A   N/A   N/A   23.3   23.5     23.7   22.7   N/A   1.0      1.2     1.2     1.2   N/A    6.80    6.75   6.84   6.60   N/A      5.6    4.8     4.8     3.9   N/A      4,611 3,941 3,903 3,575                 N/A       0.09     0.10          0.10   0.10
 16-May-04    N/A      N/A     N/A     N/A   N/A   N/A   24.8   24.1     24.0   23.5   N/A   1.0      1.2     1.2     1.2   N/A    6.66    6.62   6.64   6.60   N/A      5.7    4.0     3.8     3.7   N/A      4,305 3,918 3,941 2,722                 N/A       0.64     0.72          0.71   0.51
 17-May-04    N/A      N/A     N/A     N/A   N/A   N/A   25.4   25.7     25.5   24.0   N/A   1.0      1.2     1.2     1.2   N/A    6.91    6.60   6.62   6.38   N/A      5.3    4.9     4.3     4.0   N/A      3,444 2,705 2,704 2,987                 N/A       0.60     0.40          0.39   0.37
 18-May-04    N/A      CLR     CLR     CLR   CLR   N/A   25.3   25.1     25.1   24.3   N/A   0.5      0.9     0.8     1.1   N/A    7.12    6.96   6.89   6.62   N/A      4.7    4.8     4.5     4.3   N/A      3,666 2,886 2,874 3,243                 N/A       0.40     0.27          0.30   0.22
 19-May-04    N/A      CLR     CLR     CLR   CLR   N/A   25.4   24.6     25.0   24.7   N/A   0.4      0.6     0.7     1.2   N/A    7.00    6.76   6.73   6.53   N/A      5.2    4.8     4.0     3.8   N/A      3,023 2,509 2,493 2,553                 N/A       0.48     0.28          0.28   0.28
 20-May-04    N/A      CLR     CLR     CLR   CLR   N/A   24.6   22.4     24.4   24.3   N/A   0.8      1.3     1.2     1.8   N/A    6.87    6.56   6.54   6.58   N/A      4.8    4.0     4.0     4.1   N/A      5,210 4,345 4,766 4,122                 N/A       0.69     0.66          0.70   0.29
 21-May-04    N/A      N/A     N/A     N/A   N/A   N/A   24.6   23.8      0.0   23.5   N/A   1.2      1.3     1.3     1.2   N/A    6.82    6.52   6.54   6.46   N/A      6.1    4.0     4.2     3.2   N/A      4,232 3,617 3,598 5,660                 N/A       0.94     0.45          0.44   0.44
 22-May-04    N/A      N/A     N/A     N/A   N/A   N/A   25.3   25.2     24.7   24.9   N/A   1.0      1.7     1.3     1.2   N/A    6.85    6.52   6.49   6.38   N/A      5.3    4.8     4.6     4.4   N/A      4,248 3,796 3,802 3,546                 N/A       0.93     0.55          0.54   0.44
 23-May-04    N/A      N/A     N/A     N/A   N/A   N/A   24.8   24.8     24.7   23.9   N/A   1.0      1.2     1.2     1.3   N/A    6.83    6.40   6.45   6.46   N/A      4.8    5.4     5.3     3.9   N/A      5,380 4,350 4,355 3,998                 N/A       1.18     0.74          0.64   0.44
 24-May-04    N/A      N/A     N/A     N/A   N/A   N/A   25.5   25.7     25.7   24.9   N/A   1.0      1.2     1.3     1.2   N/A    6.91    6.43   6.41   6.37   N/A      5.0    4.2     4.4     3.4   N/A      5,190 4,016 3,990 4,245                 N/A       1.91     0.58          0.49   0.51
 25-May-04    DRY      CLR     CLR     CLR   CLR   N/A   22.8   23.0     23.2   23.7   N/A   0.9      1.5     1.9     1.7   N/A    6.70    6.38   6.34   6.53   N/A      5.7    4.5     4.5     4.3   N/A      8,390 7,950 7,930 6,080                 N/A       2.36     1.57          1.34   0.48
 26-May-04    DRY      CLR     CLR     CLR   CLR   N/A   25.2   25.4     25.6   25.0   N/A   0.8      0.9     1.1     1.1   N/A    6.63    6.28   6.23   6.28   N/A      5.0    4.4     3.9     4.3   N/A      6,280 3,742 3,456 3,713                 N/A       2.24     0.86          0.79   0.62
 27-May-04    DRY      CLR     CLR     CLR   CLR   N/A   27.6   26.2     25.8   25.2   N/A   1.1      1.5     1.3     1.2   N/A    7.28    6.34   6.30   6.31   N/A      4.5    4.7     4.4     4.3   N/A       130      644   1,785 3,009             N/A       1.66     0.23          0.37   0.27
 28-May-04    DRY      CLR     CLR     CLR   CLR   N/A   27.6   27.1     27.1   26.0   N/A   0.6      1.0     1.0     1.2   N/A    7.17    6.67   6.61   6.41   N/A      4.3    4.2     4.3     3.6   N/A      3,889 3,301 3,414 3,187                 N/A       2.73     2.48          2.59   1.30
 29-May-04    DRY      N/A     N/A     N/A   N/A   N/A    0.0   26.0     26.6   25.1   N/A   1.0      1.2     1.3     1.2   N/A    6.84    6.22   6.18   6.21   N/A      4.9    4.1     3.7     3.3   N/A      5,010 5,300 5,310 4,980                 N/A       6.44     7.10          6.80   4.77
 30-May-04    DRY      N/A     N/A     N/A   N/A   N/A   27.2   27.1     27.3   24.7   N/A   1.2      1.2     1.2     1.3   N/A    6.72    6.11   6.14   6.20   N/A      4.6    3.5     3.2     4.1   N/A      4,604 3,581 3,583 3,901                 N/A       7.26     3.53          3.53   4.74
 31-May-04    DRY      N/A     N/A     N/A   N/A   N/A   25.3   25.9     26.4   25.9   N/A   1.0      1.2     1.3     1.2   N/A    6.84    6.30   6.29   6.17   N/A      4.5    3.7     3.3     3.5   N/A      5,180 4,241 4,250 3,910                 N/A       4.39     2.08          2.19   1.98
   1-Jun-04   DRY      CLR     CLR     CLR   CLR   N/A   26.9   26.0     26.1   25.3   N/A   0.9      0.6     1.2     0.9   N/A    6.88    6.07   6.08   6.17   N/A      4.0    3.9     3.8           N/A      5,350 4,229 3,727 4,205                 N/A       3.16     3.26          2.54   1.26
   2-Jun-04   DRY      CLR     CLR     CLR   CLR   N/A   27.5   26.3     27.1   26.2   N/A   1.0      0.7     1.5     0.9   N/A    6.89    6.45   6.37   6.21   N/A      3.8    3.5     3.8     3.6   N/A       5.3     4,200 4,160 4,396              N/A       5.82     3.63          3.40   2.91
   3-Jun-04   DRY      CLR     CLR     CLR   CLR   N/A   27.0   26.3     26.8   25.9   N/A   0.9      0.9     0.9     1.2   N/A    6.80    6.10   6.08   6.12   N/A      4.3    3.7     3.4     3.9   N/A      4,880 4,449 4,467 4,198                 N/A       4.75     3.42          3.28   2.41
   4-Jun-04   DRY      CLR     CLR     CLR   CLR   N/A   26.8   25.6     25.1   25.4   N/A   0.7      0.8     1.3     1.2   N/A    6.83    6.23   6.10   6.20   N/A      4.6    3.9     4.8     3.9   N/A      5,360 5,830 5,840 4,240                 N/A       3.95     3.62          3.83   1.75
   5-Jun-04   DRY      N/A     N/A     N/A   N/A   N/A   27.1   26.5     27.4   24.7   N/A   1.3      1.2     1.2     1.3   N/A    6.82    6.38   6.24   6.21   N/A      4.6    4.5     3.7     4.3   N/A      4,190 3,396 3,402 4,610                 N/A       3.18     1.68          1.63   2.30
   6-Jun-04   DRY      N/A     N/A     N/A   N/A   N/A   28.1   26.8     26.9   26.5   N/A   1.0      1.2     1.2     1.3   N/A    6.91    6.57   6.52   6.48   N/A      4.3    4.0     4.3     3.3   N/A      4,790 3,713 3,716 3,531                 N/A       1.86     1.02          1.02   2.03
   7-Jun-04   DRY      N/A     N/A     N/A   N/A   N/A   24.2   26.0     26.0   24.9   N/A   1.2      1.3     1.3     1.4   N/A    6.93    6.50   6.56   6.51   N/A      4.1    3.0     3.4     3.8   N/A      5,940 5,730 5,770 4,273                 N/A       1.22     0.29          0.29   0.32
   8-Jun-04   DRY      CLR     CLR     CLR   CLR   N/A   23.6   23.7     24.2   24.5   N/A   1.7      1.5     1.7     1.7   N/A    6.86    6.52   6.45   6.71   N/A      5.7    5.0     4.9     2.7   N/A      9,340 8,270 8,670 8,030                 N/A       1.61     0.71          1.06   0.49
   9-Jun-04   DRY      CLR     CLR     CLR   CLR   N/A   25.9   25.5     25.7   24.7   N/A   1.2      1.1     1.5     1.7   N/A    6.98    6.62   6.52   6.72   N/A      4.3    4.1     5.4     5.4   N/A      5,550 4,362 4,348 3,049                 N/A       1.25     0.19          0.23   0.23
 10-Jun-04    DRY      CLR     CLR     CLR   CLR   N/A   25.7   26.8     27.3   26.7   N/A   1.1      1.2     0.8     1.1   N/A    6.84    6.42   6.35   6.36   N/A      5.0    3.6     3.6     4.7   N/A      4,438 3,661 3,687 3,718                 N/A       0.77     0.31          0.37   0.53
 11-Jun-04    DRY      CLR     CLR     CLR   CLR   N/A   26.2   26.2     26.2   25.7   N/A   1.5      0.9     1.6     1.9   N/A    6.80    6.50   6.41   6.37   N/A      4.1    4.0     4.4     3.6   N/A      5,010 3,627 3,672 4,176                 N/A       1.45     0.89          1.75   0.69
 12-Jun-04    DRY      N/A     N/A     N/A   N/A   N/A   27.5   25.2     24.5   24.9   N/A   1.0      1.2     1.2     1.3   N/A    6.68    6.34   6.28   6.40   N/A      4.2    4.7     5.1     4.2   N/A      5,480 4,550 4,641 5,450                 N/A       3.29     2.70          2.57   4.54
 13-Jun-04    DRY      N/A     N/A     N/A   N/A   N/A   26.0   27.0     27.4   25.7   N/A   1.0      1.2     1.2     1.2   N/A    6.77    6.49   6.43   6.18   N/A      4.8    3.0     3.1     2.6   N/A      6,370 4,940 4,920 5,400                 N/A       5.43     3.16          3.06   3.89
 14-Jun-04    DRY      N/S     N/A     N/A   N/A   N/A   N/A    24.5     24.3   22.5   N/A   N/A     25.8    35.0    10.3   N/A    N/A     6.75   6.76   6.96   N/A     N/A     2.8     2.8     3.2   N/A       N/A     4,163 4,186 3,005              N/A       2.05     2.15          2.11   0.84
 15-Jun-04    DRY      CLR     CLR     CLR   CLR   N/A   25.6   24.9     25.0   24.3   N/A   2.6      1.8     1.9     7.1   N/A    6.81    6.68   6.61   6.86   N/A      4.6    4.1     3.8     2.9   N/A      6,370 5,540 5,510 4,517                 N/A       2.69     1.19          1.20   1.56
 16-Jun-04    DRY      CLR     CLR     CLR   CLR   N/A   26.0   25.1     25.3   25.0   N/A   2.7      1.5     1.7     1.9   N/A    6.98    6.63   6.52   6.80   N/A      4.7    4.6     3.9     7.4   N/A      4,843 5,090 5,100 3,059                 N/A       0.68     0.70          0.75   0.65

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                                                                                                                                                   Table 3
                                                                                                                                    Daily Water Quality Monitoring Results
                                                                                                                                         Emergency Order No. 02-1054
                                                                                                                                      Piney Point Phosphates Complex

Parameter                Visual Observations                          Temperature (oC)                          Turbidity NTU)                      pH (Standard Units)                Dissolved Oxygen (mg/L)              Specific Conductance (µs/cm)                               Ammonia
Station        X-1       003    BR/41    X-2      AR       X-1      003   BR/41     X-2        AR      X-1   003    BR/41    X-2      AR    X-1     003    BR/41   X-2     AR    X-1     003    BR/41    X-2     AR     X-1      003   BR/41    X-2      AR           X-1       003     BR/41          X-2     AR
 17-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      26.7   26.6     26.3      25.8     N/A   2.6     1.5      1.5     1.5   N/A     7.00    6.65   6.59   6.69   N/A      4.9    4.2     4.1     4.8    N/A     5,080 3,769 3,782 3,214               N/A       0.77     1.10          1.08   0.54
 18-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      25.6   25.5     26.4      25.4     N/A   2.1     1.1      0.8     1.5   N/A     6.95    6.84   6.73   6.72   N/A      4.8    3.6     3.9     4.4    N/A     5,110 3,820 2,711 3,260               N/A       0.52     0.33          0.31   0.59
 19-Jun-04     DRY       N/A     N/A     N/A      N/A      N/A      25.8   25.3     25.4      25.3     N/A   1.0     1.2      1.2     1.0   N/A     6.90    6.77   6.85   6.81   N/A      5.0    4.5     4.3     4.3    N/A     4,240 3,426 3,483 3,265               N/A       0.72     0.79          0.90   0.72
 20-Jun-04     DRY       N/A     N/A     N/A      N/A      N/A      26.0   25.8     25.9      26.8     N/A   1.0     1.3      1.4     1.2   N/A     7.04    6.77   6.81   6.85   N/A      6.1    5.1     4.6     3.9    N/A     8,350 4,104 4,195 2,774               N/A       0.46     1.52          1.78   0.85
 21-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      27.7   26.0     27.3      26.8     N/A   1.2     1.2      1.3     1.3   N/A     6.75    6.71   6.75   6.84   N/A      5.2    5.6     5.5     3.6    N/A     5,380 4,211 4,296 4,056               N/A       1.19     0.93          0.93   0.84
 22-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      27.6   26.9     27.4      26.8     N/A   1.1     0.8      1.5     1.7   N/A     7.04    6.93   6.79   6.79   N/A      4.3    3.8     4.5     4.3    N/A     5,760 3,305 3,271 3,245               N/A       9.16     1.28          1.36   0.71
 23-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      25.9   27.0     27.0      26.7     N/A   0.8     6.6      1.0     2.0   N/A     7.23    6.85   6.78   6.72   N/A      4.3    4.0     4.6     4.0    N/A     3,507 3,548 3,578 3,568               N/A       2.83     3.00          2.95   1.90
 24-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      27.3   26.1     27.2      25.9     N/A   0.8     0.5      0.6     1.1   N/A     6.90    6.79   6.68   6.64   N/A      4.3    4.1     4.6     4.3    N/A     4,095 2,987 2,971 2,982               N/A       2.62     2.32          2.33   2.19
 25-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      26.4   25.4     27.3      26.7     N/A   0.7     0.5      1.1     1.4   N/A     6.98    6.83   6.68   6.59   N/A      3.5    3.6     4.7     4.0    N/A     3,623 3,014 3,012 3,037               N/A       2.15     1.94          2.00   2.01
 26-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      27.8   26.0     27.2      26.9     N/A   1.2     1.3      1.2     1.2   N/A     6.89    6.95   6.84   6.73   N/A      4.4    5.2     4.4     2.6    N/A     4,017 3,275 3,248 3,431               N/A       1.31     1.45          1.44   1.19
 27-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      27.7   24.9     26.5      24.9     N/A   1.0     1.3      1.3     1.2   N/A     6.96    6.58   6.58   6.49   N/A      5.1    4.1     3.4     2.5    N/A     2,844 2,077 2,067 3,193               N/A       1.32     1.31          0.56   1.25
 28-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      26.9   26.5     26.9      26.0     N/A   1.0     1.2      1.3     1.3   N/A     6.95    6.54   6.53   6.61   N/A      5.0    3.9     3.7     3.9    N/A     4,058 3,669 3,637 3,338               N/A       0.76     0.23          0.26   0.46
 29-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      26.7   26.1     26.4      25.9     N/A   1.2     0.8      0.8     1.8   N/A     6.94    6.65   6.58   6.57   N/A      4.5    4.1     5.7     4.3    N/A     3,812 2,987 2,990 2,912               N/A       0.45     0.26          0.23   0.24
 30-Jun-04     DRY       CLR     CLR     CLR      CLR      N/A      25.0   25.1     25.4      25.3     N/A   1.1     0.6      1.4     1.5   N/A     6.98    6.73   6.64   6.62   N/A      4.7    4.2     4.3     4.5    N/A     4,024 3,634 3,632 3,441               N/A       0.25     0.10          0.10   0.13
   1-Jul-04    DRY       CLR     CLR     CLR      CLR      N/A      26.2   25.6     25.6      26.2     N/A   1.1     0.6      0.7     1.5   N/A     7.19    6.93   6.77   6.73   N/A      5.0    4.1     4.7     4.8    N/A     4,004 3,469 3,458 3,308               N/A       0.43     0.43          0.41   0.26
   2-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      27.5   26.5     26.4      24.7     N/A   1.2     1.2      1.2     1.3   N/A     6.94    6.60   6.59   6.80   N/A      4.9    4.1     3.6     2.3    N/A     5,590 4,870 4,860 5,540               N/A       0.63     0.32          0.32   0.39
   3-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      24.6   26.0     N/A       25.4     N/A   1.0     1.2      1.2     1.2   N/A     6.60    6.40   6.53   6.65   N/A      4.8    4.6     4.8     4.8    N/A     9,230 5,200 5,100 4,594               N/A       0.69     1.01          0.92   0.47
   4-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      26.4   26.2     26.0      25.8     N/A   1.0     1.2      1.2     1.3   N/A     6.81    6.46   6.51   6.64   N/A      3.8    4.4     4.0     3.4    N/A     4,930 5,120 5,080 4,840               N/A       0.67     2.00          0.56   0.47
   5-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      28.6   25.4     27.5      25.2     N/A   1.0     1.2      1.3     1.3   N/A     7.18    6.88   6.93   6.79   N/A      4.2    3.3     4.2     3.9    N/A     4,308 4,808 4,830 4,660               N/A       0.29     0.12          0.12   0.19
   6-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      25.9   25.5     25.1      25.5     N/A   1.2     1.3      1.6     1.6   N/A     6.24    6.69   6.80   6.86   N/A      9.7    9.5     9.4     9.6    N/A     4,058 4,291 4,140 5,210               N/A       0.32     0.19          0.28   0.47
   7-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      23.9   25.9     25.8      25.8     N/A   1.5     1.2      1.1     1.4   N/A     6.10    6.31   6.38   6.49   N/A      7.0    5.8     5.7     5.6    N/A     4,866 2,584 5,330 2,502               N/A       1.02     1.94          2.07   1.23
   8-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      22.2   22.7     23.1      23.6     N/A   1.1     1.2      1.2     1.8   N/A     6.76    6.67   6.63   6.70   N/A      6.5    5.0     5.6     5.2    N/A     4,255 3,418 3,718 4,220               N/A       4.73     5.10          4.96   4.52
   9-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      23.3   25.1     24.4      29.2     N/A   2.9     0.9      1.0     1.2   N/A     6.60    6.57   6.50   6.51   N/A      6.7    5.6     6.2     5.6    N/A     9,730 3,574 3,363 5,940               N/A       4.61     5.37          6.95   4.17
  10-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      25.4   25.2     25.6      25.6     N/A   1.0     1.2      1.2     1.3   N/A     6.97    6.46   6.67   6.81   N/A      4.6    4.1     4.6     5.4    N/A    10,010 9,930 9,990 9,320               N/A       7.23     8.90          8.09   5.64
  11-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      25.6   26.4     26.5      26.0     N/A   1.0     1.2      1.3     1.2   N/A     6.90    6.68   6.61   6.52   N/A      5.2    4.5     4.2     3.0    N/A     5,950 4,700 4,723 9,900               N/A       3.95     1.86          1.85   3.01
  12-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      25.2   24.7     25.0      N/A      N/A   1.0     1.2      1.3     1.2   N/A     6.83    6.48   6.54   6.51   N/A      4.0    4.7     4.2     4.4    N/A     5,420 6,350 6,350 6,320               N/A       1.03     0.78          0.70   0.89
  13-Jul-04    DRY       CLR     CLR     CLR      CLR      N/A      25.4   24.7     25.4      25.8     N/A   1.2     0.6      0.6     1.6   N/A     6.83    6.62   6.50   6.62   N/A      4.9    4.0     5.2     5.0    N/A     5,630 6,350 6,420 5,900               N/A       0.74     1.45          1.50   0.26
  14-Jul-04    DRY       CLR     CLR     CLR      CLR      N/A      25.4   25.0     25.9      26.2     N/A   1.4     0.7      0.8     1.2   N/A     6.83    6.57   6.48   6.48   N/A      5.0    4.4     4.6     4.1    N/A     6,320 6,300 6,310 6,350               N/A       1.17     4.23          3.86   1.74
  15-Jul-04    DRY       CLR     CLR     CLR      CLR      N/A      25.9   25.7     25.5      26.1     N/A   1.5     0.8      0.8     1.6   N/A     6.90    6.60   6.53   6.48   N/A      4.5    4.1     3.9     4.0    N/A     6,580 6,750 6,830 9,450               N/A       8.12     7.26          7.09   7.32
  16-Jul-04    DRY       CLR     CLR     CLR      CLR      N/A      25.9   24.4     25.2      25.6     N/A   1.3     0.9      1.0     2.1   N/A     6.71    6.47   6.43   6.50   N/A      4.6    4.6     4.6     4.5    N/A     5,880 6,460 6,500 9,380               N/A      10.50     7.84          7.94   8.95
  17-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      25.7   25.4     25.4      25.0     N/A   1.2     1.4      1.3     1.3   N/A     6.84    6.46   6.63   6.61   N/A      4.4    2.4     3.6     2.9    N/A     5,810 6,020 6,040 5,920               N/A       6.83     7.66          7.54   6.23
  18-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      26.3   N/A      25.6      25.8     N/A   1.0     1.0      1.2     1.2   N/A     6.85    6.53   6.54   6.57   N/A      4.1    3.9     4.0     4.8    N/A     5,740 5,930 5,970 5,810               N/A       5.09     5.53          5.30   4.99
  19-Jul-04    DRY       N/A     N/A     N/A      N/A      N/A      25.3   25.6     27.6      26.5     N/A   1.8     0.6      0.7     2.9   N/A     6.94    7.02   6.97   6.96   N/A      5.4    4.7     4.8     4.1    N/A     5,260 2,742 5,720 5,220               N/A       3.74     2.19          2.27   1.86
  20-Jul-04    CLR       CLR     CLR     CLR      CLR      24.1     24.7   24.9     25.0      24.5     3.7   1.7     0.6      0.7     4.1   7.33    7.16    6.81   6.69   6.87   4.8      4.5    4.2     4.2     5.1   1,110 5,150 5,080 5,070 4,510                  3.01      1.01     0.83          0.82   0.75
  21-Jul-04    CLR       CLR     CLR     CLR      CLR      23.5     24.1   24.2     24.3      24.1     3.1   1.4     2.3      2.9     9.8   7.26    7.17    6.97   6.92   7.01   4.9      4.3    4.3     5.7     5.2   1,257 4,710 3,665 3,630 2,949                  0.38      1.36     1.64          1.60   1.42
  22-Jul-04    CLR       CLR     CLR     CLR      CLR      24.9     26.5   25.1     25.9      25.4     1.2   1.5     1.8      1.7     4.4   7.24    7.12    6.97   6.90   6.99   4.1      4.2    4.2     4.5     4.8   1,307 4,564 4,276 4,308 3,620                 0.297      0.58     1.17          1.19   0.78
  23-Jul-04    CLR       CLR     CLR     CLR      CLR      24.4     23.6   25.0     26.2      25.6     0.7   1.8     1.2      1.3     3.6   7.33    7.12    6.93   6.79   6.99   4.4      4.1    4.5     4.7     4.7   1,245 4,249 4,347 4,339 3,994                  2.08      0.75     0.73          0.72   0.89
  24-Jul-04    N/A       N/A     N/A     N/A      N/A      25.0     26.1   26.1     28.9      25.5     3.1   1.0     1.2      1.2     1.3   7.33    6.86    6.99   6.93   7.14   3.8      4.8    4.1     4.1     4.0   1,252 4,653 4,361 4,387 3,885                  6.76      0.45     0.98          0.97   0.55
  25-Jul-04    N/A       N/A     N/A     N/A      N/A      24.7     26.3   25.7     25.9      24.8     3.4   1.0     1.2      1.3     1.2   7.37    7.13    6.95   7.02   7.13   4.6      3.9    3.6     4.0     3.3   1,478 4,470 4,438 4,524 4,172                  7.24      0.77     0.98          0.97   0.78
  26-Jul-04    N/A       N/A     N/A     N/A      N/A      25.2     26.9   24.9     26.0      25.8     2.6   1.3     1.3      1.5     1.4   6.96    6.91    6.85   6.83   6.87   4.7      5.3    4.8     4.1     3.9    986     4,065 3,172 3,146 2,619              0.716      0.34     0.78          0.79   0.25
  27-Jul-04    CLR       CLR     CLR     CLR      CLR      24.7     25.6   24.8     25.5      25.3     0.7   1.6     1.2      1.7     3.8   7.17    7.03    6.94   6.93   7.03   4.2      4.0    4.2     4.8     4.0   1,188 4,341 4,192 4,173 3,386                  1.26      0.26     0.81          0.81   0.64
  28-Jul-04    CLR       CLR     CLR     CLR      CLR      24.9     26.3   25.5     25.2      25.4     1.3   2.1     1.2      1.2    16.7   7.05    6.99    6.89   6.89   7.07   4.2      4.3    3.8     5.3     4.3   1,223 4,453 5,880 6,030 3,085                  1.93      1.01     2.69          2.80   1.15
  29-Jul-04    CLR       CLR     CLR     CLR      CLR      24.4     26.2   25.2     25.8      25.2     2.0   1.4     1.2      1.3     3.1   7.14    7.12    6.99   6.99   6.99   4.7      4.4    4.7     4.9     4.2   1,193 4,035 3,767 3,793 3,381                   2.7      0.92     2.40          2.35   1.61
  30-Jul-04    CLR       CLR     CLR     CLR      CLR      24.9     26.2   25.5     26.1      25.7     1.1   1.6     0.9      1.3     3.7    7.1    7.15    7.04   7.01   7.05   4.5      4.0    4.2     4.7     4.6   1,249 4,268 4,589 4,667 3,704                  2.32      0.95     1.97          1.93   1.25
  31-Jul-04    N/A       N/A     N/A     N/A      N/A      24.9     26.5   25.8     26.2      25.4     2.8   1.3     1.2      1.2     1.3   7.07    6.98    6.95   7.08   7.01   4.0      5.0    4.5     4.9     2.8   1,256 4,514 4,193 4,301 3,742                  2.75      0.26     0.74          0.70   0.40


Notes:        X-1 = Upstream background station in the Buckeye Road ditch (south side).
              003 = Discharge outfall.
              BR/41 = Downstream station in the Buckeye Road ditch (north side) east of U.S. 41.
              X-2 = Downstream station in the US 41 ditch (west side) where the Buckeye Road ditch joins.
              AR = Downstream station in the CSX Railroad ditch at Armstrong Road (south side).
              DRY = Not sampled due to absence of flow.
              CLR = Clear.
              DW = Duckweed cover present.
              DF = Dead fish.

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                                                                                                                                        Table 3
                                                                                                                         Daily Water Quality Monitoring Results
                                                                                                                              Emergency Order No. 02-1054
                                                                                                                           Piney Point Phosphates Complex

Parameter               Visual Observations                          Temperature (oC)                 Turbidity NTU)                    pH (Standard Units)              Dissolved Oxygen (mg/L)              Specific Conductance (µs/cm)                                Ammonia
Station        X-1      003    BR/41     X-2      AR      X-1      003     BR/41   X-2   AR   X-1   003   BR/41    X-2     AR    X-1    003    BR/41   X-2    AR   X-1     003    BR/41    X-2     AR   X-1       003    BR/41    X-2      AR            X-1       003     BR/41  X-2     AR
            HERB = Odor of herbicide present.
            TUR = Turbid.
            N/S - No Sample due to no discharge
            * - No discharge through Outfall 003. Sample obtained from ditch.




              Printed On: 11/22/2011                                                                                                   Page 17 of 30                                                                    C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                          Table 4
                                                              Weekly Water Quality Analyses
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex


                                               Date          January 8, 2004                   January 15, 2004                      January 22, 2004
                                             Station   X-1        003           X-2      X-1         003        X-2            X-1         003        X-2
       Parameters
       pH (standard units)                             DRY        6.55           6.65    DRY         6.54         6.65        7.36          6.83         6.70
       Specific Conductance (µs/cm)                    DRY       4,738          4,677    DRY        4,606        4,333       1,589         4,707        4,565
       Temperature (oC)                                DRY       12.60          12.70    DRY        14.40        14.90        11.6         13.20        14.50
       Turbidity (NTU)                                 DRY        1.10           0.90    DRY         0.30         0.80        4.90          0.40         1.10
       Dissolved Oxygen (mg/L)                         DRY        6.55           6.65    DRY         6.54         6.65        8.60          8.20         7.30
       Ammonia as N (mg/L)                             DRY        10.2           10.5    DRY         34.5         32.1        14.8          17.5         15.1
       Ammonia, Unionized (mg/L)                       DRY       0.014         0.0228    DRY       0.0473       0.0553       0.160        0.0191       0.0412
       Total Kjeldahl Nitrogen as N (mg/L)             DRY        14.3           13.6    DRY         35.3         36.8        14.9          18.1         15.2
       Nitrate + Nitrite (mg/L)                        DRY        1.04          0.936    DRY        0.544        0.480        1.67          1.34         1.04
       Total Nitrogen (mg/L)                           DRY        15.3           14.5    DRY         35.8         37.3        16.6          19.4         16.2
       Total Phosphorus (mg/L)                         DRY        0.34           0.41    DRY         0.43         0.42        18.1          0.37         0.32
       Fluoride (mg/L)                                 DRY        1.03          0.820    DRY         1.02         1.14       0.606         0.925        0.960
       Total Suspended Solids (mg/L)                   DRY       <1.0           <1.0     DRY        <1.0         <1.0         7.20          2.00         2.00




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                   Page 18 of 30               C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                              Table 4
                                                                  Weekly Water Quality Analyses
                                                                   Emergency Order No. 02-1054
                                                                 Piney Point Phosphates Complex


                                               Date             January 29, 2004                      February 5, 2004                     February 12, 2004
                                             Station    X-1           003        X-2          X-1           003        X-2           X-1         003         X-2
       Parameters
       pH (standard units)                               6.67         6.71        6.76         6.85         6.91        6.95         6.94         6.71         6.58
       Specific Conductance (µs/cm)                     1,540        2,918       2,535        1,636        4,453       4,185        1,645        3,597        3,653
       Temperature (oC)                                  16.3        14.50       14.70         16.3        19.00       18.90         18.5        20.60        20.50
       Turbidity (NTU)                                   3.10         0.90        1.00         1.90         1.10        0.60         1.90         0.50         1.20
       Dissolved Oxygen (mg/L)                           8.30         8.00        7.10         6.20         6.70        6.40         5.90         5.80         5.80
       Ammonia as N (mg/L)                               7.98         6.07         5.9         13.6          8.6        10.4         18.0         15.7         12.4
       Ammonia, Unionized (mg/L)                       0.0346       0.0105      0.0799       0.0294       0.0118       0.014       0.0588       0.0341       0.0275
       Total Kjeldahl Nitrogen as N (mg/L)               8.85         6.32        6.54         14.4         9.69        11.2         18.0         19.6         17.0
       Nitrate + Nitrite (mg/L)                          1.15         1.17        2.48         4.54        0.915        2.07         6.54        0.493         1.35
       Total Nitrogen (mg/L)                             10.0         7.49        9.02         18.9         10.6        13.3         24.5         20.1         18.3
       Total Phosphorus (mg/L)                           12.5         0.56        0.96         23.1         0.60        7.01         28.5         1.02         1.32
       Fluoride (mg/L)                                  0.558        0.847       0.927        0.833        0.813       1.280        0.703        0.827        0.813
       Total Suspended Solids (mg/L)                     2.80         1.80        2.40          7.2         2.80        2.80         12.0         3.40         1.20




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                       Page 19 of 30                 C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                             Table 4
                                                                 Weekly Water Quality Analyses
                                                                  Emergency Order No. 02-1054
                                                                Piney Point Phosphates Complex


                                               Date            February 19, 2004                   February 26, 2004                      March 4, 2004
                                             Station   X-1           003         X-2         X-1         003         X-2           X-1        003           X-2
       Parameters
       pH (standard units)                              6.99         6.85        6.70         6.88       6.73         6.83         6.86         6.70         6.61
       Specific Conductance (µs/cm)                    1,626        4,128       4,001        1,157      4,136        2,948        1,439        5,350        4,189
       Temperature (oC)                                 11.3        13.60       13.40         19.4      19.70        19.80         18.3        19.70        20.10
       Turbidity (NTU)                                  4.20         1.00        0.70         7.40       1.50         1.90         7.90         0.30         0.80
       Dissolved Oxygen (mg/L)                         13.60        11.40       15.10         6.40       5.80         5.40         6.50         6.40         6.60
       Ammonia as N (mg/L)                              12.8         12.7        15.2         4.10       6.95         4.37         14.9         6.62         5.40
       Ammonia, Unionized (mg/L)                       0.035        0.011      0.0166       0.0145      0.015       0.0118       0.0716       0.0114       0.0151
       Total Kjeldahl Nitrogen as N (mg/L)              13.4         12.9        15.5         4.31       7.11         5.98         15.8         7.40         5.60
       Nitrate + Nitrite (mg/L)                         3.41         1.90        1.50        0.663       1.74         2.19         4.19        0.799         1.33
       Total Nitrogen (mg/L)                            16.8         14.8        17.0         4.97       8.85         8.17         20.0         8.20         6.93
       Total Phosphorus (mg/L)                          20.3         0.80        0.73         6.64       0.40         1.48         27.9         0.25         0.78
       Fluoride (mg/L)                                 0.533        0.728       0.805        0.520       1.17         1.00        0.927        0.672        0.806
       Total Suspended Solids (mg/L)                    7.60         8.60       <1.0          7.20       7.80         3.20         7.60         6.40         2.20




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                      Page 20 of 30                C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                             Table 4
                                                                 Weekly Water Quality Analyses
                                                                  Emergency Order No. 02-1054
                                                                Piney Point Phosphates Complex


                                               Date             March 11, 2004                        March 18, 2004                       March 25, 2004
                                             Station    X-1          003          X-2         X-1          003          X-2          X-1        003           X-2
       Parameters
       pH (standard units)                               7.16        6.77          6.72        6.84        6.67          6.62       N/A          6.67         6.55
       Specific Conductance (µs/cm)                     1,178       4,668         3,502       1,509       4,855         3,820       N/A         4,298        3,434
       Temperature (oC)                                 13.90       15.60         15.60       16.70       18.70         19.00       N/A         17.50        18.50
       Turbidity (NTU)                                  11.70        0.90          1.00        6.40        1.30          1.50       N/A          1.10         0.90
       Dissolved Oxygen (mg/L)                           8.80        8.10          7.90        7.70        6.10          5.70       N/A          7.00         6.00
       Ammonia as N (mg/L)                               9.63        6.67          7.38        12.6        10.4          8.21       N/A          4.39         3.00
       Ammonia, Unionized (mg/L)                       0.0417      0.00578       0.0235      0.0396      0.0199        0.0278       N/A        0.00666      0.00473
       Total Kjeldahl Nitrogen as N (mg/L)               19.2        12.5          16.1        17.9        13.7          11.5       N/A          5.64         4.16
       Nitrate + Nitrite (mg/L)                          3.59        1.34          1.08        2.28       0.963          1.31       N/A         0.689        0.843
       Total Nitrogen (mg/L)                             22.8        13.8          17.2        20.2        14.7          12.8       N/A          6.33         5.00
       Total Phosphorus (mg/L)                           23.8        0.40          0.95        19.5        0.21          0.46       N/A          0.39         0.35
       Fluoride (mg/L)                                   1.25       0.714         0.904       0.707       0.755         0.743       N/A         0.668        0.713
       Total Suspended Solids (mg/L)                     51.4         <1           1.00        17.2        3.20          3.40       N/A          1.60         1.80




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                       Page 21 of 30                 C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                          Table 4
                                                              Weekly Water Quality Analyses
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex


                                               Date          April 8, 2004                        April 15, 2004                        April 22, 2004
                                             Station   X-1       003          X-2         X-1          003           X-2         X-1         003          X-2
       Parameters
       pH (standard units)                             N/A        6.65        6.64         6.97        6.84          6.73       N/A           6.84        6.52
       Specific Conductance (µs/cm)                    N/A       5,250       3,676        1,457       5,350         4,187       N/A          3,774       3,713
       Temperature (oC)                                N/A       21.60       21.80        15.30       16.30         16.70       N/A          21.70       21.00
       Turbidity (NTU)                                 N/A        0.40        0.50         2.90        1.20          0.90       N/A           0.80        0.90
       Dissolved Oxygen (mg/L)                         N/A        7.10        5.50         7.80        7.70          6.50       N/A           6.10        5.40
       Ammonia as N (mg/L)                             N/A        5.16        6.53          1.0        4.41          3.29       N/A           5.33        5.40
       Ammonia, Unionized (mg/L)                       N/A      0.0118       0.142       0.0298      0.00846       0.00631      N/A         0.0118       0.012
       Total Kjeldahl Nitrogen as N (mg/L)             N/A        8.28        12.1         4.28        4.67          4.41       N/A           5.45        5.56
       Nitrate + Nitrite (mg/L)                        N/A        1.33        1.14         1.08        3.13          2.75       N/A           1.66        1.53
       Total Nitrogen (mg/L)                           N/A        9.61        13.2         5.36        7.80          7.16       N/A           7.11        7.09
       Total Phosphorus (mg/L)                         N/A        0.32        0.17         0.47        0.26          0.47       N/A           0.23        0.27
       Fluoride (mg/L)                                 N/A       1.620       1.840        0.695        1.59          1.80       N/A           1.83        1.14
       Total Suspended Solids (mg/L)                   N/A        2.60        2.40         12.4        1.60          2.80       N/A           2.40        2.20




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                   Page 22 of 30                 C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                          Table 4
                                                              Weekly Water Quality Analyses
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex


                                               Date          April 29, 2004                    May 6, 2004                         May 13, 2004
                                             Station   X-1        003         X-2        X-1      003          X-2          X-1        003           X-2
       Parameters
       pH (standard units)                             N/A        6.88         6.77      N/A      6.82         6.74        N/A           7.25         7.06
       Specific Conductance (µs/cm)                    N/A       5,430        4,097      N/A     2,773        2,131        N/A          5,560        4,155
       Temperature (oC)                                N/A       21.80        22.10      N/A      23.6         21.8        N/A           23.6         23.4
       Turbidity (NTU)                                 N/A        0.60         0.90      N/A      0.60         1.10        N/A           1.00         1.30
       Dissolved Oxygen (mg/L)                         N/A        6.20         4.80      N/A      5.30         5.20        N/A           4.40         4.90
       Ammonia as N (mg/L)                             N/A        2.81         7.28      N/A      1.43         0.82        N/A           0.08         0.02
       Ammonia, Unionized (mg/L)                       N/A      0.0133        0.111      N/A    0.00493      0.00487       N/A         <0.001       <0.001
       Total Kjeldahl Nitrogen as N (mg/L)             N/A        5.21         8.12      N/A      1.59         1.17        N/A           1.72         0.39
       Nitrate + Nitrite (mg/L)                        N/A        1.05         1.28      N/A      1.47        0.924        N/A           1.54        0.752
       Total Nitrogen (mg/L)                           N/A        6.26         9.40      N/A      3.06         2.09        N/A           3.26         1.14
       Total Phosphorus (mg/L)                         N/A        0.25         0.27      N/A      0.27         0.31        N/A           0.28         0.31
       Fluoride (mg/L)                                 N/A        2.02         2.56      N/A      2.05         2.30        N/A           1.91         3.84
       Total Suspended Solids (mg/L)                   N/A        3.00         2.40      N/A      2.40         1.00        N/A           2.80         2.20




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                   Page 23 of 30            C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                          Table 4
                                                              Weekly Water Quality Analyses
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex


                                               Date          May 20, 2004                      May 27, 2004                         June 3, 2004
                                             Station   X-1       003          X-2        X-1       003          X-2          X-1        003           X-2
       Parameters
       pH (standard units)                             N/A       6.87         6.54       N/A       7.28         6.30        N/A          6.80         6.08
       Specific Conductance (µs/cm)                    N/A      5,210        4,766       N/A       130         1,785        N/A         4,880        4,467
       Temperature (oC)                                N/A       24.6         24.4       N/A       27.6         25.8        N/A         27.00        26.80
       Turbidity (NTU)                                 N/A       0.80         1.20       N/A       1.10         1.30        N/A          0.90         0.90
       Dissolved Oxygen (mg/L)                         N/A       4.80         4.00       N/A       4.50         4.40        N/A          4.30         3.40
       Ammonia as N (mg/L)                             N/A       0.75         0.61       N/A       0.39       <0.01         N/A          7.03         2.43
       Ammonia, Unionized (mg/L)                       N/A     0.00205      0.00179      N/A     0.00937      <0.001        N/A        0.00766      0.00279
       Total Kjeldahl Nitrogen as N (mg/L)             N/A       2.02         1.73       N/A       0.97         0.58        N/A          7.46         2.63
       Nitrate + Nitrite (mg/L)                        N/A       1.30         1.42       N/A      0.116        0.947        N/A          3.24         3.43
       Total Nitrogen (mg/L)                           N/A       3.32         3.15       N/A       1.09         1.53        N/A          10.7         6.06
       Total Phosphorus (mg/L)                         N/A       0.22         0.36       N/A       0.20         0.61        N/A          0.12         0.19
       Fluoride (mg/L)                                 N/A       1.84         1.47       N/A       1.27         4.26        N/A          1.58         2.19
       Total Suspended Solids (mg/L)                   N/A       3.00         12.0       N/A       <1.0         1.60        N/A          4.00         3.60




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                   Page 24 of 30             C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                          Table 4
                                                              Weekly Water Quality Analyses
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex


                                               Date          June 10, 2004                     June 18, 2004                        June 25, 2004
                                             Station   X-1       003          X-2        X-1       003           X-2         X-1        003           X-2
       Parameters
       pH (standard units)                             N/A       6.84          6.35      N/A       6.95          6.73       N/A           6.98        6.68
       Specific Conductance (µs/cm)                    N/A      4,438         3,687      N/A      5,110         2,711       N/A          3,623       3,012
       Temperature (oC)                                N/A      25.70         27.30      N/A      25.60         26.40       N/A          26.40       27.30
       Turbidity (NTU)                                 N/A       1.10          0.80      N/A       2.10          0.80       N/A           0.70        1.10
       Dissolved Oxygen (mg/L)                         N/A       5.00          3.60      N/A       4.80          3.90       N/A           3.50        4.70
       Ammonia as N (mg/L)                             N/A       0.83          0.26      N/A       0.60          0.33       N/A           5.35        1.64
       Ammonia, Unionized (mg/L)                       N/A     0.00180       <0.001      N/A     0.00130       0.00141      N/A         0.0267      0.00774
       Total Kjeldahl Nitrogen as N (mg/L)             N/A       1.14          0.64      N/A       2.08          1.43       N/A           6.02        2.34
       Nitrate + Nitrite (mg/L)                        N/A       2.26          1.98      N/A       1.60          1.44       N/A           1.68        1.94
       Total Nitrogen (mg/L)                           N/A       3.40          2.62      N/A       3.68          2.87       N/A           7.70        4.28
       Total Phosphorus (mg/L)                         N/A       0.17          0.16      N/A       0.17          0.20       N/A           0.32        0.30
       Fluoride (mg/L)                                 N/A       1.81          1.91      N/A       1.92          1.99       N/A           1.82        3.07
       Total Suspended Solids (mg/L)                   N/A       3.20          4.80      N/A       6.80          4.00       N/A           6.40        2.80




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                   Page 25 of 30             C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                          Table 4
                                                              Weekly Water Quality Analyses
                                                               Emergency Order No. 02-1054
                                                             Piney Point Phosphates Complex


                                               Date          July 1, 2004                      July 9, 2004                         July 15, 2004
                                             Station   X-1       003          X-2        X-1       003          X-2          X-1         003          X-2
       Parameters
       pH (standard units)                             N/A       7.19         6.77       N/A       6.60         6.50        N/A          6.90          6.53
       Specific Conductance (µs/cm)                    N/A      4,004        3,458       N/A      9,730        3,363        N/A         6,580         6,830
       Temperature (oC)                                N/A      26.20        25.60       N/A      23.30        24.40        N/A         25.90         25.50
       Turbidity (NTU)                                 N/A       1.10         0.70       N/A       2.90         1.00        N/A          1.50          0.80
       Dissolved Oxygen (mg/L)                         N/A       5.00         4.70       N/A       6.70         6.20        N/A          4.50          3.90
       Ammonia as N (mg/L)                             N/A       0.56         0.05       N/A       8.15         5.39        N/A          7.32          7.53
       Ammonia, Unionized (mg/L)                       N/A     0.00193      <0.001       N/A      0.232       0.00779       N/A        0.00504       0.0128
       Total Kjeldahl Nitrogen as N (mg/L)             N/A       1.90         1.45       N/A       9.19         6.53        N/A          8.03          8.16
       Nitrate + Nitrite (mg/L)                        N/A       1.84         2.21       N/A       3.58         3.53        N/A          5.18          3.06
       Total Nitrogen (mg/L)                           N/A       3.74         3.66       N/A       12.8         10.1        N/A          13.2          11.2
       Total Phosphorus (mg/L)                         N/A       0.19         0.21       N/A       0.23         0.29        N/A          0.28          0.26
       Fluoride (mg/L)                                 N/A       1.84         1.91       N/A      0.295        0.567        N/A         0.391         0.616
       Total Suspended Solids (mg/L)                   N/A       2.60         3.20       N/A       6.00         3.00        N/A          10.0          5.60




       All analyses in milligrams per Liter unless
       noted.
       TBR - Sample collected and submitted to
       lab. Analyses not yet received.
       Dry - Not sampled due to absence of flow.
       ** - Values checked. Appears to be related
       to rainfall runoff
        N/S - Not Sampled
        *** - Discharged stopped prior to grab
        samples being obtained. Data from
        daily samples.




Printed On: 11/22/2011                                                   Page 26 of 30             C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                                             Table 4
                                                                 Weekly Water Quality Analyses
                                                                  Emergency Order No. 02-1054
                                                                Piney Point Phosphates Complex


                                                                 Date             July 23, 2004                           July 30, 2004
                                                               Station    X-1          003          X-2           X-1          003          X-2
                         Parameters
                         pH (standard units)                               7.33       7.12          6.79          4.50         4.00         4.70
                         Specific Conductance (µs/cm)                     1,245      4,249         4,339         1,249        4,268        4,667
                         Temperature (oC)                                 24.40      23.60         26.20         24.90        26.20        26.10
                         Turbidity (NTU)                                   0.70       1.80          1.30          1.10         1.60         1.30
                         Dissolved Oxygen (mg/L)                           4.40       4.10          4.70          4.50         4.00         4.70
                         Ammonia as N (mg/L)                               1.46       0.73          0.83          0.54         1.28         0.32
                         Ammonia, Unionized (mg/L)                       0.0327     0.00199       0.00679       0.00655      0.0189       0.00486
                         Total Kjeldahl Nitrogen as N (mg/L)               2.60       1.68          1.99          1.84         2.45         1.71
                         Nitrate + Nitrite (mg/L)                         0.957       3.01         0.765          2.81         2.26         3.34
                         Total Nitrogen (mg/L)                             3.56       4.69          2.75          4.65         4.71         5.05
                         Total Phosphorus (mg/L)                           3.76       0.26          0.56          3.46         0.18         0.47
                         Fluoride (mg/L)                                  0.638      0.905          1.11         0.762        0.658        0.856
                         Total Suspended Solids (mg/L)                     12.9       4.29          3.14          4.25         4.50         2.25




                         All analyses in milligrams per Liter unless
                         noted.
                         TBR - Sample collected and submitted to
                         lab. Analyses not yet received.
                         Dry - Not sampled due to absence of flow.
                         ** - Values checked. Appears to be related
                         to rainfall runoff
                         N/S - Not Sampled
                         *** - Discharged stopped prior to grab
                         samples being obtained. Data from
                         daily samples.




Printed On: 11/22/2011                                                     Page 27 of 30                    C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                             Table 5
                                                 Monthly Water Quality Analyses
                                                  Emergency Order No. 02-1054
                                                Piney Point Phosphates Complex
                                    Date                January-04                                     February-04
                                  Station     X-1        003               X-2            X-1           003                X-2
Parameters
Alkalinity (mg/L)                              123        15.5              32            92.0           18.0              34.0
Aluminum (mg/L)                              <0.19      <0.19            <0.19           0.401          <0.19             <0.19
Arsenic (µg/L)                                 2.01       4.87             4.52           1.02           3.25              2.46
Barium (mg/L)                               0.00693    0.00636          0.00447         0.0303         0.00977           0.00917
Beryllium (µg/L)                              <0.2       <0.2             <0.2            0.30           0.90              0.70
Biochemical Oxygen Demand (mg/L)                <2         <2              4.48           3.15            <2                <2
Cadmium (µg/L)                                 0.10       0.40             0.30           0.20           1.10              0.50
Calcium (mg/L)                                 289       1,048             957            277           1,176              783
Chemical Oxygen Demand (mg/L)                  41.0       22.9             21.7           92.5           40.7              52.0
Chloride (mg/L)                               240.0       95.0             68.6          210.0           91.2              75.2
Chromium (µg/L)                                 <1         <1               <1            3.50           1.50              1.10
Radium 226 (pCi/L)                              <1     1.2 ± 0.5          <0.9          1.4±0.6          <0.5              <0.6
Radium 228 (pCi/L)                              <1         <1               <1           <1.0            <1.0              <1.0
Copper (µg/L)                                   <1         <1               <1            21.4           1.30              3.20
Gross Alpha (pCi/L)                           <2.2     1.2 ± 0.3        2.2 ± 0.4       4.4±1.5        1.9±0.3           1.8±0.3
Iron (mg/L)                                   0.291       0.08            0.089          1.831          0.119             0.146
Lead (µg/L)                                     <1         <1               <1            9.60            2.4              43.7
Magnesium (mg/L)                               61.0       3.98             7.51           44.1           2.74              6.71
Manganese (mg/L)                             0.0359     0.0003           0.0055          0.056          0.018             0.012
Nickel (µg/L)                                <1.23        128               94            1.90           136               79.4
Potassium (mg/L)                               13.6       89.6             83.7           10.9           121               70.0
Selenium (µg/L)                                2.92     <2.04            <2.04           <2.04          <2.04             <2.04
Silica (mg/L)                                  9.32       2.51             3.86           10.3           2.55              3.33
Silver (µg/L)                                 <0.2       <0.2             <0.2            <10            <10               <10
Sulfate (mg/L)                                 449       2,516            2,688           358           3,061             1,953
Total Dissolved Solids (mg/L)                 1,152      3,840            3,408           884           4,332             2,808
Total Hardness (mg/L)                          602       1,335            1,193           460           1,391              923
Total Organic Carbon (mg/L)                    19.2      14.50            15.60           19.6           12.7              13.7
Zinc (µg/L)                                  <7.98        28.0           <7.98            23.0           31.0             <7.98
Color (PCU)                                     80         <5               15             90             <5                25

All analyses in milligrams per Liter
unless noted.

TBR - Sample collected and submitted
to lab. Analyses not yet received.
DRY = Not sampled due to absence of
flow.
* - Analysis being challenged.
< - Analyte not detected at the
J4 - Est value quality control criteria
for accuracy not met. Standard
J4* - Est value quality control
criteria for accuracy not met.
Q - Analyzed outside accepted hold
time




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                                                           Page 28C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                           Table 5
                                               Monthly Water Quality Analyses
                                                Emergency Order No. 02-1054
                                              Piney Point Phosphates Complex
                                    Date               March-04                                        April-04
                                  Station   X-1        003               X-2            X-1            003               X-2
Parameters
Alkalinity (mg/L)                           N/A         12.0             8.50           N/A             20.5              26
Aluminum (mg/L)                             N/A       <0.19            <0.19            N/A           <0.19            <0.19
Arsenic (µg/L)                              N/A          <1               <1            N/A             4.37             2.53
Barium (mg/L)                               N/A      0.00996          0.00821           N/A           0.0140           0.0111
Beryllium (µg/L)                            N/A        <0.2             <0.2            N/A            <0.2             <0.2
Biochemical Oxygen Demand (mg/L)            N/A         3.89             3.04           N/A             3.45              <2
Cadmium (µg/L)                              N/A        <0.1             <0.1            N/A             1.00             0.40
Calcium (mg/L)                              N/A         983              743            N/A            1,225             917
Chemical Oxygen Demand (mg/L)               N/A         <10              <10            N/A             25.7             31.3
Chloride (mg/L)                             N/A         82.0             64.4           N/A             97.4             79.6
Chromium (µg/L)                             N/A         1.60             1.30           N/A              <1               <1
Radium 226 (pCi/L)                          N/A        <0.4           0.4 ± 0.3         N/A            <0.6             <0.7
Radium 228 (pCi/L)                          N/A        <1.0             <1.0            N/A            <1.0             <1.0
Copper (µg/L)                               N/A          <1               <1            N/A             1.60             1.60
Gross Alpha (pCi/L)                         N/A      1.4 ± 0.3        1.1 ± 0.3         N/A          0.7 ± 0.2        2.1 ± 0.3
Iron (mg/L)                                 N/A        0.060            0.057           N/A            0.065            0.107
Lead (µg/L)                                 N/A          <1               <1            N/A              2.4              <1
Magnesium (mg/L)                            N/A         1.23             0.82           N/A             0.52             1.00
Manganese (mg/L)                            N/A       <0.010           <0.010           N/A            0.014             <10
Nickel (µg/L)                               N/A         89.0             62.7           N/A             135              104
Potassium (mg/L)                            N/A        116.0             68.0           N/A             113              97.6
Selenium (µg/L)                             N/A       <2.04            <2.04            N/A           <2.04            <2.04
Silica (mg/L)                               N/A         1.66             1.32           N/A             1.43             1.17
Silver (µg/L)                               N/A         <10              <10            N/A           <2.78            <2.78
Sulfate (mg/L)                              N/A        2,720            2,086           N/A            2,931            2,344
Total Dissolved Solids (mg/L)               N/A        4,172            3,048           N/A            4,400            3,488
Total Hardness (mg/L)                       N/A        1,351             925            N/A            1,240            1,027
Total Organic Carbon (mg/L)                 N/A         12.0             8.96           N/A             11.0             9.22
Zinc (µg/L)                                 N/A         19.0           <7.98            N/A             27.0           <7.98
Color (PCU)                                 N/A          <5               <5            N/A              <5               <5

All analyses in milligrams per Liter
unless noted.

TBR - Sample collected and submitted
to lab. Analyses not yet received.
DRY = Not sampled due to absence of
flow.
* - Analysis being challenged.
< - Analyte not detected at the
J4 - Est value quality control criteria
for accuracy not met. Standard
J4* - Est value quality control
criteria for accuracy not met.
Q - Analyzed outside accepted hold
time




     Printed On: 11/22/2011                                     of 30
                                                         Page 29C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls
                                                           Table 5
                                               Monthly Water Quality Analyses
                                                Emergency Order No. 02-1054
                                              Piney Point Phosphates Complex
                                    Date                May-04                                         June-04
                                  Station   X-1        003               X-2            X-1            003               X-2
Parameters
Alkalinity (mg/L)                           N/A          11              10             N/A             11.5              14
Aluminum (mg/L)                             N/A       <0.19            <0.19            N/A           <0.023            0.256
Arsenic (µg/L)                              N/A         2.97            2.68            N/A              <8               <8
Barium (mg/L)                               N/A      0.00903          0.0228            N/A           0.0052           0.0136
Beryllium (µg/L)                            N/A        <0.2             <0.2            N/A            <0.2             <0.2
Biochemical Oxygen Demand (mg/L)            N/A       <3.33            <3.33            N/A             11.4              <2
Cadmium (µg/L)                              N/A         0.10           <0.10            N/A              <3               <3
Calcium (mg/L)                              N/A         463             432             N/A             229              155
Chemical Oxygen Demand (mg/L)               N/A         133             <10             N/A             37.1             18.3
Chloride (mg/L)                             N/A         62.0            57.2            N/A             75.6             51.6
Chromium (µg/L)                             N/A          <1              <1             N/A              <2               <2
Radium 226 (pCi/L)                          N/A        <0.7           1.1 ± 0.6         N/A            <0.6             <0.7
Radium 228 (pCi/L)                          N/A        <1.0             <1.0            N/A            <1.0           1.7 ± 0.9
Copper (µg/L)                               N/A          <1             1.40            N/A              <4              4.40
Gross Alpha (pCi/L)                         N/A      0.8 ± 0.2        1.3 ± 0.3         N/A          1.4 ± 0.3        1.1 ± 0.3
Iron (mg/L)                                 N/A       <0.030          <0.030            N/A           0.0542            0.100
Lead (µg/L)                                 N/A          <1              <1             N/A              <3               <3
Magnesium (mg/L)                            N/A         1.29            1.09            N/A             1.50             1.01
Manganese (mg/L)                            N/A      0.00129          <0.010            N/A           <0.002           <0.002
Nickel (µg/L)                               N/A         87.8            78.0            N/A             123              87.2
Potassium (mg/L)                            N/A         83.2            87.2            N/A             116              80.8
Selenium (µg/L)                             N/A       <2.04            <2.04            N/A             9.20             23.6
Silica (mg/L)                               N/A         1.66            1.37            N/A             1.60             1.25
Silver (µg/L)                               N/A         <10             <10             N/A            <0.5             <0.5
Sulfate (mg/L)                              N/A        1,794           1,584            N/A            2,186            1,513
Total Dissolved Solids (mg/L)               N/A        2,676           2,520            N/A            3,400            2,448
Total Hardness (mg/L)                       N/A         590             539             N/A             569              392
Total Organic Carbon (mg/L)                 N/A         6.51            4.93            N/A             8.86             6.02
Zinc (µg/L)                                 N/A       <7.98            <7.98            N/A              5.3              <2
Color (PCU)                                 N/A          10              15             N/A              15               10

All analyses in milligrams per Liter
unless noted.

TBR - Sample collected and submitted
to lab. Analyses not yet received.
DRY = Not sampled due to absence of
flow.
* - Analysis being challenged.
< - Analyte not detected at the
J4 - Est value quality control criteria
for accuracy not met. Standard
J4* - Est value quality control
criteria for accuracy not met.
Q - Analyzed outside accepted hold
time




     Printed On: 11/22/2011                                     of 30
                                                         Page 30C:\Docstoc\Working\pdf\a367571c-9a74-489e-8884-adeceff0704b.xls

				
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