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B.Sc. EXAMINATION

June, 2O05

CHE-I : ATOMS AND MOI.ECUT-ES

&

\ CHE-2 : INORGAMC CHEMISTRY

Instructrons ,

7. Studenisregistered both CHE-1& CHE-2 cources

lor

shou/d onsuer both the question Impersin two

separoteonswer books entering their enrclment

number, course codeondcourse on

title cleorlg both

the answerbooks,

2, Students who hove registered CHE-1 or CHE-2

lor

should onswerthe rele\ont questionpoper ofter

entering thelr enrolmentnumber, aurse codeand

coursetitle on the onswerbook.

{.qqS. qt{r

q{, 2oo5

S.gq.{.-r , crqql sit{ €Hq!

Edt

R.q-a.d.-z: crirldRq.rrrFl

fidvr:

1. q| dr s?'Cq:d.l fr.qa.{..2

r* Etii

+ ftq rfi-fd d; ..

/ ......



'9#'

CHE.5 P.T.O.

-

(iii) RC = CR' Pd C' >

H2

Ba5O4,

' GHr)"

{iv) cH1 - cH = cH . -OH

H2O2.



(v) CH3COOH NaOH --e+

+ .. ... .



2. {a) Attempt any t.oo ol the lollowing | 2+2



lj) Which one - out ol 1,3-ieniadiene or

l,4-pentadiene - will have absorption

maximumon longer wav€length why ?

and

(ii) How will 9ou prepare.1l-nttrobenzmamine

lrorn

benzenamine (aniline)?

{iii) Write the structure of heterocycllc nucleug

present in indole alkaloids and quinolin€

alkaloids.





(b) Attempt an9 three ot the folloq,tng: 2x3

How will 9ou colvert ?

(t CHz = CH - CH2O-j-r CH2= CH-CH3



(it A --: - CqcH2cH2bH

(iii) cH3- cH : CH, -l cn, -;n - cq,

OH

{iv) cH3c= ccH3 --l- z cn.coog

..

(') Z-:r\,

\-\,

? z'v-\

----'---

lJL,

{vt) lll

\N,

\L.o.n,

3. Answerany floe of the tollowing ' 3x5

{a) Arrive ai ihe conligumiion of any luro of the

follou,lngmolecu,esusingCIP rulesi

Br _.r -H

(i) .,.,-c=ca^..

", Ln3

OH

I

(ii) cH3-9-cHo

I

H

cooH

, l

tur) H-C-OH

I

HO-C_H

I

cHs

(b) Name the symmetry clements prelent in any ,rro o{

lle following molecules :

(i) HC = CH



,.., "\^ ^,,-"'3

rr3L



?H.?H.

fl

.3 P.T.O.

(c) What do gou understand rjng chain and valence

by

tautomeisni ? Ctt€ or€ exampleo{ each.

(d) Give the reaction of nrethyl magnesiumbrcmi&

with

(t) carbondioxide

(ti) rnethylcyanide



le) Wrjte the productsof the tollowingreactions:

(r) l-propanol 573K' cu r ?





(ii) 2-methylbutanol 573K cu ) ?

A

What is the importanceol the abo\€ reactions?



Gir€ the productsobtainedv..henthe following acids

are heatedwith a mineralacid I

(i) 2-hydroxybniaroicacld

{it) 3 hldrcxybutanoicacid

{iii) 4-hydroxlbutaroicacid

{s} Ci!€ the expectedgoducts of the reactionbet'.r,/eet

ethyl benzoate the followingreagents

and r

{i) NH3, heat

aqueous

tu, Lurirl4 rotrcweoDyn3u

(iii) excess CHaMgBrfollowedfu HaO+

ol



{h) iito (i) ethanal

How can ethyleneoxide be contrerted

and (ii) erhane-l.2diol ?





CHE.5

4. Answerany tiu€ of the follo\ring : 4x5



(at I{hat is the lingerprint regto! in IR sp€ctroscopy

?

Give its utility. Whai are \.adousmediumsus€/ in

tecordlngIR spechum?



{b) Gve the mair usesof studyingmassspectnunof an

organic compolmd.What are the expectedp€aksin

the masssp€ctrumof 2,2-dimethylbutane

?



(c, Which memberof eachoI the followingpairs would

undergoSN2 reactionlaster ? Explain.

(Attemptany t4o) |

cHrcl cl

l - l

_..--\ //r\

( i ) l-.\-// l

O or lOl



t) CHz = CHCH2CI or CH3CH2CH2CI



{'ii) (CHd2CHCH2CIor (CH3)3CCI



(dl. Write short notes on any t.!ro of the following I



(i) Gattermannsynthesls



(ii) Wittg reaction



(iii) Cannizzaro reaciion



(e) Gr€ kro dilfergnf methods ot converijng

2-metiylprotranoic acid into its methyl €st€r.







P_T.O.

?

Whai is saccharln How is it manulactured Why has

?

its use be€ndsconiinuedas a sweeternng agenl ?



What G Hofrnann rearrangernent? Explain

suitableexample.



What is Reformatslg reaction ? How

3-methyl-3-hgdroxybutanoic be pr€pared

acid

z-bromoaceticacid usingthis rdction ?









CHE-5

fe*n qmo (d.qq\fr.)

sft q0{r

E;r, 2OO5

.

rtrar fo:grr

rfr.q-a.{.-sqrdfro rq*{

,

gM : Z qtti Jtelcds 3i6 : so



ria r sqfl e?T * rfr{ s?&s/

sft



r. 161 q)Frd qr€.tfr.e.m.q e&g : .r+l

frrrfrtu-r *

(i) cH3cH2ocH2cH(cH3)2

(i0 cH2 = cHcooH





(s) Frrff,tu-(n + ffi de 3rfcimqriii 1rr

sif

dFq : rx'

,u \ . l€)

' / + KoH-----+

......



r-.r Fe

tiir t2 H'r"

I

Noz



CHE-5 P.T.O.

DA-'

(iii) RC = CR' rj----::-t .

baJ!r4, n2



FHzlt' . .....

(i9 cH3-cH:cH'

w;3i

(v) CH3COOH NaOH A,

+ . .. .



z. (*) ftqfrtun t t ffi d* ss1{tuq : 2+2

(i) ].3-C€rSFfi qT r.4-qCrgF{q q q FsFqr

q-{ilsurdA nnff qi elft16.dq 3+{

A,n

?jt?

{ii) €qrq t

+S+f{ Qft-$-+) aal{iffi+$-{

fus IrdR4-{rS ?

(tit {s}d tdia,i-{ii 3*{ ffiFdq tdrdsii it

sqftqa Rq{{frq {8161 d ris{r

fttus I

(€) a{q Fqkfud sci({"il d fs€ FsR 4itt ?

(ffi di+ w{ dfqs) : 2x3



]

(0 cu"=ca _ 9urg1 rcHz=cH-cH3

(it ^ ? - -



(ii,) cHa- cH = cH2 --?- cn. - cH - cu,

- l

OH

{iv) CH.C = CCH. - i--+ 2 CH3COOH





CHE-5

--------

u



tc) Whal is the producl of photoisomerisatioir fumaric

o{

acid ? -2





(d) A mixture oi Schlorobut-1ene and 1-chlorobui-2-ene

is obiainedduring the photochemicalchlorinationof

but-2-ene. Explain the reaction with the help of

mechanism inl'lched. 3









CHE-6

6. {a) What are azo dyes ? Draw the sbucture ol any one

aza d9e,



(b) What are analgesics? Draw ihe shucture of any one

analgesic,



tc, How is soap rnanulachfed ? Why are soaps not

effective as cleanserswh€n used in hard water ? 4

(d) Name the monomer in Nylon 6 and Nylon 6, 6. 2

(e) How \^nll you prepare a dicarboxylic acid trom

diethylmalonate ? o7









CHE-6

l-5.q+T:;l

f+grrerro (d.qqfr.)

s*a q0$

Y{, 2005

TqI{r{ frArjT

fr.CES.-0,e,rdF6eftkqBii al

ffiq&

gtFl : Z Sd etfisds ni6 : so

qizt 6rd an sr# * car d&q t wi erii + aiq

sqadt



r. (s) qfq'd d]qrls d E-d-{r tfMqr{c SEsc

t

6rqqf*T{s* ers 3rFr6fiTdr + cfd{qrc4

xftltrqr Rii 6rcr * ? 2



(€) tlid{r3Trtr{$ilFl6+d qffiqr{q sr Hr 3IfEqF

{ I +@f-o fi s
iq{

dfus | 4



11;f+afrturt t +{€r ttCft." q+ot syrtdr

t

nqr eii I 3ss1 sr-jfl{ tit*+( qmqq | 4



C}

Y

1-\

o

CHE-6 7 P.T.O.

(s) tfi-d-{ d a}d-+qo } slq 3{FrBa c{ qa}

qrA sdK d {rdqr l€figq I Jsfir rupAclFr

ql {fss t 61









2 . (q) 3c{s l*+fisFr d {6rq-dl

t

3,3--gqlkdw-r,{c d 6q$u-+*16< * vm

srftFsqT cs* sffii d {rgfu dfts I

Q

1e) *ffi*q6 srq q1{;rqr { dMe qq i

fqrip-4501013rftr6- Ei 6rdri ? fuitq4

irs

w esn lofuq r

({) s, rq aqt { qqtEq{ Mi t | 3i*{-ei$ra{

c{ s s+*dqh Htd ttr t, rc n}++{

sfu

E|+r ifi d aqrq q+*d 3rh3-H{ +ff

i | 6, q dqr rT6r {wrri*$ {T qfqq I -2



(ql rif,sqq qrd aql rq 3Tdtiqr+ qrq z qer{{ *

fdfuS r iqc qi

:rqffi ii'qfiqfud 3rFrifiqr

qqrq{q d wc dftq l



3. (q) frqtutud3rFrtffisii + ffi

fr ds1 fiqrFqRT

i6{ qqf Sfts ,

(i) fsarr3rFrffrct

tio qffiq 3qFrhqr

{ ^ \

(iii) sFFIrrrqFl|frqr

(q) r+rvr-ilra {ar2)lifi-+iq;erqqcfrid sfrd +ii

dlifi E /





CHE.6

(rr) gE+fodiF|dTs6 ?{qfu6?Rqr+s{ur 6Rur

+

rqrm-$d f r effq(i {r++aii dr wqar I

Erdr

.qqlgqrd5tuffi r zi

4. (s) frqfrtud fr n +{ S ga'wirw erm*t

6ti ? ss-frffifrT S fttus I s

(t e|5+f{d 4Hq * NqFro#qr{s

til i*qr{g i tFd-{

(€) frqRtu-de$rFsqr3itn ffi #r * reR

fr

ftfuq: 3

(r) cH3- cH2- cH2- cH - cH3 alcKoH ,

- l

Bt



(iD cH. - cH"- cn" - cu - tuotcu.)rt* *Ji 5

' l

CH:



in' w HNO3

(iit -r

t o l H"SO^



Noz



cH3cH= cHcHo

zi+{ qFrs+s

M



(v)

a cHcl3, KoH







CHE-6 P.T.O.

(rr) sqFrfrqF{rur 3+{rfts t+4rur d qrst

€i

qifss r c-qs+] qe-q+r+trq si s6war

I

qcflr{q l

(s) +€Ft eqr +dt t ? qs tS srF,rFrqr

d

ffiqfi Fqlqqfss+ A-frr{q nfi fl q{cr

q

€FqtudA I z!

5. gs

(6) 3rrds6serFr+ :16r nFrs+6 Af+c ftrd

HRA I qrsr dfrs I 2 ;

(€) scg6 ffifir din Freiefur eftBrcii *

ser
rfr{fus r

oH oH









CcH
(it cH3cooc2Hs =_#

('r) Efts :rq * xqrqr-qqr+{*6{q ssK

6r

FIi 6 / 'tl

i .







(q) qe-2-i{ * vqrn-nsrqfi-+ *

4i+{t+6ior scq

:dt'ql,r,{q aqr r,mliqr-z-t+ or ftsq

c]q 6l-dr | {qt qfufud ffitI

t qi sd|{dT

t 3rF,rt*qr qrsr dfiTs r

s1



CHE.6 10

(s) tir iqs qr € ? t6{r ,t r.q tg iqo m

€{{{r ffiqq I

(q)qFrdfr q d'a t ? ffi q*fi9|Qrffsir

{r++ qqqq r

('r) Rl{4 sr sfi
qq{ 6r Tqqrrr 6q qr E Hq66If6! _ 6 5q q

_ : s





xqr4Ril {E aAt ?

(s) at{fr o asr qFefi-{ o * t+(sii fi qrq

o,

fttuq r 2

(s) i 3{rcs6sFiiffitro slq +d

qa(| I zi









CHE-6 11 3,OO0

l-cHT;l

BACHELOR OF SCIENCE (B.SC.)

Term-End Examination

June,2005



CHEMISTRY

CHE-9 : BTOCHEMISTRY



Time : 2 hours MoximumMorks: 50



Note: Answer ong lioe questions. All questions carry

equol marks,





l. (a) Define and explain the signilicance o{ ;



{t Km

(ii) Isoenzymes

(b) Name hro peptides with biological activity. Deicribe

the function of one of them briefly.





2. (a) Briefly discussdilferent stagesof protein synthesis.



(b) Differeniiate between codons and anticodons. What

is the importance of initiation' and temination

codons ? 4





CHE-9 P.T.O.

3. (a) Gi!€ a brief account of glucon€ogenesis.



(b) Give hvo etamples oI adequaie proteins. Name an9

four of the €ss€ntial amino acids.



Deline lsoelecMc point. How dd ihe amino acid

molecules b€haw in acidic or basic medium ?



4. (a) Write down the types of biological reactions with

which th€ lollowinbvtumins are associated.

Cive one

drsease each caused by the deficiency of these

vitamins I 7L

' 2



(i) Niacin

(ii) Folic acid

(iii) Biotin



{iv) Pantothenic acld

{v) Cyanocobalamine



(b) What are uncouplers and how do they act ? Gi\re one

example of an rmcoupler o1







5. Differentiate between the following pairs I ZL|"A=rc

(i) level and Oxidativephosphorylation

Substrate

(ii) DNA polymerase RNA polymerase

and

(lii) CNoroplastand Mitochondria



(iv) Competitive and Non competitive inhibition of







CHE-9

(aJ What are essentialfatty acids and why are ihey

essential

? z

{b) },{ame the ditterent lyws ot lipoprotejjnsfound in

plasma.What is ih€ir furrctional

rc\e ? 4

(c) Dscuss the impoftant functionsassociated

with an9

tour tlace elements. 4



7. Write short noteson any to r of the following :

ZNn=lO



{a) Ecosanojds

(b) r-RNA



(c) lmmobiiized€nzymes



(d) Cellularimmwtity

(eJ $phas€ of cell cycle









CHE-9

frrrc Rrca'


neiaqftqr

E{, 2oO5

TRrqqA-dtc

*a

rfr.qe.{.-s, rsrcr

gqq ; 2 qqt etfurdqai6 : 50



*e; ffi qfurn) # rar d&s r srf vr# * erq,

vqq*r



1 (d) FrEfrfud qir cffid dfqq aqr Fct qfd qi

acrqr 6ilqq :

{i) Km

(it aTqqlEq

qrA

(€) df{.s tsqFfrddr d i.zr€rii* c'F{

ftfus t

c-{qt qs * r*d w ri*c i q"fc dfqs t

2,
Sfss I

(q) *ii-c} ew vk#q) + Etq siri sc dfqq r

etttq4nqrq-qq-{dsi;ii qt q1 q5s I z



CHE-9 P.T.O.

(s) qdf{friifrv qfrridcd erqr dfrs r

(ta) ccfq *&ii * d rqrrrq €fuq r ffi qR

3rffi td+ qqfi * crq ftncE r

(rr) sqfrq-{C-€ d cffid dfuq r erei-qqqq

trtstq qiaq i QSi arc 3iq fr{ e{R 6r

a+c

4. (q) s{ qF6 efcf*qreiiS rsiii d tdfus ftiq$

f{E frfu( ffii sqfud t I {4 ffii 61

qS n,di q-d cs-c$ arnt ftloq ,

2

(il Frclkq

tii) dfu* eTq

tii0 qr+lzq

tivt Htf++ srw

(d sr{++dl.*fr-q

(s) 3rgrq6 dt t rqr i *Q sd q{a t ?

€r

ergr{ssr !$ s{€rq {feq I 2!

-2





s. fqqF{fun * fr-ssiin Rc dfuS ,

TS zlr*a=to

it frcM{ wr aqrefi+ffi sffiRd-orq

(ii} DNA ft*s lrn nNeffis

(jii) diwr€ iq 4T}strqqT

(,u) qaFq er rfrRE|rrq nqr 3Tcfr{qqitr6

€<{{

(6) exFrsd 3T€ €T dt t asTn qhsT{ s*

E{fl

€r4 E I 2

(€) +sr I qrs qraRFrf, * and++n

qr+ r-;nn

* qrqftfuc r 5+d rqrqfsq{fror m t r a

(.r) fr-
!F F6dfd

qsf 41frs | 4

7. f+4fdf€d q t GFd ar. c{ dfrF ffi

:

feFgq zfu=to

(6) 3ridtd'rs

(q) r-RNA

(r) trrqdFd qfrFq

(s) dR$tc eRqir

(s) siRrerq* qfi s-srfisr









CHE-9 3,000

BACHELOR OF SCIENCE (B.Sc.)

Term-End Examination

June,2OO5



CHE-IO: SPECTROSCOPY



Time: 2 hours MaximumMorksr 50



Note. Attempt dny tio€ qiiestions. Ali gue3fions corry

equal tnatks,



_ l. (a) Explain th€ vector nature ol orbital angular

momenfum {t). Draw the diagram showing

componeJrls anglrlarmomenhrm

ol to

corresponding





(b) Comparethe numberand type ol ax€so{ ryrnmetry

' presentin NH3 and BF3 molecules.

(c) Write tie expression relating kinetic energy and

moment of inertia. Also, give ihe significanceof

variousterms appearjngin ii.



2. {a) Siate the meaning of th€ term, group frequency.

E\plaln the use of IR spectra in strucfure

determinationusingany t'ro examples, j! 2

-







cHE-10 P.T.O.

tb) State Hooke'slaw. Also wite its rnathematical

form. .1





{c) b
(i) Zero point energy

(ii) Fundamental

transliionsand overtones

(iit Pand R branches





3. (a) Draw dlagrams illustrating streichjngand bending

ihe

vibrationsof - CHZ - group.



(b) Calculatethe stretchingand bendingmodesin CH4

moiecule. 3

(c) Explainthe terms, Stokeslines and anti-stokeslines. 2

(d) In the S-branchoI rotaiional Raman spectrum of

CO, G), a seriesof absorptionpeaksis separated by

3 16 cllir. Calc,.rlate valueol rotaiionalconstant,

the

B for COa moJecule- 2



4. (a) Derive the term slmbol for the ground state of

hydrogen|nolecule.



{b) Explain Luhy aqueous

an soJution Tiz(SOd3is red

of

purple in coiour 3

Name one source of radiation each for recording

spectrumin IR and LtV regions.









cHE-10

5. (a) Draw the block diagram of a miqowave spectrometer 3



(b) Define chemical shift. State the name and structure oi

the standard ref€rence compound used {or measuring

chemical shift. Give the names ol hro faciors that

a{fect chemica( shift. ^t

-2



(c) Fxptain why 2+ - 2



(i) ESR spectra are recorded as deri!"?tive spectra.



{ii) ESR spectrum of SO; shows a single line.



6. (a) Write short notes on the following ,



{i) Base peak

(ii) a-cleavage



(b) An organic compound having molecular formula

CoHrO showedthe lollowingspectraldata :



Massspectrum: m/z 72,43 and 57

IR spectrum.1716, 1460 and 2947 -2857 cm-r



W spectnrm : 274 nm

lH -

NMR spectrum : (6, CDC[.) :



1 0 (3H, trip:et),

247 l2H, quaftet) and

2 20 {3H' singlet)



Assign the structure of ihis compound on the basis of

the above specftal data. Also correLatevarious signals

to the structural units present in the molecule,





cHE-10 .

P . TO .

7. {a) NzO and CO2 are both linear moleculas. The bands

occur at th€ same waw numb€r in the IR and Rar,an

spectra o{ N2O wh€reas ii is not oberved for CO2.

J.rstily ihese results drawing their skeletai structufe.



Define the term, polarisahlitg of a molecule. State the

requirement for Raman band in terms of polarisabjlig.



Siate Franck- Condon principle. Using a diagram,

explain any one of the following I

(i) Predissociation

(iil Phosphorescence









-

c H E1 0

S.gq.t.-ro



G-tnqrco te1.qqs1.)

v*ia ctFr

E'r, 2oo5

d.ga.{.-ro, W'61

gqq ; 2 qv) erfuads : so

3i6

de ' fuA qFa erit * raT d&s I sE\ wit * ei6

wnq d t



l. (s) 4q-6duftq€iq tnd rRv r5ft +1erer

dfss r r= r* {'i-adurtq{+{ + qeqBt

d fu{ inr r
1uy nu, er)r BF33rEsil+ sqR-qd

{qhfd sts} 61

{iqr ett rffr d gtr+ dfvq r

(r) lfrq o-qfet s-9€ 3r1t * fiq {aiq qm

od ereld4q6ftfuq r {qfr sn+srAfrfifi

€i q1 st{6'dr \t {dr{q I

2 . (6) €T6 sn{R qq qr 3d qflqq I ffi d rqE{uil

* sc+r dnr er+m *qq +1 Tic{drfuf{oT

' q scdFnr qpa

S frfrq 1 q!

-2







cHE-10 P.r.o.

(€). gs 4r ft{q ldF€q | .asfi mrffi-q 6c S

fttus qL

-2



(rT)firiktua t f ffi- Eiqi q1qr€fl qjfuq : 2x2

(il Eq tr€ 5qt

(ii) {d €Fc'rr 3rh qFlgf6

(iit Pet R YIISI(



3. (s) - cH2 €'Td+ n'T{ r.ir rt6c d;cii d tqr

-

dRrrsfrR 6lfss I

(€) cH4xuj * fcq n-+q iifi fqqrqqR-sfud

srt'

dfuq t 3

(q) el€ 3ir cfr-€ifi' torsit q1er@Td&S r 2

(q) coz (d S Wfi nqq *qq qi s-nror ii

3 16cmI (t srA 3.q?iq"r

M +t *ofr st.a

ttft t t co, sT! * fuS qlf+ ftrni+, r *r

rrn qft-sfu(df'{s I



4. (6) 6q+i-c q.I si Td r+qr * teq qq-*irq d

E
(€) qrsfi qlfrq Fs ri2{so4)3 qd-q fffi{q sr

*

u cm-vrg$ dr dar d r

(rr) q4.6 sir qiTdrffi n +qii * 3reA€q

*i

q ff,q r+6 * kS \.s 'ira {fqq r





cHE-10

'

5. (s) W-fr.i'r dqcqrfi 4I sTRq {cFs | 3

(€) {rqrqF6 Vft +1 vftqm df$q I rrqrqFr+1ft

* qrqqii qtr+ {"+i e Gq i rs+q €rt srd

flft6 61qrq3fr{€rfl ftfus t {{FItr{ {fr

+ nl{lFd sfd A 6rGit qrqf {dFq r si

s'G *

(r) qrsr dfrq fr z+tl

{, g.sq.e{R. +edt d geq dqil 6 *

t 4di 3rFrAtud srdri t

ftqt

d-qq }-+e qs.o t€]

(ii) sot 6r {.ss.3TR.

E{txfrn d-frt t

6. (6) firqfufudqr {Rrq ffi lafuq : 4

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