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Arizona Utilities

CO2 Storage Pilot



Regional Carbon Sequestration

Partnerships Initiative Review Meeting

Pittsburgh, Pennsylvania

October 7, 2008





John Henry Beyer, Ph.D.

WESTCARB Program Manager, Geophysicist

510-486-7954, jhbeyer@lbl.gov

Lawrence Berkeley National Laboratory

Earth Sciences Division, MS 90-1116

Berkeley, CA 94720

WESTCARB region has major CO2 point sources









2

WESTCARB region has many deep saline

formations – candidates for CO2 storage









WESTCARB also created GIS layers

for oil/gas fields and deep coal basins



Source: DOE Carbon Sequestration

Atlas of the United States and Canada





3

Arizona Utilities CO2 Storage Pilot

Contracting and Funding Flow



Department of Energy Arizona Electric Power Cooperative

National Energy Technology Arizona Public Service Company

Laboratory Salt River Project

Tucson Electric Power

Lawrence Lawrence National Rural Electric Cooperative

California Energy

Berkeley National Livermore National Peabody Energy

Commission

Laboratory Laboratory









California Institute for Electric Power

Energy & Environment Research Institute

(UCOP)







– Aspen Environmental – Sandia Technologies, LLC

– Bevilacqua-Knight, Inc. – Errol L. Montgomery & Assoc.

– Schlumberger Carbon Services

– Drilling Contractor

– CO2 Supply









4

Arizona Utilities

CO2 Storage Pilot

project partners





Arizona Public Service Company

Salt River Project

Tucson Electric Power

Arizona Electric Power Cooperative

National Rural Electric Cooperative Association

Peabody Energy

Electric Power Research Institute

Lawrence Berkeley National Laboratory

Lawrence Livermore National Laboratory

California Energy Commission

U.S. Department of Energy









5

EPRI - Site Selection and Project Support







Storage potential of Arizona

geologic provinces

Significant capacity in

Colorado Plateau Province

Limited capacity in Basin and

Range Province

Minor capacity in Central

Highlands Province









6

Project Site at Arizona Public Service Company

Power Plant between Holbrook and Joseph City





Colorado Plateau location is

scientifically interesting and has

large CO2 storage potential

Potential high salinity,

carbonate reservoir formation

Thick, low permeability cap rock

Cooperative project partner that

owns surface and subsurface

rights

Near major highway, power line

Controlled access to drill site









7

Geologic section in southern Colorado Plateau









Vertical exaggeration 50:1







8

Exploratory well to confirm suitability of site

Geology at Project Site

Arizona Utilities CO2 Storage Pilot Injection Well Land Surface 5,100 Feet ASL

Proposed Completion Well Schematic

Silty Sandstone/

0

GROUND LEVEL

All depths reference Rig Kelly Bushing Moenkopi Formation Gypsum

1

Moenkopi from Surface Rig Kelly Bushing = 15’ above Ground Level 340

Ground Level ~ 5,120’

Top of Coconino +/- 225 ft Coconino Sandstone Sandstone

COMPLETION DETAILS



Fine

740

2 1. Conductor Casing: 13-3/8-inch, 48 pounds per foot, Schnebly Hill Formation Sandstone 1,000

Base of Coconino

+/- 625 ft

surface to +/-40 feet, grouted to surface

2. Surface Casing: 9-5/8-inch, 36-pounds per foot. J-55,

1,040

ST&C, Set from surface to +/-965 feet in a 12-1/4-inch

1,000 Base of Schnebly Hill hole. Cemented with Lead Slurry of 300 sacks of

“Lightweight” cement mixed at ~12.3 pounds per gallon

Siltstone

+/-925 ft

and Tail Slurry of Class “G” cement mixed at ~15.6

pounds per gallon.

Mudstone

3. Protection Casing: 5-1/2-inch 15.50 pounds per foot, J- Halite

55, LT&C. Set from surface to 4,000 feet in a 8-1/2-inch

hole. Cemented with Lead Slurry of 380 sacks of

Supai Formation

“Lightweight” Cement mixed at ~11.5 pounds per gallon

and 120 sacks of 50-50 Pozmix cement mixed at 13.5

Limestone Marker Bed 1,865

pounds per gallon. Note: The final design may include a

two stage cementing program and different cement

slurries. 1,885 2,000

3

4. Stage Tool. Will only be used if a two-stage cementing

Supai Formation Siltstone

2,000 program is required.

4

5. Injection Tubing: 2-7/8-inch, 6.5 pounds per foot, J-55, Mudstone

EUE 8rd. Surface to +/- 3,325 feet

6. Downhole completion consisting of: TAM Inflatable

Packer (set at 3,460 feet) and inflate line, w/pass through

with minor

2,525

sub on top of packer; Downhole Pressure & Temperature

Gauge and LBL Stainless Steel U-Tube Sampler below

packer. Sandstone/Dolomite

5

7. Production Perforations: Martin Fm Test Interval: 3,460

feet to 3,660 feet w/ 4 shots per foot, 90 degree phasing. 3,000

3,000

8. Planned Total Depth; +/-4,000 feet

Mudstone 3,075

Notes Naco Formation Limestone

Top of Naco Fm

The Martin Formation is the Primary Target and Sandstone

+/-2,960 ft

the Naco is the Secondary Target

Dolomite 3,575

Top of Martin Fm +/-3,460 ft

The Supai is expected to contain halite beds

below +/-1,200 feet below ground Martin Formation Mudstone 3,775

Sandia

Siltstone

7

6



Technologies, LLC

4,000

6731Theall Road, Houston, TX 77066



4,000 8 Tel: (832) 286-0471 Fax: (832) 286-0477



Drawn by: djc Date: May 2008 Drawing not to scale

Pre-Cambrian Granite

Pre-Cambrian

Basement at +/-3,660 ft Basement

Source: Sandia Technologies, LLC Source: Errol L. Montgomery & Associates







9

Evaluation of USDW above seal









Elevation and flow

TDS in Coconino

direction in

Sandstone (USDW)

Coconino Sandstone



Source: Errol L. Montgomery & Associates





10

Scientific Objectives





Determine injectivity and storage capacity of the

reservoir

Show that surface and borehole geophysical

techniques can monitor the trapping of the injected

CO2 in the subsurface

Assess and maintain caprock integrity

Demonstrate safe storage of CO2 in porous carbonate

formations containing non-potable saline water

beneath thick, low permeability seal

Develop, calibrate, and validate multiphase flow

models for CO2 injection into saline formations typical

of the Colorado Plateau in northeastern Arizona Cholla Power Plant

fly ash pond







11

Test Plan

Numerical simulation of CO2 injection

Drill and log a single well ~4,000 feet (1,200 m) deep near the APS

Cholla Power Plant fly ash pond

Ensure TDS of reservoir formation >10,000 mg/L

Step-rate injection test to determine maximum safe injection pressure

Short huff-puff test with a few tons of CO2 to estimate residual saturation,

and test water-CO2 interaction (using tracers)

Inject 2,000 tons of commercial-grade CO2

Sample fluids and tracers with U-tube system; chemical analysis

Pre- and post-CO2 injection monitoring

– Reservoir Saturation Tool (RST) logs

– Distributed Thermal Perturbation Sensor (DTPS) logs

– Vertical seismic profile (VSP) surveys

Release pressure in well and flow back fluids (water, CO2, phase-

partitioning tracers); analyze interactions





12

0

-400 Naco (L)

TOUGH2* simulation -200

Naco (U)









Z (ft)

-500

Martin









Z (ft)

of CO2 injection -400

Naco (L) -600

Injection

At end of injection

Jerome

-7000 200 400 600 800 1000

Martin

-600 X (ft)

Jerome

0 500 1000 1500 2000

Uniform high permeability 0

X (ft)



kh = kv = 100 mD Naco (U)

-200









Z (ft)

2,000 tonnes injected over 30 days (0.8 kg/s) -400

Naco (L) 1 mo. after end of injection

into Jerome Member of Martin Formation

Martin

-600

• Depth = 1,100 m (3,700 feet) Jerome

0 500 1000 1500 2000

Injection X (ft)

• P = 10.3 MPa (1,500 psi) [hydrostatic]

0

• T = 54°C (129°F) [normal gradient] Naco (U)

-200

• Porosity = 10%





Z (ft)

Naco (L) 3 mo. after end of injection

• Residual saturation, Sgr = 5% -400





SG Martin

-600

Jerome

0.50

0.45

Gas saturation 0 500 1000 1500 2000

Injection X (ft)

0.40 Fraction of

0.35 pore space 0



0.30 filled by Naco (U)

0.25 -200

supercritical CO2

Z (ft)









0.20

Naco (L)

0.15 -400 5 mo. after end of injection

0.10

0.05 Martin

* Transport Of Unsaturated -600

Jerome

0.00 Groundwater and Heat 0 500 1000 1500 2000

Injection X (ft)

0 100 200 300 400 500 600 700

meters



13

0

TOUGH2 simulation -200

Naco (U)

-500

Naco (L)









Z (ft)

Martin

of CO2 injection









Z (ft)

-600

Naco (L) At end of injection

-400 Injection

Jerome

-7000 200 400 600

High horizontal permeability -600

Martin

Jerome

X (ft)

0 500 1000 1500 2000

Low vertical permeability X (ft)

0

Naco (L)

-500

Formation Thickness kh (mD) kv (mD) Naco (U)

-200









Z (ft)

Upper Naco 76 m (250 ft) 10 1 Martin









Z (ft)

-600

Lower Naco 76 m (250 ft) 100 3 Naco (L) 1 mo. after end of injection

-400 Injection

Jerome

Upper Martin 21 m (69 ft) 100 3 -7000 200 400 600

Jerome 40 m (131 ft) 700 20 -600

Martin

X (ft)

Jerome

0 500 1000 1500 2000

2,000 tonnes injected over 30 days (0.8 kg/s) X (ft)

into Jerome Member of Martin Formation 0

Naco (L)

-500

Depth = 1,100 m (3,700 feet) -200

Naco (U)









Z (ft)

Martin









Z (ft)

P = 10.3 MPa (1500 psi) [hydrostatic] -600 5 mo. after end of injection

Naco (L)

T = 54°C (129°F) [normal gradient] -400 Injection

Jerome

-7000

Porosity = 10% Martin 200 400 600

-600 X (ft)

Jerome

Hysteretic effects included:

0 500 1000 1500 2000

– Residual saturation for drainage, Sgr = 0% X (ft)

– Residual saturation for imbibition, Sgr = 25% 0

Naco (L)

SG -500

Naco (U)

0.50 -200







Z (ft)

0.45 Martin

Z (ft)









0.40 Gas saturation -600

0.35 Fraction of -400

Naco (L) 11 mo. after end of injection

Injection

0.30 Jerome

0.25 pore space -7000 200 400 600

0.20 Martin

0.15 filled by -600

Jerome

X (ft)

0.10

0.05

supercritical CO2 0 500 1000 1500 2000

0.00

X (ft)

0 100 200 300 400 500 600 700

meters



14

TOUGH2 simulation of pressure during CO2

injection

Pressure in

reservoir formation at

injection depth



High horizontal permeability

Formation Thickness kh (mD) kv (mD)

Upper Naco 76 m (250 ft) 10 1

Lower Naco 76 m (250 ft) 100 3

Upper Martin 21 m (69 ft) 100 3

Jerome 40 m (131 ft) 700 20



Leading edge of CO2 plume

2,000 tonnes injected over 15 days (1.6 kg/s) 2.7% pressure

into Jerome Member of Martin Formation increase

• Depth = 1,100 m (3,700 feet)

• P = 10.4 MPa (1558 psi) [hydrostatic] Background hydrostatic pressure = 1558 psi

• T = 54°C (129°F) [normal gradient]

• Porosity = 10%

• Residual saturation for drainage, Sgr = 0%

0 25 50 75 100 125

meters





15

U-Tube System – continuous water, CO2, and

tracer samples at reservoir pressure





On-site

chemical

analysis









Pressurized

Packer sample

storage



Well





U-tube and check

valve strapped to

Frio Brine CO2 Pilot, Texas

production tubing

Source: Barry Freifeld, LBNL





16

Distributed Thermal Perturbation Sensor (DTPS)

for tracking CO2 migration in the subsurface



Thermal conductivity measurements

during and after CO2 injection to monitor

the distribution of CO2 near the well



The DTPS consists of a borehole-length electrical

resistance heater and fiber optic distributed

temperature sensor

Constant heating is applied along the borehole,

then is turned off. The temperature sensor

measures the decay

The low thermal conductivity of CO2 versus water

allows for estimates of CO2 saturation

The DTPS has been successfully tested at the

CO2SINK project in Germany

Source: Barry Freifeld, LBNL







17

Permitting





DOE Environmental Questionnaire/NEPA –

Approved by DOE

US EPA Region 9, UIC permit application –

Submitted for Class V Experimental Well

Aquifer Protection Program permit, Arizona

Department of Environmental Quality –

Application submitted

Drilling permit, Arizona Oil & Gas Conservation

Commission – to be submitted









18

ADEQ Aquifer Protection Program (APP) Permit





All aquifers are designated as Drinking Water Aquifers



Aquifer – a geologic unit with sufficient permeable to produce

5 gallons of water per day



Water quality is not specified in law or regulation (no TDS limit)



Use Best Available Demonstrated Control Technology (BADCT)



Point of Compliance is the location down-dip where water quality

returns to background level









19

Proposed APP Permit Conditions

Point of Compliance: 400 ft (122 m) up dip from well



VSP

Model predictions form basis of

Point of Compliance (POC)

Injection

Well

Verification:

– Lateral POC determined

Base of fresh water

by VSP

– Vertical POC determined

by RST well logs

– Injection zone Vertical POC

monitoring of pressure

Confining layer

& temperature

Naco (L)





Injection Zone Martin

Well logs

Jerome Lateral POC

(400 ft, 122 m)





20

Arizona Utilities CO2 Pilot Summary

WESTCARB has …



Completed a hydrogeologic study

Selected a site for the AZ pilot test

Added new industry partners

Characterized the hydrogeology

Modeled CO2 plume size and

formation pressure

Received NEPA approval from DOE

Submitted APP and UIC permit

applications

Engaged in public outreach to the

community through public meetings

…and will begin

Drilling and testing in January 2009







21



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