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posted:
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Health and Safety

& Risk Assessment

for users of

Brunel 007 - Composites

Manufacturing Laboratory

Staff associated with

composite modules

• Academic

– Stephen Grove,

– John Summerscales

– Mike Miles (MATS320),

– Miggy Singh (projects)



• Technicians

– Richard Cullen, Greg Nash, Richard Kenyon

• Researchers

– Richard Cullen, David Harman,

– (from 23 January 2011) Daniel Okanigbe

Principal material groups

• Resins

– unsaturated polyester (UPE)

– epoxide/epoxy (Ep)

– phenolic

• Thermoplastics

– polypropylene (PP)

– nylon (PA: polyamide)

– polyester (PET: polyethylene terephthalate)

– poly ether ether ketone (PEEK)

• Fibres

– aramid (Kevlar, Twaron)

– carbon

– glass (usually E-glass)

• Solvents, release agents, etc

Health and Safety

• Control of Substances Hazardous to Health (COSHH)

– can you substitute a safer material

– can you use an engineering solution

– are you using appropriate personal protection





• Environmental Protection Act

– you must dispose of materials in the correct manner





• A clean and tidy workplace is a safer workplace

– if you are not using it put it away

– if you must leave anything out,

make sure it is clearly labelled

Health and Safety:

Unsaturated PolyEster resin (UPE)

• base resin: polymer chains with reactive sites (50%)

• styrene: reactive diluent (50%)

– volatile

– flammable:

• flash point 31 degrees Centigrade, explosive limits 1.1-8.0%

• NO SMOKING, no naked flames

– toxic:

• (inhalation) ODOUR threshold 25 ppm (Scandinavian Occupational Exposure Limit)

– little inhalation irritation 4 g/kg of body weight

• (skin contact) IRRITATING: evident as itching and redness

– frequent or prolonged contact leads to dermatitis

– degreases skin

• (eye contact) IRRITATION may last several hours

Health and Safety:

Unsaturated PolyEster resin (UPE)

• COSHH

– substitution: resin without styrene (eg epoxy)

or low styrene emission resin

• Engineering controls

– general ventilation to reduce background level

– local exhaust ventilation with flow away from operator

– use shielded rollers to reduce droplet cloud

– protection:lab coat, barrier cream, gloves, goggles

• Disposal to waste solvent bottle if resin uncured

Health and Safety:

Unsaturated PolyEster resin (UPE)

• Peroxide Initiator (usually added as 1-2%)

– acetyl acetone peroxide (AAP), benzoyl peroxide (BzO2),

hydrogen peroxide (H2O2), methyl ethyl ketone peroxide (MEKP)

– SEVERE IRRITANTS to skin

– CAUSE BURNS: wash immediately for 15 minutes with water

and obtain doctors attention

– CORROSIVE to moist tissue (eyes, nose, throat, airways to lungs)

– Irreversible damage may be caused to eyes by prolonged contact

– avoid contact between MEKP and rust

– BzO2: EXTREME RISK OF EXPLOSION by shock, friction, fire or ignition

• COSHH

– substitution: different resin system?

– engineering controls: use as a dilute solution if practicable

– protection: protective clothing, face/eye protection

• Handle and open container with care

• Ignition: contact with combustible material may cause fire

– do not mop up with e.g. paper cloths

• Disposal do not empty into drains

Health and Safety:

Unsaturated PolyEster resin (UPE)

• Accelerators (1-2%)

– cobalt-based solutions in styrene

(cobalt naphthenate or cobalt-octoate)

– amine-based 25% solution in styrene

• TOXIC if swallowed, inhaled or

allowed to remain in contact with the skin

• FUMES from burning accelerators

contain toxic materials

Health and Safety:

Unsaturated PolyEster resin (UPE)





NEVER, NEVER mix

initiator directly with accelerator,

they will form an



EXPLOSIVE mixture

Health & Safety:

Epoxy resin (Ep)

• Base resin

– mild to moderate primary skin irritants

– irritation potential increased by prolonged

skin contact

– EPOXY SENSITIZATION:

• skin reddens in close proximity to uncured resin

• For all curing agents

– wear protective clothing and goggles

– ventilation is essential

Health & Safety:

Epoxy resin curing agents

• Aliphatic amines

– alkaline caustic materials

– cause burns and severe tissue damage to skin, mucous membranes and eyes

– ALL contact should be avoided

• Solid aromatic amines

– less caustic, less irritating and less sensitising than aliphatic amines

– diaminodiphenylmethane (DAPM) is toxic/known to cause liver damage in humans

– DAPM can be absorbed through the skin so all contact should be avoided

• Cycloaliphatic amines

– variable in their irritation and sensitising effect

– extremely irritating to the eyes

• Polyamides

– skin irritants of varying sensitivity, but generally non-sensitising to the skin

– extremely irritating to the eyes

Health & Safety:

thermoplastics



• generally chemically inert

• need to be processed at high temp.

– beware of molten polymer (hot!)

Health & Safety:

Reinforcement Fibres

• all reinforcements should be regarded as a nuisance dust

when cutting/machining

• control limits are 10 mg/m3 total dust

– 5 mg/m3 for man-made mineral fibre

• respirable dust is believed to have a particle size of <3 μm

– for safety a value of 5 μm is assumed

– the major reinforcement fibre diameters are in the range 6-15 μm

– carbon and glass fibres are not expected

to break into lengths shorter than the diameter

– aramid (and polyethylene) fibres have a complex microstructure

and may fibrillate into particles of <3 μm (respirable?)

• disposal

– All man-made fibres are a notifiable waste

and must be disposed of into the bagged bins provided

Health & Safety:

ancillary materials

• you are also likely to use ....

– solvents

– release agents

– etcetera

• read the Material Safety Data Sheet and

compile your own risk assessment

before you start work

Health & Safety:

sharps

• You will be working with

potentially dangerous chemicals

• They need not be harmful

if they are treated with respect

• The most common entries in the

Accident Book are cuts from knives

or from sharp edges on demoulding

First Aid at Work plus ...

• The nominated First Aiders for Brunel are:

– Steve Edmonds,  2.32536 Brunel W15

– Tony Tapp,  2.32539 Brunel W14

– both in laboratories near to the South door

• Cumberland Centre Minor Accident Unit  567999

• Royal Eye Infirmary  315159

• In an emergency, call Security first on 3333,

(Security can than expedite the services once on site)

then ring for external services using 9.999

Health & safety: summary

• Remember to:

• read and follow suppliers safety sheet and instructions for use

• store and handle materials in the appropriate safe way

• consider alternative materials and engineering controls

• use ventilation and fume/dust control equipment properly

• wear appropriate personal protection

• good housekeeping is essential for

your safety and that of your colleagues

Health & safety: summary

• Do not:

– smoke, eat or drink

in the laboratory or storage areas

– mix peroxide initiator with accelerators

– allow waste to accumulate

– use solvents for cleaning skin

– use combustible materials

to soak up spillage

And ...





if in doubt



ASK !!

Risk assessment

• really, this is simple:

– probability * severity = risk factor (RF)

– if RF is high, then how can it be reduced?

• http://www.tech.plym.ac.uk/sme/mats324/risk.htm

Risk assessment

• probability

1 = unlikely

2 = possible

3 = probable

• http://www.tech.plym.ac.uk/sme/mats324/risk.htm

Risk assessment

• severity

1 = minor

2 = serious

3 = critical

• http://www.tech.plym.ac.uk/sme/mats324/risk.htm

Risk assessment

• remember, risk factor is calculated

– risk factor (RF) = probability * severity

1-3 = low risk

4 = medium risk

6 or 9 = high risk

– RF cannot be 5, 7 or 8

• http://www.tech.plym.ac.uk/sme/mats324/risk.htm

Some people do stupid things …

• The winners of the competition: safety at work

• Construction workers

• The Galway Car Recovery incident

• DeWalt power tools

• Petrol tanker in Paraguay and mobile-phone-as-a-light


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