AAA Price Sheet

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Cost Proposal Schedule of Standard Rates  Equipment  Miscellaneous Equipment  Disposable Items  Protocol Pricing  Parameter Pricing  AAA Environmental Industries, Inc. 3240 West Elm Road Franklin, Wisconsin 53132 (414) 761-9421 (800) 776-7142 Page 1 Schedule of Standard Rates Effective July 1, 2002 The Personnel Protective Equipment schedule of standard rates applies to level A, B, and C protection or equivalent. Level A, B full encapsulated suits will be charged per suits donned. All other level B protection or equivalent will be charged on a daily basis regardless of the protection factor or number of tyvek suits, gloves, boots or other protective equipment donned per man. Level C protection or equivalent will be charged on a daily basis regardless of the protection factor or number of tyvek suits, gloves, boots, replacement cartridges, or other protective equipment donned per man. Notes for the Schedule of standard Rates: 1. Straight time hours for hourly personnel are based on an nine hour per day work period. The normal hourly employee workday is 7:00 a.m. to 4:00 p.m. on weekdays. Other work hours must be agreed upon in writing in advance. Time taken by personnel to decontaminate and re-don protective clothing and equipment is billed as part of the work. 2. Time over nine (9) hours in a 24 hour period during the Monday through Friday work week and until Saturday 11:00 p.m. is considered overtime and will be billed at 1.5 times the applicable straight time rate for all hourly personnel. 3. After Saturday 11:00 p.m. through Monday 7:00 a.m., holiday and day after are considered premium time and will be billed at 2.0 times the applicable straight time rate for all hourly personnel. 4. All emergency call outs after 4:00 p.m. will be subject to a one-time response charge of $50.00 per responder. This is a pass-thru charge that AAA Environmental Industries, Inc. pays to all responders in an effort to insure that they respond in a timely and professional manner. 5. Cellular phone charge of $50.00 shall be charged for emergency response jobs. For long term clean ups, a charge of cost plus twenty percent (20%) will apply. 6. Charges for safety plans are assessed on all emergency response projects or those involving OSHA Regulated Substances Site Specific Health and Safety Plans, prepared for the customer or as required by applicable regulations, will be quoted on an individual basis. 7. Lodging and subsistence of AAA ENVIRONMENTAL INDUSTRIES, INC. personnel in the area included in a per diem charge of $125.00 per person per day. AAA per diem rates are charged for subcontractors whose expenses are paid by AAA. 8. All heavy equipment (i.e. frac tank, excavator, dozer, front end loaders and large generators will be charged portal to portal (mobilization and demobilization included). Services provided prior, during and/ or subsequent to actual site activities also will be charged. 9. All times will be billed in fifteen-minute (15) increments. 10. If equipment is damaged, a repair or replacement charge will be assessed for damaged or consumable items. Those items considered consumable (single use items) will be charged per unit used. 11. Mileage for service vehicles are charged at $0.50 per mile. 12. Mileage for semi-tractors will be charged at $1.68 per mile. Page 2 Schedule of Standard Rates, continued 13. Daily rate is also for and including storage in vehicle. This pertains to material which is not compatible with our process, storage capabilities, or permit requirements, which will require controlled storage until disposal options are evaluated and actual disposal takes place. 14. Fuel for motors will be charged at actual amount used + 20%. 15. Due to the nature of hazardous chemical cleanups, it may be necessary to dispose of equipment and/ or protective clothing due to chemical action or by wear. If necessary, the above rates will be charged plus replacement cost + 20%. 16. All sub-contracting services and rental equipment charges will be billed at cost + 20%. 1. Rain for Rent 2. Lincoln Contractor 3. United Rental 4. Bartel Trucking and Excavating 5. Big Guy Trucking 6. Endeavor Environmental Services, Inc. 7. Airgas Safety Supplies 8. Milwaukee Rubber 9. Hertz 10. Premium Water Supply 11. U. S. Analytical Laboratory 12. SF Analytical Laboratory 17. The rates for analytical services may vary depending upon the turn around time and numbers of samples. AAA Environmental Industries, Inc. is committed to our customers to seek out the lowest pricing available and in most cases without a mark up. AAA has retained the services of several laboratories through out the state in an effort to obtain the best pricing for your particular needs. Laboratories that AAA currently utilize: 1. U.S. Analytical Laboratory 1090 Kennedy Ave. Kimberly, WI 54136 WI DNR Certified Lab # 445027660 Phone: 920-735-8295 2. SF- Analytical Laboratory 6125 West National Avenue P.O. Box 14513 Milwaukee, WI 53214 WI DNR Certified Lab #241249360 Phone: 800-300-6700 3. TESTAMERICA, Inc. (Watertown) P.O. Box 288 Watertown, WI 53094 WI DNR Certified Lab # 128053530 Phone: 920-261-1660 4. Environmental Monitoring and Technologies, Inc. 8100 North Austin Avenue Morton Grove, IL 60053-3203 WI DNR Certified Lab # 999888890 Phone: 847-967-6666 Page 3 Schedule of Standard Rates Effective July 1, 2002 STANDARD LABOR RATES (Monday- Friday 7:00 a.m.-4:00 p.m.) (Non-Holiday) Technician/ Driver/ Operator Equipment Operator Heavy Equipment Hauler Welder/ Mechanic Project Manager Supervisor Field Supervisor Clerical Hydrologist/ Industrial Hygienist Hydrologist Technician Incident Commander $ $ $ $ $ $ $ $ $ $ $ 45.00/ Hour 50.00/ Hour 70.00/ Hour 50.00/ Hour 65.00/ Hour 60.00/ Hour 55.00/ Hour 20.00/ Hour 85.00/ Hour 60.00/ Hour 75.00/ Hour OVERTIME RATES (Monday- Friday 4:00 p.m.- 7:00 a.m. after 4:00 p.m. Friday-Saturday 11:00 p.m.) Technician/ Drivers/ Operator $ 67.50/ Hour Equipment Operator $ 75.00/ Hour Heavy Equipment Hauler $105.00/ Hour Welder/ Mechanic $ 75.00/ Hour Project Manager $ 97.50/ Hour Supervisor $ 90.00/ Hour Field Supervisor $ 82.50/ Hour Clerical $ 30.00/ Hour Hydrologist/ Industrial Hygienist $127.50/ Hour Hydrologist Technician $ 90.00/ Hour Incident Commander $112.50/ Hour DOUBLE TIME RATES (After Saturday 11:00 p.m.- Monday 7:00 a.m. Holiday and day after) Technician/ Drivers/ Operators $ 90.00/ Hour Equipment Operator $100.00/ Hour Heavy Equipment Hauler $140.00/ Hour Welder/ Mechanic $100.00/ Hour Project Manager $130.00/ Hour Supervisor $120.00/ Hour Field Supervisor $110.00/ Hour Clerical $ 40.00/ Hour Hydrologist/ Industrial Hygienist $170.00/ Hour Hydrologist Technician $120.00/ Hour Incident Commander $150.00/ Hour Page 4 Cost Proposal Schedule of Standard Rates  Equipment  Miscellaneous Equipment  Disposable Items  Protocol Pricing  Parameter Pricing  AAA Environmental Industries, Inc. 3240 West Elm Road Franklin, Wisconsin 53132 (414) 761-9421 (800) 776-7142 Page 5 EQUIPMENT Vacuum Trucks/ Trailers and Equipment Supersucker 5500 CFM $80.00/ Hour $75.00/ Hour $68.00/ Hour $65.00/ Hour $55.00/ Hour $50.00/ Day $55.00/ Day $50.00/ Hour $45.00/ Hour (17 yard Capacity) (5,000 Gallon Capacity) (5,000 Gallon Capacity) (5,000 Gallon Capacity) (3,000 Gallon Capacity) (Mileage Included) $100.00/ Shift (Mileage Included) $100.00/ Shift $200.00/ Shift $360.00/ Shift $250.00/ Day $200.00/ Day $50.00/ Hour $50.00/ Per Person $400.00/ Shift Super Hi Vac 4000 CFM Hi Vac Vacuum Trailer Straight Truck (vacuum) Utility Truck/ Car/ Suburban Utility Truck with Lift Gate Emergency Response Trailer Skidsteer Semi-with Code Tanker Semi- with Liquid Transporter Boat with Motor Emergency Response 1800 CFM Frac Tanks 21,000 Gallon- Uncoated 21,000 Gallon- Coated 21,000 Gallon- Stainless Steel Frac Tank Hauling Frac Tank Hauling $37.00/ Day $39.00/ Day $125.00/ Day Plus 20% Plus 20% Plus 20% $70.00/ Hour Straight Time $105.00/ Hour Overtime and Weekends Heavy Equipment 4 WD Backhoe Extendahoe 450 Dozer 4,500 Lb. Excavator 8,000 Lb. Excavator 27,000 Lb. Excavator 47,000 Lb. Excavator 56,000 Lb. Excavator $200.00/ Day $250.00/ Day $350.00/ Day $175.00/ Day $225.00/ Day $375.00/ Day $525.00/ Day $625.00/ Day Plus 20% Plus 20% Plus 20% Plus 20% Plus 20% Plus 20% Plus 20% Plus 20% Heavy Equipment Hauling Heavy Equipment Hauling Page 6 $78.00/ Hour Straight Time 7:00 a.m.-4:00 p.m. $200.00/ Hour Overtime and Weekends Heavy Equipment, continued: 5.6 Generator 15 KW Generator 25 KW Generator 50 KW Generator $75.00/ Day $130.00/ Day $175.00/ Day $225.00/ Day Plus 20% Plus 20% Plus 20% Plus 20% Light Tower $115.00/ Day Plus 20% Jetting, Waterblasting, Washing Equipment 10,000 PSI Jetter 4,000 PSI Jetter 3,000 PSI Jetter Pressure Washer Hot/ Cold $80.00/ Hour $65.00/ Hour $50.00/ Hour Pumps 2” Trash Pump 3” Trash Pump 4” Trash Pump 6” Trash Pump Diaphram Pump Teflon Acid Pump Shop Vac $60.00/ Day $65.00/ Day $85.00/ Day $210.00/ Day $50.00/ Day $100.00/ Day $25.00/ Day Plus 20% Plus 20% Plus 20% Plus 20% Vacuum Hoses (if damaged) 2” Kanaflex 3” Kanaflex 4” Kanaflex 3” Petroleum 4” Petroleum 6” Kanaflex Braided $2.58/ Feet $3.99/ Feet $6.96/ Feet $9.62/ Feet $13.00/ Feet $13.98/ Feet Plus 20% Plus 20% Plus 20% Plus 20% Plus 20% Plus 20% Page 7 Cost Proposal Schedule of Standard Rates  Equipment  Miscellaneous Equipment  Disposable Items  Protocol Pricing  Parameter Pricing  AAA Environmental Industries, Inc. 3240 West Elm Road Franklin, Wisconsin 53132 (414) 761-9421 (800) 776-7142 Page 8 Miscellaneous Equipment Effective July 1, 2002 Items Video Camera Digital Camera Decontaminated Equipment Shovel- Aluminum Long Handle Shovel- Aluminum Short Handle Shovel- Plastic Hepa Vac X/ P Blower (Copus) X/ P Ice Scraper X/ P Spade Shovel Plasma Cutter (with goggles, shield, gloves, and apron) Torch (with goggles, shield, gloves, and apron) Saw Zall Blades Chop Saw Blades Drum Cart Squeegees Slik Bar Flexbin (haz) Poly Sheeting (4 mil) Poly Sheeting (6 mil) PH Paper Cubic Yard Bags Cubic Yard Box Bag House Filters (Supersucker) Drill Saw Zall Drum Gaskets Labels Radios Chop Saw Plug-N-Dike Fire Extinguisher Air Hoses Page 9 Costs $35.00/ Day $50.00/ Day $25.00/ Day $6.00/ Each $5.50/ Each $10.00/ Each $40.00/ Day $50.00/ Day $15.00/ Each $35.00/ Each $100.00/ Day $100.00/ Day $5.00/ Blade $16.00/ Blade $5.00/ Day $4.75/ Each $95.00/ 40 Feet Section $65.00/ Each $45.00/ Each $60.00/ Roll $1.00/ Test $30.00/ Each $50.00/ Each $15.00/ Bag x 60 Bags N/C N/C N/C N/C N/C N/C N/C N/C N/C Cost Proposal Schedule of Standard Rates  Equipment  Miscellaneous Equipment  Disposable Items  Protocol  Parameter Pricing  AAA Environmental Industries, Inc. 3240 West Elm Road Franklin, Wisconsin 53132 (414) 761-9421 (800) 776-7142 Disposable Items Page 10 Effective July 1, 2002 The following lists disposable items offered by AAA Environmental Industries, Inc. and the cost for each item. This list will be adjusted periodically to reflect supplier price changes. Items Push Brooms Home Brooms Fireman Boots Hip Waders Chest Waders Rain Suits Chicken Boots (included in Level B and C response) Safety Goggles (included in response) Level B Suits (includes mask, gloves, boots, and cartridge) Level C Suits (includes mask, gloves, boots, and cartridge) Tyvek suit Cotton Gloves Chemical Gloves Universal Absorbent Pads Haz Pad Absorbent Speedy Dri Vermiculite Pig 2’ X 4’ Level A Suits Haz Cat Kit Boom Socks Water Boom Containment Boom Plastic Bags (6 mil) Duct Tape Caution Tape Danger Tape Chemical Classification Kit 55 Gallon Steel Open Top Drum 55 Gallon Steel Closed Head Drum 55 Gallon Plastic Drum Page 11 Cost $12.50/ Each $9.00/ Each $125.00/ Each $37.27/ Each plus 20% $59.00/ Each plus 20% $22.00/ Each plus 20% N/C N/C $250.00/ Per Man $125.00/ Man $10.00/ Each $0.78/ Pair plus 20% $38.00/ Pair $1.00/ Each $1.10/ Each $8.00/ 50lb. Bag $14.93/ 20lb. $3.50/ Unit $850.00/ Suit $15.00/ Test $68.00/ Box $100.00/ 40 Feet $8.00/ Foot $3.50/ Bag $5.00/ Roll $7.77/ Roll $7.77/ Roll $2.00/ Test $20.00/ each $18.00/ Each $53.00/ Each Disposable Items, continued: Items 85 Gallon Steel Overpack 95 Gallon Plastic Overpack 30 Gallon Steel Open Top Drum 30 Gallon Plastic Drum 5 Gallon Steel Pail 5 Gallon Plastic Pail Nitrile Gloves (include with response) Cones Road Deflector Respirator Replacement Cartridges (included in Level C response) Cost $115.00/ Each $170.00/ Each $18.50/ Each $15.00/ Each $5.25/ Each $5.50/ Each N/C N/C N/C N/C Page 12 Cost Proposal Schedule of Standard Rates  Equipment  Miscellaneous Equipment  Disposable Items  Protocol Pricing  Parameter Pricing  AAA Environmental Industries, Inc. 3240 West Elm Road Franklin, Wisconsin 53132 (414) 761-9421 (800) 776-7142 PROTOCOL A Page 13 PROTOCOL pH Specific Gravity Total Solids Free Liquids Flash Point Arsenic Barium Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Zinc Chlorine Reactive Sulfide Phenol Reactive Cyanide Benzene Carbon Tetrachloride Chlorobenzene Chloroform o-Cresol m-Cresol p-Cresol 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethylene 2,4-Dinitrotoluene Hexachlorobenzene Heaxachloro-1.3-butadiene Hexachloroethane Methyl Ethyl Ketone Nitrobenzene Pentachlorophenol Pyridine Tetrachloroethylene Trichloroethylene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Vinyl Chloride 1 ACCEPTANCE LIMITS 2.0 < pH < 12.5 No limit No limit 0% free liquids (paint filter test) > 140 degrees F TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 1.0 mg/l TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 0.2 mg/l TCLP extraction procedure < 35.0 mg/l TCLP extraction procedure < 1.0 mg/l TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 200.0 mg/l < 1.0% * 200 ppm TCLP extraction procedure < 0.5 mg/l 200 ppm TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 6.0 mg/l TCLP extraction procedure < 200.02mg/l TCLP extraction procedure < 200.02mg/l TCLP extraction procedure < 200.02mg/l TCLP extraction procedure < 7.5 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 0.7 mg/l TCLP extraction procedure < 0.131mg/l TCLP extraction procedure < 0.131mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 3.0 mg/l TCLP extraction procedure < 200.0 mg/l TCLP extraction procedure < 2.0 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 5.01mg/l TCLP extraction procedure < 0.7 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 400.0 mg/l TCLP extraction procedure < 2.0 mg/l TCLP extraction procedure < 0.2 mg/l CONSTITUENTS *If chlorine is > 1%, the following Compounds must be analyzed: Tetrachloroethylene Trichloroethylene Methylene chloride 1,1,1-trichloroethane Carbon tetrachloride Ortho-dichlorobenzene Dichlorodifluoromethane 1,1,2 trichloro – 1,2,2 trifluoroethane trichlorofluoromethane 1,1 Dichloroethylene 1,2 Dichloroethylene Chloroform ACCEPTANCE LIMITS SUM MUST BE LESS THAN 1% OF TOTAL WEIGHT. Quantitation limit is greater than the calculated regulatory level. The quantitation limit, therefore becomes the regulatory level. If o.m-, and p-Cresol concentrations cannot be differentiated, the total Cresol (D026) concentration is used. The regulatory level for total Cresol is 200 mg/l. 2 For all constituents which are identified as TCLP extraction, it is permissible to do a totals anyalysis (on wastes which contain 0% free liquids) instead of the extraction. If the totals analysis is not over 20 times the acceptance limit, no extraction is required. Pricing: $832.00 Page 14 PROTOCOL B PROTOCOL pH Specific Gravity Total Solids Free Liquids Flash Point Arsenic Barium Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Zinc Chlorine Reactive Sulfide PCB’S Phenol Reactive Cyanide Benzene Carbon Tetrachloride Chlorobenzene Chloroform o-Cresol m-Cresol p-Cresol 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethylene 2,4-Dinitrotoluene Hexachlorobenzene Heaxachloro-1.3-butadiene Hexachloroethane Methyl Ethyl Ketone Nitrobenzene Pentachlorophenol Pyridine Tetrachloroethylene Trichloroethylene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Vinyl Chloride 1 ACCEPTANCE LIMITS 2.0 < pH < 12.5 No limit No limit 0% free liquids (paint filter test) > 140 degrees F TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 1.0 mg/l TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 0.2 mg/l TCLP extraction procedure < 35.0 mg/l TCLP extraction procedure < 1.0 mg/l TCLP extraction procedure < 5.0 mg/l TCLP extraction procedure < 200.0 mg/l < 1.0% * 200 ppm < 50 ppm TCLP extraction procedure < 0.5 mg/l 200 ppm TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 6.0 mg/l TCLP extraction procedure < 200.02mg/l TCLP extraction procedure < 200.02mg/l TCLP extraction procedure < 200.02mg/l TCLP extraction procedure < 7.5 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 0.7 mg/l TCLP extraction procedure < 0.131mg/l TCLP extraction procedure < 0.131mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 3.0 mg/l TCLP extraction procedure < 200.0 mg/l TCLP extraction procedure < 2.0 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 5.01mg/l TCLP extraction procedure < 0.7 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 400.0 mg/l TCLP extraction procedure < 2.0 mg/l TCLP extraction procedure < 0.2 mg/l CONSTITUENTS *If chlorine is > 1%, the following Compounds must be analyzed: Tetrachloroethylene Trichloroethylene Methylene chloride 1,1,1-trichloroethane Carbon tetrachloride Ortho-dichlorobenzene Dichlorodifluoromethane 1,1,2 trichloro – 1,2,2 trifluoroethane trichlorofluoromethane 1,1 Dichloroethylene 1,2 Dichloroethylene Chloroform ACCEPTANCE LIMITS SUM MUST BE LESS THAN 1% OF TOTAL WEIGHT. Quantitation limit is greater than the calculated regulatory level. The quantitation limit, therefore becomes the regulatory level. If o.m-, and p-Cresol concentrations cannot be differentiated, the total Cresol (D026) concentration is used. The regulatory level for total Cresol is 200 mg/l. 2 For all constituents which are identified as TCLP extraction, it is permissible to do a totals anyalysis (on wastes which contain 0% free liquids) instead of the extraction. If the totals analysis is not over 20 times the acceptance limit, no extraction is required. Pricing: $912.00 Page 15 PROTOCOL D-1 Underground storage tanks subject to 40 CFR 280 Regulations containing leaded, unleaded, or aviation gasoline, diesel oil #1, 2, 4, & 6 or crude oil, lube oil. PROTOCOL Free Liquids Flash Point Lead Benezene GRO (for all gasoline, Mineral spirits, stoddard ACCEPTANCE LIMITS 0% freee liquids (paint filter test) > 1400 F (close cup) TCLP Extraction procedure < 5.0 mg/l* TCLP Extraction procedure < 0.5 ppm * < 2000 ppm < 2000 ppm ANALYTICAL EPA 9095 EPA Methods EPA Methods EPA Methods Wisconsin DNR Modified GRO Wisconsin DNR Modified DRO DRO (for diesel, jet Fuel, kerosene, #1, 2 & 4 or fuel oil, Crude oil, lube oil) For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis if < 20 times the regulatory levels. If the totals analysis is > 20 times regulatory limits, the TCLP extraction is required. TCLP extraction is required for benzene if tank is not regulated under 40 CFR 280. Lead test is only required for gasoline. The laboratory report must include the following information: 1) 2) 3) 4) 5) 6) 7) 8) Sample type, description, and location. The type of sample preservation. The sample integrity upon receipt by the lab. Temperature of the sample when received. The analytical methods used to analyze the sample. Sample results. The laboratory limits of detection. Data sampled, received, extracted and analyzed. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: $314.00 Page 16 PROTOCOL D-2 Underground storage tanks subject to 40 CFR 280 Regulations containing waste oil or unknown petroleum products. PROTOCOL Free Liquids Flash Point Lead Cadmium Reactive Cyanide Reactive Sulfides GRO (unknown petroleum) DRO (unknown petroleum) (waste oil) ACCEPTANCE LIMITS 0% free liquids (paint filter test) > 140o F TCLP Extraction procedure <5.0 mg/l* TCLP Extraction procedure <1.0 mg/l* <200 ppm ** <200 ppm *** <2000 ppm <2000 ppm ANALYTICAL EPA 9095 EPA Methods EPA Methods EPA Methods SW 846 SW 846 Wisconsin DNR Modified GRO Wisconsin DNR Modified DRO * For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis if <20 times the regulatory levels. If the totals analysis is >20 times regulatory limits, the TCLP extraction is required. TCLP extraction is required for benzene if tank is not regulated under 40 CFR 280. For facilities which have purchased cyanide or performed metal finishing such as heat treating, stripping, or plating. For facilities which purchased metal cutting oils or performed metal finishing. ** *** The laboratory report must include the following information: 1) 2) 3) 4) 5) 6) 7) Sample type, description, and location. The type of sample preservation. The sample integrity upon receipt by the lab. The analytical methods used to analyze the sample. Sample results. The laboratory limits of detection. Data sampled, received, extracted and analyzed. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: $447.00 Page 17 PROTOCOL D-3 Above ground tanks or spills of petroleum contaminated soils of gasoline, diesel fuel oil or new petroleum products. PROTOCOL Free Liquids Flash Point Lead Benzene Carbon Tetrachloride Chlorobenzene Chloroform o-Cresol m-Cresol p-Cresol 1,4 – Dichlorobenzene 1,2 – Dichloroethane 1,1 – Dichloroethylene 2,4 – Dinitrotoluene Hexachlorobenzene Hexachloro – 1.3 - butadiene Hexachloroethane Methyl Ethyl Ketone Nitrobenzene Pentachlorophenol Pyridine Tetrachloroethylene Trichloroethylene 2,4,5 – Trichlorophenol 2,4,6 – Trichlorophenol Vinyl Chloride DRO (for diesel, jet fuel, kerosene, #1, 2 or 4 Fuel oil, crude oil, lube oil) GRO (for all gasolines, mineral spirits, Stoddard Solvent, texsolve, naphtha) 1 ACCEPTANCE LIMITS 0% free liquids (paint filter test) > 140o F TCLP extraction procedure < 5.0 mg/l3 TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 6.0 mg/l TCLP extraction procedure < 200.02 mg/l TCLP extraction procedure < 200.02 mg/l TCLP extraction procedure < 200.02 mg/l TCLP extraction procedure < 7.5 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 0.7 mg/l TCLP extraction procedure < 0.131 mg/l TCLP extraction procedure < 0.131 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 3.0 mg/l TCLP extraction procedure < 200.0 mg/l TCLP extraction procedure < 2.0 mg/l TCLP extraction procedure < 100.0 mg/l TCLP extraction procedure < 5.01 mg/l TCLP extraction procedure < 0.7 mg/l TCLP extraction procedure < 0.5 mg/l TCLP extraction procedure < 400.0 mg/l TCLP extraction procedure < 2.0 mg/l TCLP extraction procedure < 0.2 mg/l < 2000 ppm < 2000 ppm Quantitation limits is greater than the calculated regulatory level. The quantitation limit therefore becomes the regulatory level. If o,m– and p–Cresol concentration cannot be differentiated, the total Cresol (D026) concentration is used. The regulatory level for total Cresol is 200 mg/l Lead test to be performed on leaded gasoline, or unknown petroleum containing tank. 2 3 For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis instead of the extraction. If the total analysis is not over the acceptance limit no extraction is required. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: Page 18 $719.00 PROTOCOL D – 4 Above ground tanks or spills of waste oil contaminated soils. PROTOCOL ACCEPTANCE LIMITS Constituents ACCEPTANCE Free liquids 0% free liquids (paint filter test) *If clorine is > 1%, the LIMITS Flash point > 1400 F (closed cup) following compounds SUM MUST BE Lead TCLP Extraction procedure <5.0 mg/l* must be analyzed LESS THAN 1% Chlorine < 1.0% * tetrachlorethylene OF TOTAL PCB’S < 50 ppm trichloroethylene WEIGHT. Benzene TCLP Extraction procedure < 0.5 mg/l methylene chloride Carbon Tetrachloride TCLP Extraction procedure < 0.5 mg/l. 1, 1, 1 - trichlorothane Chlorobenzene TCLP Extraction procedure < 100.0 mg/l carbon tetrachloride Chloroform TCLP Extraction procedure < 6.0 mg/l chlorlform o-Cresol TCLP Extraction procedure < 200.0 2 mg/l ortho – dichlorobenzene m-Cresol TCLP Extraction procedure < 200.0 2 mg/l dichlorodifluoromethane p-Cresol TCLP Extraction procedure < 200.02mg/l 1, 1, 2 trichloro – 1,2,2 trifluoroethane 1, 4 Dichlorobenzene TCLP Extraction procedure <7.5 mg/l trichlorofluormethane1 1, 2 – Dichloroethane TCLP Extraction procedure < 0.5 mg/l 1, 1 dichloroethylene 1, 1 – Dichloroethylene TCLP Extraction procedure < 0.7 mg/l 1, 2 dichloroethylene 2, 4 – Dinitrotoluene TCLP Extraction procedure < 0.131 mg/l Hexachlorobenzene TCLP Extraction procedure <0.13 1 mg/l Hexachloro- 1.3 – butadiene TCLP Extraction procedure <0.5 mg/l Hexachloroethane TCLP Extraction procedure <3.0 mg/l Methyl Ethyl Ketone TCLP Extraction procedure < 200.0 mg/l Nitrobenzene TCLP Extraction procedure <2.0 mg/l Pentachlorophenol TCLP Extraction procedure < 100.0 mg/l Pyridine TCLP Extraction procedures <5.0 1 mg/l Tetrachloroethylene TCLP Extraction procedures <0.7 mg/l Trichloroethylene TCLP extraction procedures <0.5 mg/l 2, 4, 5 – Trichlorophenol TCLP Extraction procedures < 400.0 mg/l 2, 4, 6 – Trichlorophenol TCLP Extraction procedures < 2.0 mg/l Vinyl Chloride TCLP Extraction procedures < 0.2 mg/l DRO (for diesel, jet fuel, < 2000 ppm Kerosene, #1, 2, 4, or #6 fuel Oil, crude oil, lube oil) GRO (for all gasolines, mineral < 2000 ppm Spirits, stoddard solvent, texsolve, Naphtha) *Quantitation limits is greater than the calculated regulatory level. The quantitation limit therefore becomes the regulatory level. *If o, m – and p – Cresol concentration cannot be differentiated, the total Cresol (D026) concentration is used. The regulatory level for total Cresol is 200 mg/l *For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis instead of the extraction. If the total analysis is not over the acceptance limit no extraction is required. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: $809.00 Page 18 PROTOCOL BIO - 1 Underground storage tanks subject to 40 CFR 280 Regulations containing leaded, unleaded, or aviation gasoline, diesel oil #1, 2, 4, & 6 or crude oil, lube oil. PROTOCOL Lead Benezene ACCEPTANCE LIMITS TCLP Extraction procedure <5.0 mg/l* No Limits ANALYTICAL METHODS EPA Methods EPA Methods Wisconsin DNR Modified GRO GRO (for all gasoline, No Limits Mineral spirits, stoddard Solvent, texsolve, naphtha) DRO (for diesel, jet fuel, No Limits Kerosene, #1, 2, 4, or 6 fuel oil, Crude oil, lube oil) Wisconsin DNR Modified DRO For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis if <20 times the regulatory levels. If the totals analysis is >20 times regulatory limits, the TCLP extraction is required. TCLP extraction is required for benzene if tank is not regulated under 40 CFR 280. Lead test is only required for gasoline. The laboratory report must include the following information: 1. 2. 3. 4. 5. 6. 7. 8. Sample type, description, and location. The type of sample preservation. The sample integrity upon receipt by the lab. Temperature of the sample when received. The analytical methods used to analyze the sample. Sample results. The laboratory limits of detection. Data sampled, received, extracted and analyzed. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: $284.00 Page 19 PROTOCOL BIO - 2 Underground storage tanks subject to 40 CFR 280 Regulations containing waste oil or unknown petroleum products. PROTOCOL Lead Cadmium Reactive Cyanide Reactive Sulfides ACCEPTANCE LIMITS ANALYTICAL METHODS TCLP Extraction procedure <5.0 mg/l* EPA Methods TCLP Extraction procedure <1.0 mg/l <200 ppm ** <200 ppm EPA Methods SW 846 SW 846 GRO (Unknown petroleum) No Limits Wisconsin DNR Modified GRO DRO (Unknown petroleum waste oil) No Limits Wisconsin DNR Modified DRO *For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis if <20 times the regulatory levels. If the totals analysis is >20 times regulatory limits, the TCLP extraction is required. TCLP extraction is required for benzene if tank is not regulated under 40 CFR 280. **For facilities which have purchased cyanide or performed metal finishing such as heat treating, stripping, or plating. *** For facilities which purchased metal cutting oils or performed metal finishing. The laboratory report must include the following information: 1) 2) 3) 4) 5) 6) 7) Sample type, description, and location. The type of sample preservation. The sample integrity upon receipt by the lab. The analytical methods used to analyze the sample. Sample results. The laboratory limits of detection. Data sampled, received, extracted and analyzed. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: $277.00 Page 20 PROTOCOL BIO - 3 Above ground tanks or spills of petroleum contaminated soils of gasoline, diesel fuel oil or new petroleum products. PROTOCOL ACCEPTANCE LIMITS Lead TCLP Extraction procedure <5.0 mg/l* Benzene TCLP Extraction procedure < 0.5 mg/l Carbon Tetrachloride TCLP Extraction procedure < 0.5 mg/l Chlorobenzene TCLP Extraction procedure < 100.0 mg/l Chloroform TCLP Extraction procedure < 6.0 mg/l o-Cresol TCLP Extraction procedure < 200.0 2 mg/l m-Cresol TCLP Extraction procedure < 200.0 2 mg/l p-Cresol TCLP Extraction procedure <200.02 mg/l 1, 4 – Dichlorobenzene TCLP Extraction procedure <7.5 mg/l 1 , 2 – Dichloroethane TCLP Extraction procedure < 0.5 mg/l 1, 1 – Dichloroethylene TCLP Extraction procedure < 0.7 mg/l 2, 4 – Dinitrotoluene TCLP Extraction procedure < 0.13 1 mg/l Hexachlorobenzene TCLP Extraction procedure <0.13 1 mg/l Hexachloro- 1.3 – butadiene TCLP Extraction procedure <0.5 mg/l Hexachloroethane TCLP Extraction procedure <3.0 mg/l Methyl Ethyl Ketone TCLP Extraction procedure < 200.0 mg/l Nitrobenzene TCLP Extraction procedure <2.0 mg/l Pentachlorophenol TCLP Extraction procedure < 100.0 mg/l Pyridine TCLP Extraction procedures <5.0 1 mg/l Tetrachloroethylene TCLP Extraction procedures <0.7 mg/l Trichloroethylene TCLP extraction procedures <0.5 mg/l 2, 4, 5 – Trichlorophenol TCLP Extraction procedures < 400.0 mg/l 2, 4, 6 – Trichlorophenol TCLP Extraction procedures < 2.0 mg/l Vinyl Chloride TCLP Extraction procedures < 0.2 mg/l DRO (Kerosine, Lube Oil, #2, 4, 6 Fuel Oil, Crude Oil, Diesel, Jet Fuels) No Limits GRO (for all gasolines, mineral Spirits, stoddard solvent, texsolve, Naphtha) No Limits *Quantitation limits is greater than the calculated regulatory level. The quantitation limit therefore becomes the regulatory level. *If o, m – and p – Cresol concentration cannot be differentiated, the total Cresol (D026) concentration is used. The regulatory level for total Cresol is 200 mg/l *Lead test to be performed on leaded gasoline, or unknown petroleum containing tank. *For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis instead of the extraction. If the total analysis is not over the acceptance limit no extraction is required. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: $744.00 Page 21 PROTOCOL BIO - 4 Above ground tanks or spills of waste oil contaminated soil. PROTOCOL Lead Chlorine PCB’S Benzene Carbon Tetrachloride Chlorobenzene Chloroform o-Cresol m-Cresol p-Cresol 1, 4 – Dichlorobenzene 1 , 2 – Dichloroethane 1, 1 – Dichloroethylene 2, 4 – Dinitrotoluene Hexachlorobenzene Hexachloro- 1.3 – butadiene Hexachloroethane Methyl Ethyl Ketone Nitrobenzene Pentachlorophenol Pyridine Tetrachloroethylene Trichloroethylene 2, 4, 5 – Trichlorophenol 2, 4, 6 – Trichlorophenol Vinyl Chloride ACCEPTANCE LIMITS TCLP Extraction procedure <5.0 mg/l* <1.0% < Detection limits TCLP Extraction procedure < 0.5 mg/l TCLP Extraction procedure < 0.5 mg/l TCLP Extraction procedure < 100.0 mg/l TCLP Extraction procedure < 6.0 mg/l TCLP Extraction procedure < 200.0 2 mg/l TCLP Extraction procedure < 200.02 mg/l TCLP Extraction procedure <200. 2 mg/l TCLP Extraction procedure <7.5 mg/l TCLP Extraction procedure < 0.5 mg/l TCLP Extraction procedure < 0.7 mg/l TCLP Extraction procedure < 0.131 mg/l TCLP Extraction procedure <0.13 1 mg/l TCLP Extraction procedure <0.5 mg/l TCLP Extraction procedure <3.0 mg/l TCLP Extraction procedure < 200.0 mg/l TCLP Extraction procedure <2.0 mg/l TCLP Extraction procedure < 100.0 mg/l TCLP Extraction procedures <5.0 1 mg/l TCLP Extraction procedures <0.7 mg/l TCLP extraction procedures <0.5 mg/l TCLP Extraction procedures < 400.0 mg/l TCLP Extraction procedures < 2.0 mg/l TCLP Extraction procedures < 0.2 mg/l *Quantitation limits is greater than the calculated regulatory level. The quantitation limit therefore becomes the regulatory level. *If o, m – and p – Cresol concentration cannot be differentiated, the total Cresol (D026) concentration is used. The regulatory level for total Cresol is 200 mg/l *For all constituents which are identified as TCLP extractions, it is permissible to do a total analysis instead of the extraction. If the total analysis is not over the acceptance limit no extraction is required. Note: All analytical must be performed by WDNR certified laboratory or Waste Management certified laboratory. Pricing: $776.00 Page 22 Cost Proposal Schedule of Standard Rates  Equipment  Miscellaneous Equipment  Disposable Items  Protocol Pricing  Parameter Pricing  AAA Environmental Industries, Inc. 3240 West Elm Road Franklin, Wisconsin 53132 (414) 761-9421 (800) 776-7142 Page 23 WATER AND WASTEWATER TESTS PERFORMED – 2002 PRICES Parameter Alkalinity Aluminum Aluminum Ammonia Antimony Antimony Arsenic Arsenic Barium Beryllium Beryllium BOD5 Boron Bromide Cadmium Cadmium Calcium Chloride Chlorine Chromium Chromium Cobalt Cobalt COD Conductivity Copper Copper Copper (Drinking Water) Cyanide Dissolved Oxygen Fluoride Hexavalent Chromium Iron Lead Lead Lead (Drinking Water) Magnesium Manganese Mercury Mercury (low level) Molybdenum Nickel Nickel Method* *310.1 SM3111B, 6010B SM3113B *350.1 SM3111B, 6010B SM3113B *6010B SM3113B SM3111B, 6010B SM3111B, 6010B SM3113B *405.1 *6010B *300.0 SM3111B, 6010B SM3113B 6010B *300.0 *331.3, 331.5 SM3111B, 6010B SM3113B SM3111B, 6010B SM3113B *410.4 *121.1 SM3111B, 6010B SM3113B SM3111B *335.1, 335.2 *360.2 *340.1, 300.0 SM 3500-CR D SM3111B, 6010B SM3111B, 6010B SM3113B SM3113B 6010B 6010B *245.1 *245.1 6010B SM3111B, 6010B SM3113B Limit of Detection 0.86 mg/L 0.1 mg/L 1 ug/L 0.04 mg/L 0.1 mg/L 1 ug/L 0.06 mg/L 1.1 ug/L 0.006 mg/L 0.004 mg/L 0.03 ug/L 2 mg/L 0.1 mg/L 0.007 mg/L 0.010 mg/L 0.06 ug/L 0.2 mg/L 0.231 mg/L 0.1, 0.031 mg/L 0.01 mg/L 0.4 ug/L 0.03 mg/L 1 ug/L 6 mg/L 1 umho/CM 0.02 mg/L 0.8 ug/L 4 ug/L 2 ug/L 0.2 mg/L 0.09, 0.022 mg/L 2.52 ug/L 0.04 mg/L 0.04 mg/L 1 ug/L 1 ug/L 0.2 mg/L 0.01 mg/L 0.04 ug/L 0.02 ug/L 0.06 mg/L 0.04 mg/L 1.3 ug/L Cost $21.00 $16.50 $31.00 $24.00 $16.50 $31.00 $16.50 $31.00 $16.50 $16.50 $16.50 $31.00 $16.50 $21.00 $16.50 $31.00 $16.50 $21.00 $25.00 $16.50 $31.00 $16.50 $31.00 $25.00 $15.00 $16.50 $31.00 $17.00 $35.00 $15.00 $21.00 $25.00 $16.50 $16.50 $31.00 $31.00 $16.50 $16.50 $32.00 $75.00 $16.50 $16.50 $31.00 Page 24 WATER AND WASTEWATER TESTS PERFORMED – 2002 PRICES Continued Parameter Nitrate Nitrates (NO3 + NO2) Nitrate Oil & Grease (grav) Oil & Grease (grav. TRPH) Oil & Grease (HEV) Oil & Grease (TRO&G) Oil & Grease (TRPH) Orthophosphate pH Phenols Phosphorus Potassium Selenium Selenium Silica Silver Silver Sodium Sulfate Sulfide Thallium Tin Titanium Total Dissolved Solids Total Hardness Total Kjeldahl Nitrogen Total Solids Total Suspended Solids Turbidity Zinc Method* *300.00 *300.00 *300.00 *413.1 SM 5521 F *1664 *413.2 *418.1 *365.2, 300.0 *150.1 *421.1 *365.2 6010B 6010B SM3113B *370.1 SM3111B SM3113B 6010B *300.0 *376.1 SM3113B 6010B 6010B *160.1 *131.2 *351.3 *160.3 *160.2 *180.1 SM3111B, 6010B Limit of Detection 0.013 mg/L 0.02 mg/L 0.02 mg/L 2 mg/L 0.5 mg/L 1.3 mg/L 0.05 mg/L 0.05 mg/L 0.058 mg/L N.A. 0.005 mg/L 0.01 mg/L 0.2 mg/L 0.08 mg/L 2.4 ug/L 0.02 mg/L 0.01 mg/L 0.2 ug/L 0.2 mg/L 0.052 mg/L 0.1 mg/L 0.9 ug/L 0.2 mg/L 0.02 mg/L 1 mg/L 1 mg/L 0.1 mg/L 1 mg/L 1 mg/L 0.1 NTU 0.02 mg/L Cost $21.00 $25.00 $21.00 $37.00 $60.00 $50.00 $60.00 $60.00 $21.00 $ 7.00 $38.00 $24.00 $16.50 $16.50 $31.00 $21.00 $26.00 $31.00 $16.50 $21.00 $31.00 $31.00 $16.50 $16.50 $18.00 $25.00 $30.00 $18.00 $18.00 $18.00 $16.50 *EPA Method Number SM – Standard Methods for the Examination of Water and Wastewater # Furnace Method Note: A $15.00 digestion fee will be added to the first metal of a group of flame or furnace metals. SLUDGE ANALYSIS PRICE LIST – 2002 PRICES PARAMETER EPA Metals (10) List Nutrients List 1 Fecal Coliforms PCB’s Radium 226 Cyanide Silver Total Solids, Volatile Solids DESCRIPTION As, Cd, Cr, Cu, Pb, Hg, Mo, Ni, Se, Zn Solids, TKN, NH3-N, P, K, pH Metals + Nutrients (same sample) 7 Samples with Total Solids Subcontracted Subcontracted Added to above list PRICE $190.00 $194.25 $219.00 $301.25 $115.25 $134.00 $51.50 $15.50 $15.50 PAINT ANALYSIS PRICE LIST – 2002 PRICES Page 25 Acid Value PARAMETER Density/Specific Gravity Nonsustainable combustibility DESCRIPTION D1639-90 D1475-90 DOT PRICE $27.00 $33.75 $114.50 GENERAL ANALYSIS PRICE LIST – 2002 PRICES PARAMETER Ash BTU/pound Bromine Carbon, Hydrogen Carbon, Hydrogen, Nitrogen Chloroform Extract Chromic Oxide Fluroine Halogens, Total Heavy Metals as Pb Lime Neut. Index (AOAC) Loss of Ignition (LOI) Mercury Metals, each required preparation Metals, FAAS Metals, GFAAS Metals, ICP Moisture (see also Water) Nitrogen Nitrogen Paranitrophenol (PNP) Proximate Analysis Sand Analysis Sieve Analysis Sieve Analysis, wet Solids, Total Solids, Volatile Sulfide Sulfur Total Sulfur Total TRPH Total Halogens as CI Viscosity Volatile Matter Water Water pH DESCRIPTION Coal, coke, etc. Bomb method Bomb/ISE Leco CHN-600 Leco CHN-600 Leather (ALCA) Leather (ALCA) Bomb/ISE Bomb method USP/FCC Cold vapor AAS Sample digestion Each metal, prepared samples Each metal, prepared samples Each metal, prepared samples Kjeldahl, solid sample Leco, solid sample Leather Coal, coke, etc. Moist, Vol, Ash, Sulfur Si, Al, Fe, Ti, Ca, Mg, Na, K, LOI, ph Up to six sieves Up to six sieves Oven method SW 846 (solid samples, total) Bomb method Leco IR method Bomb method Brookfield Coal, coke, etc. Karl-Fisher Distillation Solid samples PRICE $23.75 $46.25 $43.00 $58.75 $97.75 $29.75 $39.50 $43.00 $41.50 $65.50 $44.50 $23.75 $32.50 $28.00 $19.25 $19.75 $13.50 $28.50 $39.50 $71.75 $82.50 $112.25 $225.75 $45.50 $80.25 $23.75 $28.75 $48.50 $39.50 $41.50 $107.75 $39.50 $40.75 $28.50 $38.25 $42.50 $19.25 Page 26

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